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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 793 records · Page 44
All sourcesNASA NTRSDOE OSTI
DOE OSTI2018

Facile Synthesis of Spinel Ferrites with Enhanced Magnetic Properties from Two Intractable Metallurgical Resources: Zinc-Bearing Dust and Nickel Laterite Ore

Nickel laterite ore and zinc-bearing dust are multi-metal-associated and intractable resources. Comprehensive and cooperative utilization of zinc-bearing dust and nickel laterite ore for the preparation of spinel ferrites with enhanced magnetic properties by a facile process was proposed. The structure and magnetic properties of as-prepared spinel ferrites were characterized by X-ray diffraction (XRD), Raman spectroscopy, and Physical Property Measurement System (PPMS). The effect of mass ratios of zinc-bearing dust to nickel laterite ore, calcination temperature, and Zn substitution content on the as-prepared samples was investigated in detail. A single phase of Zn-substituted spinel ferrites (x= 0.00, 0.10, 0.20, and 0.30) could be obtained when the mass ratios were controlled at 1:0.4, 1:4:1.8, 1:2:1.5, and 1:1:1.2 after being calcined at 900 {sup ∘}C for 30 min, respectively. The magnetic property tests present that the as-prepared spinel ferrite exhibits enhanced magnetic properties with the saturation magnetization (Ms) value of 66.8 emu g{sup − 1} and the coercivity (Hc) value of 26 Oe when the mass ratio was controlled at 1:1:1.2. This research could provide an effective way to transfer two intractable resources into soft magnetic materials.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1990

Nonintrusive method and apparatus for monitoring the cure of polymeric materials

The invention is a nonintrusive method of monitoring the cure of a polymeric material using an electromagnetic field to sense a change of resistance of the polymeric material in the electromagnetic field that occurs during curing. This change of resistance is used to vary the impedance of an alternating voltage power supply that produces the electromagnetic field and which change of impedance is measured periodically or continuously to monitor the cure of said polymeric material. The apparatus for practicing the method of this invention may include a nonintrusive sensing head providing an inner, electromagnetic core within an open ended outer pot formed of magnet material. The open end of the pot core is positioned from a selected area of the surface of a sheet of the polymeric material. An alternating voltage supply circuit includes an inductance coil around the electromagnetic core and capacitor connected in parallel with the inductance coil forms a resonant tank circuit when energized. The resulting change in resistance of the polymeric material opposite the open end, a function of the curing, is measured as a corresponding change in the impedance of the power supply circuit to thereby monitor the cure of the polymeric material in the selected area.

Johnston, David F.↗
NASA NTRS1991

Actively controlled superconducting bearings

Actively controlled conventional radial beating using copper winding and soft magnetic material can provide only up to 200 N/sq cm of pressure. Large cryogenic pumps for space applications operating at 30,000 rpm and high rpm machines may require larger magnetic pressure. We show that using superconducting winding in the rotor and the stator of a magnetic bearing system increases the pressure by an order of magnitude. The paper addresses winding configuration, stability, ac losses, and power requirement for the superconducting winding.

Eyssa, Yehia M.↗
NASA NTRS1996

Design and Performance Improvements of the Prototype Open Core Flywheel Energy Storage System

A prototype magnetically suspended composite flywheel energy storage (FES) system is operating at the University of Maryland. This system, designed for spacecraft applications, incorporates recent advances in the technologies of composite materials, magnetic suspension, and permanent magnet brushless motor/generator. The current system is referred to as an Open Core Composite Flywheel (OCCF) energy storage system. This paper will present design improvements for enhanced and robust performance. Initially, when the OCCF prototype was spun above its first critical frequency of 4,500 RPM, the rotor movement would exceed the space available in the magnetic suspension gap and touchdown on the backup mechanical bearings would occur. On some occasions it was observed that, after touchdown, the rotor was unable to re-suspend as the speed decreased. Additionally, it was observed that the rotor would exhibit unstable oscillations when the control system was initially turned on. Our analysis suggested that the following problems existed: (1) The linear operating range of the magnetic bearings was limited due to electrical and magnetic saturation; (2) The inductance of the magnetic bearings was affecting the transient response of the system; (3) The flywheel was confined to a small movement because mechanical components could not be held to a tight tolerance; and (4) The location of the touchdown bearing magnifies the motion at the pole faces of the magnetic bearings when the linear range is crucial. In order to correct these problems an improved design of the flywheel energy storage system was undertaken. The magnetic bearings were re-designed to achieve a large linear operating range and to withstand load disturbances of at least 1 g. The external position transducers were replaced by a unique design which were resistant to magnetic field noise and allowed cancellation of the radial growth of the flywheel at high speeds. A central rod was utilized to ensure the concentricity of the magnetic bearings, the motor/generator, and the mechanical touchdown bearings. In addition, the mechanical touchdown bearings were placed at two ends of the magnetic bearing stack to restrict the motion at pole faces. A composite flywheel was made using a multi-ring interference assembled design for a high specific energy density. To achieve a higher speed and better efficiency, a permanent magnet DC brushless motor was specially designed and fabricated. A vacuum enclosure was constructed to eliminate windage losses for testing at high speeds. With the new improvements the OCCF system was tested to 20,000 RPM with a total stored energy of 15.9 WH and an angular momentum of 54.8 N-m-s (40.4 lb-ft-s). Motor current limitation, caused by power loss in the magnetic bearings, was identified as causing the limit in upper operating speed.

Pang, D.↗
DOE OSTI2022

Adrian Portales Coop Internship Report

Using the thesis of W.R. Nolan (cite) as a guide, Cobalt Iron (CoFe) powders were reacted with 0.1 wt.% and 0.2 wt.% phosphoric acid in a 20:1 ratio of acetone to phosphoric acid. The powders were then dried at room temperature. The resulting phosphate coated CoFe was then mixed with 0.75 wt.% of the lubricant N,N' ethylene bis-stearamide (trade name: Acrawax C) and hot pressed to form a consolidated soft magnetic material referred to as CoFeP. With an avenue of synthesis for CoFeP determined, a proper amount of stock was synthesized for continuous “brick” production. While under current optimization, these 1x1 mm magnetic bricks will ultimately be placed and secured along the inside wall of each MK Magnetics transformer core by an appropriate CoFeP dispersed epoxy. As of now each brick has been produced though a pressing and annealing process via square 2x2 cm die. Before a brick is made a pressure calculation is run to ensure the dies maximum operating pressure is not exceeded. Figure 1. ensures the user’s safety by showing that the tons-on-ram required for a 2x2 cm square die to reach 760 MPa is below the point of die failure.

36 MATERIALS SCIENCE↗
NASA NTRS1983

Application of advanced materials to rotating machines

In discussing the application of advanced materials to rotating machinery, the following topics are covered: the torque speed characteristics of ac and dc machines, motor and transformer losses, the factors affecting core loss in motors, advanced magnetic materials and conductors, and design tradeoffs for samarium cobalt motors.

Triner, J. E.↗
NASA NTRS1994

Core Losses In Three Alloys

Report describes experimental investigation of core losses and dynamic magnetic flux densities as functions of magnetomotive force of three soft magnetic materials under sine-wave voltage excitation at frequencies from 1 to 50 kHz and at temperatures from 23 to 300 degrees C. Prompted by need for data to design magnetic cores for efficient, lightweight power supplies operating in harsh environments.

Schwarze, G. E.↗
NASA NTRS2008

Elastic Distribution of Microshutters, Measurements Obtainable on James Web Space Telescope

Spectrographic astronomy measurements in the near-infrared region will be done by functional two-dimensional microshutter arrays that are being fabricated at the NASA Goddard Space Flight Center for the James Webb Space Telescope (JWST). These micro-shutter arrays will represent the first mission-critical MEMS devices to be flown in space. JWST will use microshutter arrays to select focal plane object. 2-D programmable aperture masks of more than 200,000 elements select such space object. The use of silicon wafer material promises high efficiency and high contrast. Microshutter operation temperature is around 35K. Microshutter arrays are fabricated as close-packed silicon nitride membranes with a unit cell size of 105 x 204 micrometers. A layer of magnetic material is deposited onto each shutter. Individual shutters are equipped with a torsion flexure. Reactive ion etching (RIE) releases the shutters so they can open up to 90 degrees using the torsion flexure. Shutter rotation is initiated into a silicon support structure via an external magnetic field. Two electrically independent aluminum electrodes are deposited, one onto each shutter and another onto the support structure side-wall, permitting electrostatic latching and 2-D addressing to hold specific shutters open via external electronics.

Kletetschka, Gunther↗
NASA NTRS2020

Core Losses in Co-Rich Inductors with Tunable Permeability

High frequency, low loss power systems enable electrified aircraft propulsion. Filter inductors that reduce noise in high current systems can account for 50% of the motor drive mass. Efficient inductor cores with tunable permeability reduce system mass by producing less heat, that removes heat sink mass. Requirements for filter inductors vary based on the chosen topology, but all inductor cores must operate below saturation levels. As the saturation flux density is limited (less than ~2 T), high differential current applications require cores with low relative permeabilities. The large induced anisotropies possible in Co-rich metal amorphous nanocomposite materials enables gapless inductors with relative permeabilities down to ~20. These materials have fine grain size ~8nm with a faulted, close packed structure. The impact of different processing methods on core losses are presented along with comparison to other low permeability soft magnetic materials.

Leary, Alex↗
NASA NTRS1973

Remanent magnetization and structural effects due to shock in natural and man-made iron-nickel alloys

Explosive shock or meteorite impact are significant remagnetization processes. The mechanisms of remagnetization associated with the dynamic processes depend on the peak shock pressure, the nature of the shocked materials, and the behavior of the shock in the material. Magnetic measurements can be used to classify products formed during a shock process, and magnetic measurements can be used to investigate the process itself because of the special characteristics of the remanent magnetization vectors. The magnetic coercive force increases more rapidly in quenched and annealed iron-nickel alloys as nickel is added than it does in the alloys which have been shocked.

Wasilewski, P. J.↗
DOE OSTI2020

Insensitivity of Magnetic Coupling to Ligand Substitution in a Series of Tetraoxolene Radical-Bridged Fe 2 Complexes

The elucidation of magnetostructural correlations between bridging ligand substitution and strength of magnetic coupling is essential to the development of high-temperature molecule-based magnetic materials. Toward this end, we report the series of tetraoxolene-bridged Fe II 2 complexes [(Me 3 TPyA) 2 Fe 2 ( R L)] n + (Me 3 TPyA = tris(6-methyl-2-pyridylmethyl)amine; n = 2: OMe LH 2 = 3,6-dimethoxy-2,5-dihydroxo-1,4-benzoquinone, Cl LH 2 = 3,6-dichloro-2,5-dihydroxo-1,4-benzoquinone, Na 2 [ NO 2 L] = sodium 3,6-dinitro-2,5-dihydroxo-1,4-benzoquinone; n = 4: SMe 2 L = 3,6-bis(dimethylsulfonium)-2,5-dihydroxo-1,4-benzoquinone diylide) and their one-electron-reduced analogues. Furthermore, variable-temperature dc magnetic susceptibility data reveal the presence of weak ferromagnetic superexchange between Fe II centers in the oxidized species, with exchange constants of J = +1.2(2) (R = OMe, Cl) and +0.3(1) (R = NO 2 , SMe 2 ) cm –1 . In contrast, X-ray diffraction, cyclic voltammetry, and Mössbauer spectroscopy establish a ligand-centered radical in the reduced complexes. Magnetic measurements for the radical-bridged species reveal the presence of strong antiferromagnetic metal–radical coupling, with J = -57(10), -60(7), -58(6), and -65(8) cm –1 for R = OMe, Cl, NO 2 , and SMe 2 , respectively. The minimal effects of substituents in the 3- and 6-positions of R L x –• on the magnetic coupling strength is understood through electronic structure calculations, which show negligible spin density on the substituents and associated C atoms of the ring. Finally, the radical-bridged complexes are single-molecule magnets, with relaxation barriers of U eff = 50(1), 41(1), 38(1), and 33(1) cm –1 for R = OMe, Cl, NO 2 , and SMe 2 , respectively. Taken together, these results provide the first examination of how bridging ligand substitution influences magnetic coupling in semiquinoid-bridged compounds, and they establish design criteria for the synthesis of semiquinoid-based molecules and materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2015

New Photocathode materials for electron-ion-colliders

Our aim has been to explore new photocathode materials and schemes to develop strategies and technologies for next generation nuclear physics accelerator capabilities, particularly for Electron Ion Colliders (EIC). Thus, we investigated thin film deposition and ensuing properties for several adequate magnetic materials applicable to spin-polarized photocathodes. We also implemented a full experimental setup for light incidence at an acute angle onto the photocathode surface in order to excite surface Plasmon resonance hence increasing light absorption by a metallic surface. We successfully tested the setup with a thermionic cathode as well as Plasmonic silver-MgO samples and obtained very encouraging results. Our first results are very encouraging since the photocurrent measured on this preliminary plasmonic Ag-MgO sample under low power (~ 1mW) cw red light from a HeNe laser was 256 pA, thus two orders magnitude larger than that reported by others following also plasmonic approaches. We extended our studies to shorter wavelengths and we also started preliminary work on chemically ordered MnAl thin films –a component of the tertiary Ag-Mn-Al (silmanal) alloy in order to develop spin-polarized photocathodes capable of sustaining surface Plasmon resonance. It is worthwhile mentioning that a graduate student has been directly involved during this project ensuring the training of next generation of scientists in this area of research.

43 PARTICLE ACCELERATORS↗
NASA NTRS1985

Numerical methods for analyzing electromagnetic scattering

Numerical methods to analyze electromagnetic scattering are presented. The dispersions and attenuations of the normal modes in a circular waveguide coated with lossy material were completely analyzed. The radar cross section (RCS) from a circular waveguide coated with lossy material was calculated. The following is observed: (1) the interior irradiation contributes to the RCS much more than does the rim diffraction; (2) at low frequency, the RCS from the circular waveguide terminated by a perfect electric conductor (PEC) can be reduced more than 13 dB down with a coating thickness less than 1% of the radius using the best lossy material available in a 6 radius-long cylinder; (3) at high frequency, a modal separation between the highly attenuated and the lowly attenuated modes is evident if the coating material is too lossy, however, a large RCS reduction can be achieved for a small incident angle with a thin layer of coating. It is found that the waveguide coated with a lossy magnetic material can be used as a substitute for a corrugated waveguide to produce a circularly polarized radiation yield.

Lee, S. W.↗
DOE OSTI2015

Ion energy-angle distribution functions at the plasma-material interface in oblique magnetic fields

The ion energy-angle distribution (IEAD) at the wall of a magnetized plasma is of fundamental importance for the determination of the material processes occurring at the plasma-material interface, comprising secondary emissions and material sputtering. Here, we present a numerical characterization of the IEAD at the wall of a weakly collisional magnetized plasma with the magnetic field inclined at an arbitrary angle with respect to the wall. The analysis has been done using two different techniques: (1) a fluid-Monte Carlo method, and (2) particle-in-cell simulations, the former offering a fast but approximate method for the determination of the IEADs, the latter giving a computationally intensive but self-consistent treatment of the plasma behavior from the quasi-neutral region to the material boundary. The two models predict similar IEADs, whose similarities and differences are discussed. Data are presented for magnetic fields inclined at angles from normal to grazing incidence (0°–85°). We show the scaling factors of the average and peak ion energy and trends of the pitch angle at the wall as a function of the magnetic angle, for use in the correlation of fluid plasma models to material models.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2025

Spin excitations and dynamics in 2D magnets: An overview of magnons and magnetic skyrmions

van der Waals magnetic materials open up exciting possibilities to investigate fundamental spin properties in low-dimensional systems and to build compact functional spintronic structures. This review focuses on the recent progress in two-dimensional (2D) magnets that explore beyond the homogenous magnetically ordered state, including magnons (spin waves), magnetic skyrmions, and complex magnetic domains. Properties of these spin and topology excitations in 2D magnets provide insights into spin-orbit interactions and other forms of coupling between electrons, phonons, and spin-dependent excitations. Such spin-based quasiparticles can also serve as information carriers for next-generation high-speed computing elements. Furthermore, we will first lay out the general theoretical basis of dynamical responses in magnetic systems, followed by detailed descriptions of experimental progress in magnons and spin textures (including magnetic domains and skyrmions). Discussion on the experimental techniques and future perspectives are also included.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2021

Giant magnetostriction and nonsaturating electric polarization up to 60 T in the polar magnet $\mathrm{CaBaCo_4O_7}$

Giant magnetostriction in insulating magnetic materials is highly required for applications but is rarely observed. Here we show that giant magnetostriction (> 1500 ppm) can be achieved in an insulating transition metal oxide CaBaCo 4 O 7 where the ferrimagnetic ordering at T c ~ 62K is associated with a huge change in the lattice. Moreover, because this material is pyroelectric with a nonswitchable electric polarization (P), the giant magnetostriction results in a pronounced magnetoelectric effect—a huge change of electric polarization (ΔP ~ 1.6μC/cm 2 ) in response to the applied magnetic field up to 60 T. Geometric frustration as well as the orbital instability of Co 2+ /Co 3+ ions is believed to play a crucial role in the giant magnetostriction. Here our study provides insights on how to achieve both giant magnetostriction and pronounced magnetoelectric effect in insulating transition metal oxides.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2024

Designed Spin‐Texture‐Lattice to Control Anisotropic Magnon Transport in Antiferromagnets

Abstract Spin waves in magnetic materials are promising information carriers for future computing technologies due to their ultra‐low energy dissipation and long coherence length. Antiferromagnets are strong candidate materials due, in part, to their stability to external fields and larger group velocities. Multiferroic antiferromagnets, such as BiFeO 3 (BFO), have an additional degree of freedom stemming from magnetoelectric coupling, allowing for control of the magnetic structure, and thus spin waves, with the electric field. Unfortunately, spin‐wave propagation in BFO is not well understood due to the complexity of the magnetic structure. In this work, long‐range spin transport is explored within an epitaxially engineered, electrically tunable, 1D magnonic crystal. A striking anisotropy is discovered in the spin transport parallel and perpendicular to the 1D crystal axis. Multiscale theory and simulation suggest that this preferential magnon conduction emerges from a combination of a population imbalance in its dispersion, as well as anisotropic structural scattering. This work provides a pathway to electrically reconfigurable magnonic crystals in antiferromagnets.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Correlated states in β-Li 2 IrO 3 driven by applied magnetic fields

Magnetic honeycomb iridates are thought to show strongly spin-anisotropic exchange interactions which, when highly frustrated, lead to an exotic state of matter known as the Kitaev quantum spin liquid. However, in all known examples these materials magnetically order at finite temperatures, the scale of which may imply weak frustration. Here we show that the application of a relatively small magnetic field drives the three-dimensional magnet β-Li 2 IrO 3 from its incommensurate ground state into a quantum correlated paramagnet. Interestingly, this paramagnetic state admixes a zig-zag spin mode analogous to the zig-zag order seen in other Mott-Kitaev compounds. The rapid onset of the field-induced correlated state implies the exchange interactions are delicately balanced, leading to strong frustration and a near degeneracy of different ground states.

36 MATERIALS SCIENCE↗