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At least 793 records · Page 44
All sourcesNASA NTRSDOE OSTI
NASA NTRS2020

The Chlorine-Isotopic Composition of Lunar KREEP From Magnesian-Suite Troctolite 76535

We conducted in-situ Cl isotopic measurements of apatite within intercumulus regions and within a holocrystalline olivine-hosted melt inclusion in magnesian-suite troctolite 76535 from Apollo 17. These data were collected to place constraints on the Cl-isotopic composition of the last liquid to crystallize from the lunar magma ocean (i.e., urKREEP, named after its enrichments in incompatible lithophile trace elements like potassium, rare earth elements, and phosphorus). The apatite in the olivine-hosted melt inclusion and within the intercumulus regions of the sample yielded Cl-isotopic compositions of 28.3 ± 0.9 ‰ (2σ) and 30.3 ± 1.1 ‰ (2σ), respectively. The concordance of these values from both textural regimes we analyzed indicates that the Cl-isotopic composition of apatites in 76535 likely represents the Cl-isotopic composition of the KREEP-rich magnesian-suite magmas. Based on the age of 76535, these results imply that the KREEP reservoir attained a Cl-isotopic composition of 28–30 ‰ by at least 4.31 Ga, consistent with the onset of Cl-isotopic fractionation at the time of lunar magma ocean crystallization or shortly thereafter. Moreover, lunar samples that yield Cl-isotopic compositions higher than the value for KREEP are likely affected by secondary processes such as impacts and/or magmatic degassing. The presence of KREEP-rich olivine-hosted melt inclusions within one of the most pristine and ancient KREEP-rich rocks from the Moon provides a new opportunity to characterize the geochemistry of KREEP. In particular, a broader analysis of stable isotopic compositions of highly and moderately volatile elements could provide an unprecedented advancement in our characterization of the geochemical composition of the KREEP reservoir and of volatile-depletion processes during magma ocean crystallization, more broadly.

Francis M. McCubbin↗
NASA NTRS2008

Effects of High-Temperature Annealing in Air on Hi-Nicalon Fiber-Reinforced Celsian Matrix Composites

BN/SiC-coated Hi-Nicalon fiber-reinforced celsian matrix composites (CMC) were annealed for 100 h in air at various temperatures to 1200 C, followed by flexural strength measurements at room temperature. Values of yield stress and strain, ultimate strength, and composite modulus remain almost unchanged for samples annealed up to 1100 C. A thin porous layer formed on the surface of the 1100 C annealed sample and its density decreased from 3.09 to 2.90 g/cu cm. The specimen annealed at 1200 C gained 0.43 wt%, was severely deformed, and was covered with a porous layer of thick shiny glaze which could be easily peeled off. Some gas bubbles were also present on the surface. This surface layer consisted of elongated crystals of monoclinic celsian and some amorphous phase(s). The fibers in this surface ply of the CMC had broken into small pieces. The fiber-matrix interface strength was characterized through fiber push-in technique. Values of debond stress, alpha(sub d), and frictional sliding stress, tau(sub f), for the as-fabricated CMC were 0.31+/-0.14 GPa and 10.4+/-3.1 MPa, respectively. These values compared with 0.53+/-0.47 GPa and 8.33+/-1.72 MPa for the fibers in the interior of the 1200 C annealed sample, indicating hardly any change in fiber-matrix interface strength. The effects of thermal aging on microstructure were investigated using scanning electron microscopy. Only the surface ply of the 1200 C annealed specimens had degraded from oxidation whereas the bulk interior part of the CMC was unaffected. A mechanism is proposed explaining the various steps involved during the degradation of the CMC on annealing in air at 1200 C.

Bansal, Narottam P.↗
NASA NTRS2024

Investigating Bennu’s Volatile Accretion History Through Step-Heating N-Ne-Ar Analyses of Single Aggregate Particles

NASA’s OSIRIS-REx spacecraft delivered a sample from the carbonaceous asteroid (101955) Bennu to Earth on September 24, 2023. Since Bennu presumably accreted in the outer protoplanetary disk, beyond Jupiter’s orbit, the collected material is expected to be rich in highly volatile elements such as H, C, N, and noble gases—similar to Ivuna-type (CI) carbonaceous chondrites and material from asteroid (162173) Ryugu returned by JAXA’s Hayabusa2 spacecraft. This type of material may have contributed to the volatile inventory of Earth and the other terrestrial planets. Bulk CI chondrites record a narrow range of δ 15 N values (i.e., the permil difference from the atmospheric 15 N/ 14 N ratio), averaging between +42 and 49‰. In contrast, recent analyses at CRPG’s noble gas facility revealed that two pelletized Ryugu samples have lower δ 15 N values of +18.1 ± 0.9‰ and +19.5 ± 0.9‰. Together with the low measured N abundances, this observation suggests that Ryugu has lost a 15 N-rich, labile organic phase due to pervasive aqueous alteration. Subsequent high-resolution step-heating analyses of an additional Ryugu particle demonstrated that the δ 15 N value varies significantly during successive extraction steps (between +1.0 ± 1.0‰ and 65.8 ± 1.1‰); the variable N isotopic composition points to the presence of several isotopically distinct N-carrier phases in CI-type material. Here, we report preliminary N-Ne-Ar results obtained for individual particles from an aggregate Bennu sample using the Noblesse-HR (Nu Instruments) noble gas mass spectrometer at CRPG’s noble gas facility. In a companion abstract, we will present the noble gas (He, Ne, Ar, Kr, Xe) characteristics of other aggregate particles determined with a HELIX MC Plus. Whereas the abundance and isotopic composition of noble gases permit detection of various presolar phases and the so-called phase Q, as well as quantification of solar wind–derived and cosmogenic components, the abundance and isotopic composition of N are expected to provide further insights into the origin and evolution of N-bearing phases in carbonaceous asteroids.

E Füri↗
NASA NTRS2013

Sample Tube Sealing for Future Proposed Mars Sample Return Missions

A key premise of a proposed Sample Caching Rover, a crucial element of the proposed Mars Sample Return (MSR) campaign, is that the samples could be packaged and left on Mars for an extended period of time (at least five Mars years) without loss of scientific value (Fig. 1). The MEPAG E2E-iSAG (2011) concluded that the single most important factor in preserving the scientific integrity of the samples during the interval between their collection and their analysis is effective sealing of the samples.

sample integrity↗
NASA NTRS1983

Design, implementation and flight testing of PIF autopilots for general aviation aircraft

The designs of Proportional-Integrated-Filter (PIF) auto-pilots for a General Aviation (NAVION) aircraft are presented. The PIF autopilot uses the sampled-data regulator and command generator tracking to determine roll select, pitch select, heading select, altitude select and localizer/glideslope capture and hold autopilot modes. The PIF control law uses typical General Aviation sensors for state feedback, command error integration for command tracking, digital complementary filtering and analog prefiltering for sensor noise suppression, a control filter for computation delay accommodation and the incremental form to eliminate trim values in implementation. Theoretical developments described in detail, were needed to combine the sampled-data regulator with command generator tracking for use as a digital flight control system. The digital PIF autopilots are evaluated using closed-loop eigenvalues and linear simulations. The implementation of the PIF autopilots in a digital flight computer using a high order language (FORTRAN) is briefly described. The successful flight test results for each PIF autopilot mode is presented.

Broussard, J. R.↗
NASA NTRS2010

Environmental Stress Testing of the Single Sample Cylinder: A Proven Consensus Standard for Internal Gas Analysis (IGA) or Residual Gas Analysis (RGA)

In August 2008, Schuessler Consulting was contracted by NASA GSFC in support of the NASA Electronic Parts and Packaging (NEPP) program to perform two separate studies on moisture laden air in a stainless steel cylinder that had been designed to become a consensus standard for Test Method 1018. This Test Method was originally released for hybrids under Mil. Std. 883 but was quickly utilized on other microelectronic devices under the auspice of Mil. Std. 750. The cylinder had subsequently been fabricated for the 750 community. It was back-filled with moist air and subsequently analyzed over a period of time under a previous NASA contract. It had been shown that moisture in the 4000 - 5000 ppm range could be analyzed rather precisely with a mass spectrometer, commonly referred to as a Residual Gas Analyzer (RGA). The scope of this study was to ascertain if the composition and precision varied as a function of thermal shock at sub-zero temperatures and whether there was consensus when the standard was submitted to other RGA units. It was demonstrated and published that the consensus standard would yield precise RGA data for moisture within +/- 1% when optimized for a given RGA unit. It has been subsequently shown in this study at Oneida Research Services, that sub-zero storage did not affect that precision when a well-defined protocol for the analysis was followed. The consensus standard was taken to a second facility for analysis where it was found that moisture adsorption on the transfer lines caused precision to drop to +/- 12%. The Single Sample Cylinder (SSC) is a one liter stainless steel cylinder with associated sampling valves and has considerable weight and volume. But this considerable size allows for approximately 300 gas samples of the same composition to be delivered to any RGA unit. Lastly, a smaller cylinder, approximately 75 cc, of a second consensus standard was fabricated and tested with a different mix of fixed gases where moisture was kept in the 100 ppm range. This second standard has the potential of providing 30 gaseous samples and can be readily shipped to any analytical facility that desires to generate comparison RGA data. A series of comparison residual gas analyses was performed at the Honeywell Federal Manufacturing & Technologies facility in the National Nuclear Facility Administration s plant in Kansas City to complete this project. It was shown that improvements in the precision of a given RGA unit can be done by controlling the cycle time for each analysis and increasing analysis temperatures to minimize moisture adsorption. It was also found that a "one time event" in the subzero storage of the large SSC did not effect the units ability to continuously supply precise samples of the same chemistry, however the "event" caused a permanent +8% shift in the reported value of the moisture content. Lastly, a set of SSC RGA results was plotted on a common graph with DSCC "correlation study" RGA data. The result demonstrates the ability of the SSC to remove many of the individual variances that single, individual samples introduce. The consensus standards are now in storage at Oneida Research Services, one of the DSCC certified houses that does RGA to Military Standards, where they await future studies. The analytical data and the operational parameters of the instruments used are provided in the following discussion. Limitations and suggested means for improvement of both precision and accuracy are provided.

Schuessler, Philipp WH↗
NASA NTRS2000

Determining CDOM Absorption Spectra in Diverse Coastal Environments Using a Multiple Pathlength, Liquid Core Waveguide System. Measuring the Absorption of CDOM in the Field Using a Multiple Pathlength Liquid Waveguide System

We evaluated the accuracy, sensitivity and precision of a multiple pathlength, liquid core waveguide (MPLCW) system for measuring colored dissolved organic matter (CDOM) absorption in the UV-visible spectral range (370-700 nm). The MPLCW has four optical paths (2.0, 9.8, 49.3, and 204 cm) coupled to a single Teflon AF sample cell. Water samples were obtained from inland, coastal and ocean waters ranging in salinity from 0 to 36 PSU. Reference solutions for the MPLCW were made having a refractive index of the sample. CDOM absorption coefficients, a(sub CDOM), and the slope of the log-linearized absorption spectra, S, were compared with values obtained using a dual-beam spectrophotometer. Absorption of phenol red secondary standards measured by the MPLCW at 558 nm were highly correlated with spectrophotometer values (r > 0.99) and showed a linear response across all four pathlengths. Values of a(sub CDOM) measured using the MPLCW were virtually identical to spectrophotometer values over a wide range of concentrations. The dynamic range of a(sub CDOM) for MPLCW measurements was 0.002 - 231.5/m. At low CDOM concentrations (a(sub 370) < 0.1/m) spectrophotometric a(sub CDOM) were slightly greater than MPLCW values and showed larger fluctuations at longer wavelengths due to limitations in instrument precision. In contrast, MPLCW spectra followed an exponential to 600 nm for all samples. The maximum deviation in replicate MPLCW spectra was less than 0.001 absorbance units. The portability, sampling, and optical characteristics of a MPLCW system provide significant enhancements for routine CDOM absorption measurements in a broad range of natural waters.

Miller, Richard L.↗
NASA NTRSDate not supplied

Logical shadow tomography: Efficient estimation of error-mitigated observables

We introduce a technique to estimate error-mitigated expectation values on noisy quantum computers. Our technique performs shadow tomography on a logical state to produce a memory-efficient classical reconstruction of the noisy density matrix. Using efficient classical post-processing, one can mitigate errors by projecting into the codespace as in subspace expansion and taking powers of the density matrix as in virtual distillation. Relative to subspace expansion which requires Ω (2^((n-1)k) samples to estimate a Pauli observable with an [[n; k]] stabilizer code, our technique requires only Ө(2^k) samples. Relative to virtual distillation, our technique can compute powers of the density matrix without implementing additional copies of quantum states the quantum computer. We present numerical results using logical states encoded with up to sixty physical qubits and show fast convergence to error-free expectation values with only 10^5 samples under 1% depolarizing noise.

quantum computing↗
NASA NTRS2006

Gamma-Ray Burst Afterglows as Probes of Environment and Blastwave Physics: Absorption by Host Galaxy Gas and Dust - 1

We use a new approach to obtain limits on the absorbing columns towards an initial sample of 10 long Gamma-Ray Bursts observed with BeppoSAX and selected on the basis of their good optical and nIR coverage, from simultaneous fits to nIR, optical and X-ray afterglow data, in count space and including the effects of metallicity. In no cases is a MIV-like ext,inction preferred, when testing MW, LMC and SMC extinction laws. The 2175A bump would in principle be detectable in all these afterglows, but is not present in the data. An SMC-like gas-to-dust ratio or lower value can be ruled out for 4 of the hosts analysed here (assuming Sh4C metallicity and extinction law) whilst the remainder of the sample have too large an error to discriminate. We provide a more accurate estimate of the line-of-sight extinction and improve upon the uncertainties for the majority of the extinction measurements made in previous studies of this sample. We discuss this method to determine extinction values in comparison with the most commonly employed existing methods.

Starling, R. L. C.↗
NASA NTRS2002

Comparison of Aerosol Single Scattering Albedos Derived by Diverse Techniques In Two North Atlantic Experiments

Aerosol single scattering albedo omega (the ratio of scattering to extinction) is important in determining aerosol climatic effects, in explaining relationships between calculated and measured radiative fluxes, and in retrieving aerosol optical depths from satellite radiances. Recently, two experiments in the North Atlantic region, the Tropospheric Aerosol Radiative Forcing Observational Experiment (TARFOX) and the Second Aerosol Characterization Experiment (ACE-2), determined aerosol omega by a variety of techniques. The techniques included fitting of calculated to measured radiative fluxes; retrievals of omega from skylight radiances; best fits of complex refractive index to profiles of backscatter extinction, and size distribution; and in situ measurements of scattering and absorption at the surface and aloft. Both TARFOX and ACE-2 found a fairly wide range of values for omega at midvisable wavelengths approx. 550 nm, with omega(sub midvis) greater than or equal to 0.85 and less than or equal to 0.99 for the marine aerosol impacted by continental pollution. Frequency distributions of omega could usually be approximated by lognormals in omega(sub max) - omega, with some occurrence of bimodality, suggesting the influence of different aerosol sources or processing. In both TARFOX and ACE-2, closure tests between measured and calculated radiative fluxes yielded best-fit values of omega(sub midvis) 0.90 +/- 0.04 for the polluted boundary layer. Although these results have the virtue of describing the column aerosol unperturbed by sampling, they are subject to questions about representativeness and other uncertainties (e.g., thermal offsets, unknown gas absorption) The other techniques gave larger values for omega(sub midvis) for the polluted boundary layer, with a typical result of omega(sub midvis) = 0.95 +/- 0.04. Current uncertainties in omega are large in terms of climate effects More tests are needed of the consistency among different methods and of humidification effects on omega.

Russell, P. B.↗
NASA NTRS2003

Array biosensor for detection of toxins

The array biosensor is capable of detecting multiple targets rapidly and simultaneously on the surface of a single waveguide. Sandwich and competitive fluoroimmunoassays have been developed to detect high and low molecular weight toxins, respectively, in complex samples. Recognition molecules (usually antibodies) were first immobilized in specific locations on the waveguide and the resultant patterned array was used to interrogate up to 12 different samples for the presence of multiple different analytes. Upon binding of a fluorescent analyte or fluorescent immunocomplex, the pattern of fluorescent spots was detected using a CCD camera. Automated image analysis was used to determine a mean fluorescence value for each assay spot and to subtract the local background signal. The location of the spot and its mean fluorescence value were used to determine the toxin identity and concentration. Toxins were measured in clinical fluids, environmental samples and foods, with minimal sample preparation. Results are shown for rapid analyses of staphylococcal enterotoxin B, ricin, cholera toxin, botulinum toxoids, trinitrotoluene, and the mycotoxin fumonisin. Toxins were detected at levels as low as 0.5 ng mL(-1).

Review↗
NASA NTRS1991

On the utility of low resolution IUE spectroscopy of the 2800 A Mg II lines as a stellar chromosphere indicator

Low resolution IUE spectroscopy of the 2800-A Mg II h and k lines is shown to provide a useful means for documenting chromospheric activity among relatively young dwarf stars. An index I(Mg II) has been defined which measures the integrated flux in the region 2784-2814 A relative to the flux interpolated from nearby comparison regions. Values of this index have been derived from low resolution IUE spectra for a sample of field dwarfs for which Ca II H and K line indices have been published as part of the Mount Wilson HK program. The large range in chromospheric activity among field dwarfs that is exhibited by the Mount Wilson Ca II S index is found to also be reflected by the lower resolution I(Mg II) index. Using an age calibration of Ca II emission line strengths derived by Barry, it is found that the value of I(Mg II) can be used to distinguish between dwarfs younger and older than 3 Gyr. The low resolution nature of the I(Mg II) index means that it holds potential for use as an age diagnostic for stellar population studies. Among dwarfs of age greater than 3 Gyr there is some evidence that this Mg II index is affected by line blanketing.

Smith, Graeme H.↗
NASA NTRS1974

An interdisciplinary study of the estaurine and coastal oceanography of Block Island Sound and adjacent New York coastal waters

ERTS-1 photographic data products have been analyzed using additive color viewing and electronic image analysis techniques. Satellite data were compared to water sample data collected simultaneously with the data of ERTS-1 coverage in New York Bight. Prediction of the absolute value of total suspended particles can be made using composites of positives of MSS bands 5 and 6 which have been precisely made using the step wedge supplied on the imagery. Predictions of the relative value of the extinction coefficient can be made using bands 4 and 5. Thematic charts of total suspended particles (particles per litre) and extinction coefficient provide scientists conducting state and federal water sampling programs in New York Bight with data which improves the performance of these programs.

Yost, E.↗
NASA NTRS1972

Two-dimensional finite-element temperature variance analysis

The finite element method is extended to thermal analysis by forming a variance analysis of temperature results so that the sensitivity of predicted temperatures to uncertainties in input variables is determined. The temperature fields within a finite number of elements are described in terms of the temperatures of vertices and the variational principle is used to minimize the integral equation describing thermal potential energy. A computer calculation yields the desired solution matrix of predicted temperatures and provides information about initial thermal parameters and their associated errors. Sample calculations show that all predicted temperatures are most effected by temperature values along fixed boundaries; more accurate specifications of these temperatures reduce errors in thermal calculations.

Heuser, J. S.↗
NASA NTRS1971

Elevation-relief ratio, hypsometric integral, and geomorphic area-altitude analysis.

Mathematical proof establishes identity of hypsometric integral and elevation-relief ratio, two quantitative topographic descriptors developed independently of one another for entirely different purposes. Operationally, values of both measures are in excellent agreement for arbitrarily bounded topographic samples, as well as for low-order fluvial watersheds. By using a point-sampling technique rather than planimetry, elevation-relief ratio (defined as mean elevation minus minimum elevation divided by relief) is calculated manually in about a third of the time required for the hypsometric integral.

Pike, R. J.↗
NASA NTRS1974

Liquid rocket combustion computer model with distributed energy release. DER computer program documentation and user's guide, volume 1

A computer program for analyzing rocket engine performance was developed. The program is concerned with the formation, distribution, flow, and combustion of liquid sprays and combustion product gases in conventional rocket combustion chambers. The capabilities of the program to determine the combustion characteristics of the rocket engine are described. Sample data code sheets show the correct sequence and formats for variable values and include notes concerning options to bypass the input of certain data. A seperate list defines the variables and indicates their required dimensions.

Combs, L. P.↗
NASA NTRS1976

The measurement of carbon monoxide and methane in the national capital air quality control region. III - Correlation interferometer results

Two types of experiments were performed with a correlation interferometer on-board a Bell Jet Ranger 206 Helicopter. The first consisted of simultaneous ground- and air-truth measurements as the instrumented helicopter passed over the Cheverly site. The second consisted of several measurement flights in and around the national capital air quality control region (Washington, D.C.). The correlation interferometer data, the infrared Fourier spectrometer data, and the integrated altitude sampling data showed agreement within the errors of the individual measurements. High values for CO were found from the D.C. flight data to be reproducible and concentrated in areas of stop-and-go traffic. It is concluded, that pollutants at low altitudes are detectable from an air-borne platform by remote correlation interferometry and that the correlation interferometer measurements agree with ground- and air-truth data.

Goldstein, H. W.↗
NASA NTRS1977

Distribution and concentration of suspended matter in Delaware Bay

The author has identified the following significant results. The problem of remote sensing of suspended matter in water was analyzed in terms of the single-scattering albedo, and a semiempirical relationship between satellite radiance measurements and the concentration of suspended matter in the water was developed. The relationship was tested using data from the 7 July 1973 LANDSAT overpass of Delaware Bay with good results. Suspended sediment concentration maps for the entire Delaware Bay were prepared using radiance values extracted from LANDSAT MSS imagery and correlating them with ground truth samples collected from boats and helicopter.

Klemas, V.↗