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At least 793 records · Page 44
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Gramicidin and chlorhexidine encapsulated in bicontinuous microemulsions: Antimicrobial activity performance and their impact on self‐assembly

The utility of bicontinuous microemulsions (BMEs) as carriers of the antimicrobial peptide (AMP) gramicidin D and antiseptic chlorhexidine was investigated for possible topical delivery to chronic wounds. The two water-insoluble solutes dissolved in pre-formed one-phase BMEs of Water/Polysorbate 80/Limonene/Ethanol/Glycerol and Water/Aerosol-OT (AOT)/Polysorbate 85/Isopropyl Myristate and an AOT/Polysorbate 85 Winsor-III system, achieving gramicidin and chlorhexidine concentrations of 1.0 wt% and 0.5% individually and 0.5% and 0.3% in mixtures at 22°C, respectively. Small-angle neutron scattering measurements demonstrated that both solutes decreased surfactant interfacial activity and increased interfacial fluidity for the Polysorbate 80 system. For the AOT/Polysorbate 85 systems, ellipsoidal aggregates consisting of gramicidin and likely adsorbed surfactant and oil formed, while chlorhexidine enhanced the surface activity of surfactants. According to bioassays performed on artificial skin, the incorporation of melittin, gramicidin, and chlorhexidine in general enhanced the bioactivity of Polysorbate 80 BMEs for 24 h treatment against relevant antibiotic-resistant bacteria found on skin relative to controls. Yet, BME treatments were less effective than aqueous melittin control, in contrast to well diffusion bioassays performed previously. The results reflect the strong impact of AMPs and antiseptics on BME structure and dynamics and the complexity of formulating BMEs for optimal antimicrobial activity.

antimicrobial peptides↗
NASA NTRS1985

Impact melting of the Cachari eucrite 3.0 Gy ago

The chemical compositions and Ar-isotope gas-retention ages of host phase and glass veins in the Cachari eucrite are determined by microprobe and neutron-activation analysis and mass spectrometry, respectively. The results are presented in tables, graphs, and back-scattered electron images and characterized in detail. The compositions are found to support the thesis that the glass formed by shock melting of the host rock (or of rock having the same composition). The Ar-39/Ar-40 ages of host and glass are given as 3.04 + or - 0.07 Gyr and 3.47 + or - 0.04 Gyr, respectively; the former value is taken as the true data of melting, and the latter is attributed to incomplete postmelt degassing of Ar from the glass phase. The implications of the relative youth of this and other eucrites and howardites for the regolith history of the parent body are considered.

Bogard, D. D.↗
DOE OSTI2025

Bayesian inference of nuclear-matter density from proton scattering

Background: Proton elastic scattering at intermediate energy is widely employed as a tool for determining the matter radius of atomic nuclei. Here, the sensitivity of the approach relies on high-resolution measurements at small scattering angles and low-momentum transfer. Under these conditions, the Glauber multiple scattering theory accurately describes the proton-nucleus elastic cross section. Purpose: Investigate the sensitivity of the Glauber multiple scattering theory to uncertainties associated with input parameters such as the nuclear-matter density distribution and nucleon-nucleon data. Method: A joint Bayesian inference was performed using 12 angular distributions of elastic scattering at different energies on 58 Ni, 90 Zr, and 208 Pb targets. A Metropolis-Hastings algorithm was implemented to make an uncertainty quantification analysis for the input parameters used in the Glauber multiple scattering theory. Results: The experimental cross sections were fitted simultaneously using a joint Bayesian inference approach. Posterior probability density distributions of 42 input parameters were obtained from the analysis. A moderate correlation between the nuclear density parameters and the nucleon-nucleon cross sections was found. This correlation impacts the extraction of the nuclear-matter radius. Conclusions: The present analysis provided a consistent method for extracting the nuclear-matter density distribution of 58 Ni, 90 Zr, and 208 Pb from data across different incident energies. Due to the correlation of the nucleon-nucleon cross sections with the other input parameters, a constrained Bayesian inference using free nucleon-nucleon cross section data was performed. The nuclear-matter radii obtained from the analysis are in good agreement with multiple results reported in the literature.

190 ≤ A ≤ 219↗
NASA NTRSDate not supplied

Urban Air Mobility Noise: Current Practice, Gaps, and Recommendations

AN Air Mobility (UAM) is an opportunity for aviation to improve transportation systems across the world. Representative UAM vehicle attributes include electrical vertical takeoff and landing (eVTOL) vehicles that can accommodate up to 6 passengers (or equivalent cargo), are possibly autonomous, perform missions of up to 100 nautical miles at altitudes up to 3000 ft. above ground level, have flight speeds up to 200 knots, and weigh between 800 and 8000 pounds. Along with the many anticipated benefits, there will be noise issues that need to be addressed. In 2018, NASA formed an Urban Air Mobility Noise Working Group (UNWG) to assemble noise experts from industry, universities and government agencies to identify, discuss, and address UAM noise issues. This oral presentation summarizes technology gaps and goals associated with four areas of interest: Tools & Technologies, Ground & Flight Testing, Human Response & Metrics, and Regulation & Policy, and is drawn from a draft white paper [1] by the same title. Tools & Technologies include noise prediction tools and noise reduction technologies that have been developed for conventional rotorcraft and fixed-wing vehicles that may be applicable or need to be modified for UAM. Prediction tools need to be able to account for variable speed rotors and other temporal variation effects that impact community noise. A reprioritization of noise sources needs to be done since UAM vehicles include multiple rotors/propellers, often in proximity to one another and/or the airframe, with dynamic transition, and new noise sources such as electric motors or hybrid-electric propulsion. Scattering and propagation methods need to be developed that include the vehicle components and surfaces near a receiver such as buildings and vertiports. Validation databases are needed to quantify prediction uncertainties. Prediction tools used to evaluate community noise will need source models appropriate for a wide range of UAM vehicles. Existing noise reduction technologies need to be evaluated and new noise reduction technologies should be developed in anticipation of future noise requirements. Although the prediction and treatment of interior cabin noise is a secondary goal, it is recognized that new tools and methods may be needed due to the uniqueness of the vehicle design and the presence of both acoustic and structure-borne loads. Ground & Flight Testing has been a critical part of validating noise reduction technologies and verifying that an air vehicle is ready for certification. UAM vehicles introduce new challenges for test procedures such as different source noise directivity, unsteady sources due to maneuvers, and a variety of takeoff and approach trajectories. The operating environment will be more complex than current aircraft with the introduction of vertiports in populated areas with “urban canyons” making reflections an important part of noise prediction and annoyance. It is expected that new test procedures and measurement methods will be necessary. Consideration will need to be given for both piloted and autonomous operations. Human Response & Metrics may be very different for UAM noise compared to current experience with airport noise. Current metrics used to certify rotorcraft and fixed-wing aircraft may not be as useful for evaluating UAM noise. Operations at lower altitudes may influence annoyance. Psychoacoustic and community testing will be needed to quantify annoyance and assess appropriate metrics. In addition to conventional noise level metrics, considerations such as audibility and temporal variation of the sound may be required. Differences between indoor or outdoor exposure will have an impact with dependence on urban and residential flight paths. Aircraft noise is currently regulated at a national level and typically involves partnerships with the industry to establish regulations. Regulators realize that current policies and procedures may not be appropriate for some of the emerging air vehicles and new procedures may be needed to address UAM noise. Development of new policies and procedures are needed so that local communities do not hastily attempt to establish their own restrictions that will both limit growth of the market and create an inconsistent and confusing regulatory environment. To expedite this development, it is crucial early measurement data are shared through partnership arrangements to support both noise certification and noise modeling/noise assessment. At the same time, an effective engagement strategy should be developed to address local community noise issues associated with UAM vehicles and flight operations as they arise.

urban air mobility↗
DOE OSTI2022

Failure Mode Identification of Insulin Drug Products – Impact of Relevant Stress Conditions on the Quality of the Drug

Fast-acting insulin drug products (DPs) are carried and administered by diabetic patients to maintain their blood glucose level throughout the day, exposing the DPs to stress conditions. Apidra, Novolog, and Humalog insulin DPs were tested under various stress conditions. Dynamic light scattering (DLS), and size exclusion chromatography (SEC) were used to monitor the stability and aggregation. Thermal stress alone did not influence the stability. However, 24 hr exposure to vigorous mechanical stress shifted the DLS size peaks of Novolog and Humalog from 5 ± 1 nm to > 50.9 ± 25.6 nm, and the SEC native protein peak areas decreased 52% for Novolog and 18.4% for Humalog. Combined stress accelerated protein aggregation more drastically. Novolog and Humalog size shifted (>75 nm) after 3 hr and the peak area decreased > 97.9% after 6 hr exposure, indicating that high temperature accelerated the aggregation triggered by agitation. Soluble aggregates were captured by DLS early on compared to SEC. Apidra was comparably stable indicating DP formulation plays a critical role in stability. Here this study provides a greater understanding of potential failure modes patients and care givers may encounter while handling insulin DPs.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Engineering phonon transport through cation disorder in dimensionally constricted high entropy MXene

Designing materials with low thermal conductivity is a crucial objective for applications in thermal insulation and thermoelectrics. Traditional methods such as doping, mechanical strain and introducing defects in perfect crystals have been widely explored to impede the flow of heat. Here, this work introduces dimensional constriction and cationic disorder as novel avenues to manipulate lattice thermal conductivity (LTC). High entropy materials characterized by random distribution of multiple elements, creates a suitable environment for thermal insulation due to its configurational disorder and local lattice distortions. On the other hand, MXenes, derived from MAX-phase, have garnered considerable attention due to their unique structural attributes, leading to potential applications in catalysis and energy storage. Ti 2 AlC MAX-phase is examined to understand the impact of dimensional constriction on phonon transport of Ti 2 C with cationic disorder, i.e., (Ti 0.25 Nb 0.25 Cr 0.25 Ta 0.25 ) 2 C. The exponential reduction in LTC of HE-MXene is attributed to disorder scattering that significantly limits phonon mean free path (MFP) and relaxation time. The spread of mode-resolved LTC with MFP highlights the influence of disorder on phonon scattering. This work provides a systematic approach to engineer LTC through dimensional constriction and cationic disorder, laying the foundation for tailored materials with desired thermal properties.

2D materials↗
DOE OSTI2023

Dynamics of collision-induced energy transfer

Collisions are of fundamental importance in many relevant physico-chemical phenomena in the gas phase and at the gas-surface interface. Collision-induced energy transfer not only offers a sensitive probe of interatomic interactions, but also impacts an array of processes ranging from transport to reactivity. This perspective highlights some recent advances on collision-induced energy transfer dynamics. In the gas phase, cold collisions revealed remarkable quantum effects and stereodynamics of bimolecular inelastic scattering, which motivated development of new state-to-state quantum scattering methods. For surface processes, experiments of hydrogen atom scattering from various surfaces combined with first-principles molecular dynamics simulations shed valuable light on the relative importance of adiabatic energy transfer to surface phonons and nonadiabatic energy transfer to surface electrons. We outline further challenges in these fields and expect more fruitful interplay between experiment and theory.

Cold collision↗
DOE OSTI2026

Exploring the impact of nucleotide length on lipid nanoparticle structure and properties

Lipid nanoparticles (LNPs) are versatile carriers for nucleic acid (NA) therapeutics, including ASOs, siRNA, mRNA, and poly-IC. While lipid composition is known to influence LNP properties, the impact of NA length on morphology and internal structure is less understood, particularly during the stages of carrier–cargo assembly. Here, we examine NA length and lipid composition immediately after mixing using high-throughput SAXS, dynamic light scattering, and cryogenic electron microscopy. All LNPs form ordered NA/lipid compartments, with longer NAs promoting inverse hexagonal (H II ) phases and larger intercompartment distances. In contrast, short NAs, especially in formulations with SM102 ionizable lipid, favor lamellar phases. SAXS peak deconvolution quantifies ordered versus disordered phases via a Robustness of Ordered Phase factor, which correlates with particle size and encapsulation efficiency. Formulations with MC3 ionizable and DOPE helper lipids exhibit the most stable H II -phase packing, highlighting the role of helper-lipid curvature in compartment stabilization. Variations in NA compartmentalization indicate differences in payload capacity, offering a framework for rational LNP design across diverse nucleic acid cargos.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2022

Measurement of scintillation response of CsI[Na] to low-energy nuclear recoils by COHERENT

Here, we present results of several measurements of CsI[Na] scintillation response to 3–60 keV energy nuclear recoils performed by the COHERENT collaboration using tagged neutron elastic scattering experiments and an endpoint technique. Earlier results, used to estimate the coherent elastic neutrino-nucleus scattering (CEvNS) event rate for the first observation of this process achieved by COHERENT at the Spallation Neutron Source (SNS), have been reassessed. We discuss corrections for the identified systematic effects and update the respective uncertainty values. The impact of updated results on future precision tests of CEvNS is estimated. We scrutinize potential systematic effects that could affect each measurement. In particular we confirm the response of the H11934-200 Hamamatsu photomultiplier tube (PMT) used for the measurements presented in this study to be linear in the relevant signal scale region.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
NASA NTRS1977

Electron-impact excitation of the low-lying electronic states of HCN

The first study of the low-energy electron-impact excitation of low-lying electronic transitions in the HCN molecule is reported. Measurements were made at incident electron energies of 11.6 and 21.6 eV in the energy-loss range of 3-10 eV, and at scattering angles of 20-130 deg. Inelastic scattering spectra were placed on the absolute cross-section scale by determining first the ratio of inelastic-to-elastic scattering cross sections, and then separately measuring the absolute elastic scattering cross section. Several new electronic transitions are observed which are intrinsically overlapped in the molecule itself. Assignments of these electronic transitions are suggested. These assignments are based on present spectroscopic and cross-sections measurements, high-energy electron scattering spectra, optical absorption spectra, and ab initio molecular orbital calculations.

Chutjian, A.↗
NASA NTRS1979

The vertical structure and thickness of Saturn's rings

The steady state thickness and vertical structure of Saturn's rings are discussed with regard to whether a collapse to a monolayer due to particle collisions may be prevented by various mechanisms. The differences between thick rings and wavy monolayers are outlined and used to show that such coherent perturbations to the rings as satellite and solar gravitational effects would produce a wavy monolayer while such dispersive mechanisms as meteoroid impact, radiation pressure, Kepler shear and radial spreading, which would produce the random particle motions necessary to maintain a thick layer, are probably insignificant. Given a typical power law distribution of particle sizes, it is found that gravitational scattering of small particles by large ones would maintain a ring thickness of several times the radius of the largest particles. A steady state ring thickness of 20 to 50 meters, derived from energy considerations, would imply a maximum particle size of a few meters.

Cuzzi, J. N.↗
NASA NTRS1999

Development of Prototype Micro-Lidar using Narrow Linewidth Semiconductor Lasers for Mars Boundary Layer Wind and Dust Opacity Profiles

We have developed a compact Doppler lidar concept which utilizes recent developments in semiconductor diode laser technology in order to be considered suitable for wind and dust opacity profiling in the Mars lower atmosphere from a surface location. The current understanding of the Mars global climate and meteorology is very limited, with only sparse, near-surface data available from the Viking and Mars Pathfinder landers, supplemented by long-range remote sensing of the Martian atmosphere. The in situ measurements from a lander-based Doppler lidar would provide a unique dataset particularly for the boundary layer. The coupling of the radiative properties of the lower atmosphere with the dynamics involves the radiative absorption and scattering effects of the wind-driven dust. Variability in solar irradiance, on diurnal and seasonal time scales, drives vertical mixing and PBL (planetary boundary layer) thickness. The lidar data will also contribute to an understanding of the impact of wind-driven dust on lander and rover operations and lifetime through an improvement in our understanding of Mars climatology. In this paper we discuss the Mars lidar concept, and the development of a laboratory prototype for performance studies, using, local boundary layer and topographic target measurements.

Menzies, Robert T.↗
NASA NTRS1997

MEASUREMENT OF THE NOISE IMPROVEMENT OF A 34-METER CASSEGRAIN ANTENNA RETROFITTED WITH A LOW-BACKSCATTERING STRUT

Large axially-symmetric ground-based dual-reflector antennas are used in a variety of applications simultaneously requiring very high gain and very low noise (e.g., satellite communications, radio astronomy, deep-space communications, and radar). In these systems, reducing the noise by 10 % is equivalent to increasing the antenna gain by roughly 0.5 dB. Since the early days of radio-astronomy this fact has continuously driven efforts to reduce the noise of front-end low-noise amplifiers--a major noise contributor. As the performance of the front-end amplifiers improved, the relative importance of the noise generated by the surrounding warm ground increased, causing the antenna noise to become a major factor in the overall system sensitivity. Since large ground-based reflectors have been around for several decades, the various electrical and mechanical parameters affecting their performance have received considerable attention and are generally well understood. However, the impact of the subreflector supporting struts on the antenna noise performance remains a source of uncertainty. The reason for this stems from the usually large electrical dimensions involved, which precludes the accurate modeling of the various strut-scattering mechanisms. For the particular antennas used on NASA's Deep Space Network, which have been designed to minimize all noise sources, several studies have typically reported measured noise temperatures between 2 and 3 K (at approx. 8.45 GHz, antenna pointing at zenith), attributed to the struts and other unknown effects (see for example [1] and [2]). With this in mind, an effort has recently been conducted to determine optimal strut shapes to reduce the associated noise contribution [3].

Prata, A., Jr.↗
DOE OSTI2022

Depletion-Driven Assembly of Polymer-Coated Nanocrystals

Depletion-driven assembly has been widely studied for micron-sized colloids, but questions remain at the nanoscale where the governing physics are impacted by stabilizing surface ligands or wrapping polymers, whose dimensions are similar to those of the colloidal core and the depletant. Here, we probe how wrapping colloidal tin-doped indium oxide nanocrystals with polymers affects their depletion-induced interactions and assembly in solutions of polyethylene glycol. Copolymers of polyacrylic acid grafted with polyethylene oxide provide nanocrystal wrappings with different effective polymer graft densities and molecular weights. (Ultra) small angle X-ray scattering, coarse-grained molecular dynamics simulation, and molecular thermodynamic theory were combined to analyze how depletant size and polymer wrapping characteristics affect depletion interactions, structure, and phase behavior. The results show how depletant molecular weight, as well as surface density and molecular weight of polymer grafts, set thresholds for assembly. These signatures are unique to depletion-driven assembly of nanoscale colloids and mirror phase behaviors of grafted nanoparticle–polymer composites. Optical and rheological responses of depletion-driven assemblies of nanocrystals with different polymer shell architectures were probed to learn how their structural differences impact properties. Finally, we discuss how these wrinkles for depletion-driven assembly at the nanoscale may provide fresh opportunities for designing responsive depletion interactions and dynamically reconfigurable materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS2000

Spacewatch Survey of the Solar System

The purpose of the Spacewatch project is to explore the various populations of small objects throughout the solar system. Statistics on all classes of small bodies are needed to infer their physical and dynamical evolution. More Earth Approachers need to be found to assess the impact hazard. (We have adopted the term "Earth Approacher", EA, to include all those asteroids, nuclei of extinct short period comets, and short period comets that can approach close to Earth. The adjective "near" carries potential confusion, as we have found in communicating with the media, that the objects are always near Earth, following it like a cloud.) Persistent and voluminous accumulation of astrometry of incidentally observed main belt asteroids MBAs will eventually permit the Minor Planet Center (MPQ to determine the orbits of large numbers (tens of thousands) of asteroids. Such a large body of information will ultimately allow better resolution of orbit classes and the determinations of luminosity functions of the various classes, Comet and asteroid recoveries are essential services to planetary astronomy. Statistics of objects in the outer solar system (Centaurs, scattered-disk objects, and Trans-Neptunian Objects; TNOs) ultimately will tell part of the story of solar system evolution. Spacewatch led the development of sky surveying by electronic means and has acted as a responsible interface to the media and general public on this discipline and on the issue of the hazard from impacts by asteroids and comets.

McMillan, Robert S.↗
DOE OSTI2022

Impact of CH 4 addition on the electron properties and electric field dynamics in a Ar nanosecond-pulsed dielectric barrier discharge

Non-equilibrium plasmas derive their low temperature reactivity from producing and driving energetic electrons and active species under large electric fields. Therefore, the impact of reactants on the plasma properties including electron number density, electric field, and electron temperature is critical for applications such as plasma CH 4 reforming. Due to experimental complexity, electron properties and the electric field are rarely measured together in the same discharge. Here, we combine time-resolved Thomson scattering and electric field induced second harmonic generation (EFISH) to probe electron temperature, electron density, and electric field strength in a 60 Torr CH 4 /Ar nanosecond-pulsed dielectric barrier discharge (ns-DBD) while varying the CH 4 mole fraction from 0 to 8%. These measurements are compared to a 1-D numerical model to benchmark its predictions and identify areas of uncertainty. Nonlinear coupling between CH 4 addition, electron temperature, electron density, and the electric field was directly observed. Contrary to previous measurements in He, the electron temperature increased with CH 4 mole fraction. This rise in electron temperature is identified as electron heating by residual electric fields that increased with larger CH 4 mole fraction. Moreover, the electron number density has been found to decrease rapidly with the increase of methane mole fraction. Comparison of these measurements with the model yielded better agreement at higher CH 4 mole fractions and with the usage of ab initio calculated Ar electron-impact cross-sections from the B-spline R-matrix (BSR) database. Furthermore, the calculated plasma properties are shown to be sensitive to the residual surface charge implanted on the quartz dielectric surfaces. Without considering surface charge in the simulations, the calculated electric field profiles agreed well with the measurements, but the electron properties were underpredicted by more than a factor of three. Therefore, measurements of either the electric field or electron properties measurements alone are insufficient to fully validate modelling predictions.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS2010

Evaluating the Impact of Vegetation Cover and Atmospheric Characteristics on the Estimation of Snow Water Equivalent from Spaceborne Microwave Radiometry

A radiative transfer model for estimating snow water equivalent (SWE, mm) from satellite-observed brightness temperature (K) at 19 and 37 GHz (respectively, T(sub B(sub, sat,19)) and T(sub B(sub, sat,37)) over partially forested area is presented, as an extension of a previously published model, by considering scattering of radiation within the canopy. For the specific case of dense vegetation covering fractional area f, the model can be written as, SWE = alpha{ A. delta (T(sub B(sub, sat)) + B - C. f}/(l f), where delta T(sub B(sub, sat)), is the difference of T(sub B(sub, sat,19)) and T(sub B(sub, sat,37)), alpha(mm/K) is the slope of SWE vs. brightness temperature difference at 19 and 37 GHz that would be obtained by ignoring the presence of atmosphere, delta(T(sub B)sub g)), for a homogeneous snow cover (which varies with grain size). The parameters A, B, and C, are determined primarily by atmospheric characteristics, and for a likely range of atmospheric conditions appear to be in the range of, respectively, 1.15-1.63, 0.69-2.84 K and 0.59-2.39 K. Ignoring atmospheric correction would introduce bias towards underestimation of SWE (and also, snow cover area and snow depth). Increasing cloud liquid water path (L) has the effect of increasing A, and ignoring this variation of A with L would have the impact of biasing the estimate of SWE (and snow extent). Such biasing is further exacerbated with increasing f, because of the appearance of term (l-f) in the denominator. The impact of ignoring the intercept parameters (B and C) would be noticeable at low values of SWE (appearing as a bias towards underestimation of SWE), which has been determined to be about 6 mm for average environmental conditions. The uncertainty in estimating SWE due to variations in the atmospheric characteristics is likely to be less than 15%, but could be up to 25% for non-vegetated snow-covered areas. Better estimates of SWE (and snow extent) would be obtained by adjusting the parameters of the above model to regional differences in the atmospheric characteristics. The biases in determining SWE arising due to variations in atmospheric conditions and due to changes in fractional forest cover are not independent, since they interact as {A/(l-f)}. The present calculations also show that improvement in determining snow cover area from the microwave data is likely to occur when these data are corrected for atmospheric effects, as demonstrated by a specific case study.

Choudhury, Bhaskar J.↗