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DOE OSTI2022

Feasibility Study of Millimeter Wave Radars For Safeguards Applications

Containment and surveillance are fundamental measures in nuclear safeguards. Techniques such as video surveillance and laser curtain for containment provide effective monitoring in areas where maintaining continuity of knowledge is required. These systems, however, can be susceptible to loss of monitoring capabilities under certain environmental conditions such as poor visibility (i.e. low light conditions, smoke, fog, etc.) or extended power loss past the duration that the backup power system is designed for. Brookhaven National Laboratory has been investigating the feasibility of millimeter waves (mmWave) as a new perimeter seal in which radio frequency waves in the range of 60-64 GHz are used to detect and monitor objects of interest. Signals in this frequency range are not susceptible to environmental conditions. For proof-of-concept tests, mmWave sensors from Texas Instruments (TI), specificallyIWR6843, are used in a test bed at BNL's Waste Management facility to simulate the operations at nuclear facilities. The unique design of TI mmWave sensors requires less memory and power consumption compared to counterpart systems. These devices are capable of exporting 3D point-cloud data, which is visualized graphically and compared to videos recorded at the same time to validate the performance of the mmWave sensor. A set of experiments were planned to test the feasibility of the mmWave in this application, including monitoring static containers in a storage area and detecting intrusions at the boundaries of the area. In addition, the experiments also identify potential blind spots relative to sensor position and utilize multiple operating sensors simultaneously to reduce or eliminate such blind spots. The optimal positioning of multiple sensors was determined for the experimental room configuration. In this paper, we will discuss the details of this novel perimeter sealing concept and present the test results.

98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗

DOE OSTI2023

Geospatial Characterization of Low-Temperature Heating and Cooling Demand in the United States: Preprint

Geothermal resources at temperatures below 150 degrees C have great potential as energy sources for various direct-use applications including heating and cooling in residential and commercial buildings. This study geospatially quantifies U.S. heating and cooling demand in residential, commercial, and manufacturing sectors; heating demand in the agricultural sector; and cooling demand in data centers at the county level through end-use energy consumption, expenditure, and commissioned power analyses. Heating and cooling demand in the residential sector was estimated using energy consumption data obtained from the U.S. Energy Information Administration accounting for different U.S. climate zones. For commercial sector analysis, the end-use major fuel energy intensity at the census division level was disaggregated to the county level with respect to principal building activities. Heating and cooling demand analysis for the manufacturing sector was based on end-use energy consumption for direct-use total process categorized by the North America Industry Classification System. Fuel expenditures in the U.S. Department of Agriculture Farm Production Expenditures were examined for heating demand analysis in the agricultural sector, particularly for the greenhouse, nursery, and floriculture production category. Lastly, commissioned power for data centers in the United States were explored for cooling demand analysis. Results indicated a significant fraction of U.S. primary energy consumption is used for low-temperature heating and cooling applications. Heating and cooling demand in residential and commercial sectors is significantly affected by the number of housing units and climate zone designations, while heating and cooling demand in manufacturing and agricultural sectors and data centers are mainly dependent on the number of facilities and their locations. Maps were generated visualizing where heating and cooling demand is high and, overlain with geothermal resource maps, can indicate locations where geothermal energy can supply this heating and cooling demand.

cooling demand↗

DOE OSTI2023

Geospatial Characterization of Low-Temperature Heating and Cooling Demand in the United States

cooling demand↗

DOE OSTI2017

Observation of Downward Facing Pool Boiling on a Hemispherical Vessel under External Reactor Vessel Cooling

It is a great challenge to ensure the safety of nuclear power plant during a severe accident. One of the major concerns is to overheat the reactor core which potentially may create a nuclear crisis if the core cooling fails. The concept of In-vessel retention (IVR) by passive external reactor vessel cooling (ERVC) in a flooded cavity of pressurized water reactor (PWR) is a viable and effective approach to retain radioactive core melt within the reactor pressure vessel (RPV). As long as the heat flux at the lower head of the RPV is lower than the critical heat flux (CHF) limit at the corresponding point, nucleate boiling will be the prevailing regime. In that case, the temperature of outer surface can be maintained near the saturated temperature of water such that the reactor vessel is able to be sufficiently cooled to sustain its thermal and structural integrity. Owing to the practical significance of this IVR-ERVC concept, there were many experimental and theoretical studies to investigate the two-phase flow natural circulation phenomena including the effect of inclination angle on the CHF, based on which many different empirical or semiempirical correlations were developed for CHF by fitting the experimental results. For the engineering applications, reactor-scale facilities such as ULPU series, KAIST facility, CYBL and FIRM were built to experimentally verify and validate the feasibility of ERVC for different design of reactors. Besides, for the research on physical mechanism of downward facing pool boiling, laboratory-scale experiments such as DELTA, CASA and SBLB were performed to visually and theoretically simulate the process of IVR-ERVC. All of the aforementioned test facilities and experiments provided a simulation of the downward facing boiling process and experimental study on the CHF limits during the ERVC conditions of different types of reactors. There were also some visualized investigations on the two-phase flow behavior in both quenching and steady state experiments. In this study, a scale-down three-dimensional downward facing pool boiling facility (iSBLB) was built to investigate the two phase natural circulation flow characteristics during the ERVC process. The general morphologies of vapor mass at different locations were visually recorded using the high-speed camera. The observation results showed that vapor behavior along the hemispherical curved surface was periodical. The boiling phenomenon was quite different from those on all other surface orientations.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2013

Pilot Scale Water Gas Shift - Membrane Device for Hydrogen from Coal

The objectives of the project were to build pilot scale hydrogen separation systems for use in a gasification product stream. This device would demonstrate fabrication and manufacturing techniques for producing commercially ready facilities. The design was a 2 lb/day hydrogen device which included composite hydrogen separation membranes, a water gas shift monolith catalyst, and stainless steel structural components. Synkera Technologies was to prepare hydrogen separation membranes with metallic rims, and to adjust the alloy composition in their membranes to a palladium-gold composition which is sulfur resistant. Chart was to confirm their brazing technology for bonding the metallic rims of the composite membranes to their structural components and design and build the 2 lbs/day device incorporating membranes and catalysts. WRI prepared the catalysts and completed the testing of the membranes and devices on coal derived syngas. The reactor incorporated eighteen 2'' by 7'' composite palladium alloy membranes. These membranes were assembled with three stacks of three paired membranes. Initial vacuum testing and visual inspection indicated that some membranes were cracked, either in transportation or in testing. During replacement of the failed membranes, while pulling a vacuum on the back side of the membranes, folds were formed in the flexible composite membranes. In some instances these folds led to cracks, primarily at the interface between the alumina and the aluminum rim. The design of the 2 lb/day device was compromised by the lack of any membrane isolation. A leak in any membrane failed the entire device. A large number of tests were undertaken to bring the full 2 lb per day hydrogen capacity on line, but no single test lasted more than 48 hours. Subsequent tests to replace the mechanical seals with brazing have been promising, but the technology remains promising but not proven.

01 COAL, LIGNITE, AND PEAT↗

DOE OSTI2014

Enhancing User Customization through Novel Software Architecture for Utility Scale Solar Siting Software

There is a need for a spatial decision support application that allows users to create customized metrics for comparing proposed locations of a new solar installation. This document discusses how PVMapper was designed to overcome the customization problem through the development of loosely coupled spatial and decision components in a JavaScript plugin architecture. This allows the user to easily add functionality and data to the system. The paper also explains how PVMapper provides the user with a dynamic and customizable decision tool that enables them to visually modify the formulas that are used in the decision algorithms that convert data to comparable metrics. The technologies that make up the presentation and calculation software stack are outlined. This document also explains the architecture that allows the tool to grow through custom plugins created by the software users. Some discussion is given on the difficulties encountered while designing the system.

14 SOLAR ENERGY↗

DOE OSTI2015

Dramatic Demand Reduction In The Desert Southwest

This report summarizes a project that was funded to the University of Nevada Las Vegas (UNLV), with subcontractors Pulte Homes and NV Energy. The project was motivated by the fact that locations in the Desert Southwest portion of the US demonstrate very high peak electrical demands, typically in the late afternoons in the summer. These high demands often require high priced power to supply the needs, and the large loads can cause grid supply problems. An approach was proposed through this contact that would reduce the peak electrical demands to an anticipated 65% of what code-built houses of the similar size would have. It was proposed to achieve energy reduction through four approaches applied to a development of 185 homes in northwest part of Las Vegas named Villa Trieste. First, the homes would all be highly energy efficient. Secondly, each house would have a PV array installed on it. Third, an advanced demand response technique would be developed to allow the resident to have some control over the energy used. Finally, some type of battery storage would be used in the project. Pulte Homes designed the houses. The company considered initial cost vs. long-term savings and chose options that had relatively short paybacks. HERS (Home Energy Rating Service) ratings for the homes are approximately 43 on this scale. On this scale, code-built homes rate at 100, zero energy homes rate a 0, and Energy Star homes are 85. In addition a 1.764 Wp (peak Watt) rated PV array was used on each house. This was made up of solar shakes that were in visual harmony with the roofing material used. A demand response tool was developed to control the amount of electricity used during times of peak demand. While demand response techniques have been used in the utility industry for some time, this particular approach is designed to allow the customer to decide the degree of participation in the response activity. The temperature change in the residence can be decided by the residents by adjusting settings. In a sense the customer can choose between greater comfort and greater money savings during demand response circumstances. Finally a battery application was to be considered. Initially it was thought that a large battery (probably a sodium-sulfur type) would be installed. However, after the contract was awarded, it was determined that a single, centrally-located battery system would not be appropriate for many reasons, including that with the build out plan there would not be any location to put it. The price had risen substantially since the budget for the project was put together. Also, that type of battery has to be kept hot all the time, but its use was only sought for summer operation. Hence, individual house batteries would be used, and these are discussed at the end of this report. Many aspects of the energy use for climate control in selected houses were monitored before residents moved in. This was done both to understand the magnitude of the energy flows but also to have data that could be compared to the computer simulations. The latter would be used to evaluate various aspects of our plan. It was found that good agreement existed between actual energy use and computed energy use. Hence, various studies were performed via simulations. Performance simulations showed the impact on peak energy usage between a code built house of same size and shape compared to the Villa Trieste homes with and without the PV arrays on the latter. Computations were also used to understand the effect of varying orientations of the houses in this typical housing development, including the effect of PV electrical generation. Energy conservation features of the Villa Trieste homes decreased the energy use during peak times (as well as all others), but the resulting decreased peak occurred at about the same time as the code-built houses. Consideration of the PV generation decreases the grid energy use further during daylight hours, but did not extend long enough many days to decrease the peak. Hence, a demand response approach, as planned, was needed. With participation of the residents in the demand response program developed does enable the houses to reduce the peak demand between 66% and 72%, depending on the built years. This was addressed fully in the latter part the study and is described in the latter part of this report.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2021

A measure of active interfaces in supported catalysts for high-temperature reactions

Formulating knowledge of structure-function relationships in heterogeneous catalysis is central to the design of efficient catalysts; yet, the elucidation of dominant reaction sites has remained as a challenge. Here, in this paper, we present a methodology that can be used to visualize metal-gas and metal-oxide-gas interfaces in three dimensions and to quantify their catalytic activity levels. As a case study, CH 4 oxidation occurring in a Pt/CeO 2 system is chosen. By employing thermally robust Pt@CeO 2 model catalysts with size-tunable and monodisperse cores, and gas-permeable shells, we reconstruct a series of structures in 3D via electron tomography and match the information to activity data and theoretical calculations. This strategy reveals that two different interfaces catalyze the CH 4 oxidation and that their contribution to the overall rate changes with the Pt size, temperature, and gas atmosphere. Our results provide an analytic platform on which to explore reaction pathways and mechanisms applicable to multiple reactions and materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

Canister valve and actuator deposition in metered dose inhalers formulated with low-GWP propellants

A challenge in pressurised metered-dose inhaler (pMDI) formulation design is management of adhesion of the drug to the canister wall, valve and actuator internal components and surfaces. Wall-material interactions differ between transparent vials used for visual inspection and metal canister pMDI systems. This is of particular concern for low greenhouse warming potential (GWP) formulations where propellant chemistry and solubility with many drugs are not well understood. In this study, we demonstrate a novel application of X-ray fluorescence spectroscopy using synchrotron radiation to assay the contents of surrogate solution and suspension pMDI formulations of potassium iodide and barium sulphate in propellants HFA134a, HFA152a and HFO1234ze(E) using aluminium canisters and standard components. Preliminary results indicate that through unit life drug distribution in the canister valve closure region and actuator can vary significantly with new propellants. For solution formulations HFO1234ze(E) propellant shows the greatest increase in local deposition inside the canister valve closure region as compared to HFA134a and HFA152a, with correspondingly reduced actuator deposition. This is likely driven by chemistry changes. For suspension formulations HFA152a shows the greatest differences, due to its low specific gravity. These changes must be taken into consideration in the development of products utilising low-GWP propellants.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2014

Capacitive Deionization of High-Salinity Solutions

Desalination of high salinity solutions has been studied using a novel experimental technique and a theoretical model. Neutron imaging has been employed to visualize lithium ions in mesoporous carbon materials, which are used as electrodes in capacitive deionization for water desalination. Experiments were conducted with a flow-through capacitive deionization cell designed for neutron imaging and with lithium chloride ( 6 LiCl) as the electrolyte. Sequences of neutron images have been obtained at a relatively high concentration of lithium chloride ( 6 LiCl) solution to provide information on the transport of ions within the electrodes. A new model that computes the individual ionic concentration profiles inside mesoporous carbon electrodes has been used to simulate the capacitive deionization process. Modifications have also been introduced into the simulation model to calculate results at high electrolyte concentrations. Experimental data and simulation results provide insight into why capacitive deionization is not effective for desalination of high ionic-strength solutions. The combination of experimental information, obtained through neutron imaging, with the theoretical model will help in the design of capacitive deionization devices, which can improve the process for high ionic-strength solutions.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2015

Visualization of Electrochemically Driven Solid-state Phase Transformations Using Operando Hard X-ray Spectro-imaging

N/A

Li, L↗

DOE OSTI2015

Evolving the Land Information System into a Cloud Computing Service

The Land Information System (LIS) was developed to use advanced flexible land surface modeling and data assimilation frameworks to integrate extremely large satellite- and ground-based observations with advanced land surface models to produce continuous high-resolution fields of land surface states and fluxes. The resulting fields are extremely useful for drought and flood assessment, agricultural planning, disaster management, weather and climate forecasting, water resources assessment, and the like. We envisioned transforming the LIS modeling system into a scientific cloud computing-aware web and data service that would allow clients to easily setup and configure for use in addressing large water management issues. The focus of this Phase 1 project was to determine the scientific, technical, commercial merit and feasibility of the proposed LIS-cloud innovations that are currently barriers to broad LIS applicability. We (a) quantified the barriers to broad LIS utility and commercialization (high performance computing, big data, user interface, and licensing issues); (b) designed the proposed LIS-cloud web service, model-data interface, database services, and user interfaces; (c) constructed a prototype LIS user interface including abstractions for simulation control, visualization, and data interaction, (d) used the prototype to conduct a market analysis and survey to determine potential market size and competition, (e) identified LIS software licensing and copyright limitations and developed solutions, and (f) developed a business plan for development and marketing of the LIS-cloud innovation. While some significant feasibility issues were found in the LIS licensing, overall a high degree of LIS-cloud technical feasibility was found.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2018

A Unified Data-Driven Approach for Programming In Situ Analysis and Visualization Final Scientific/Technical Report

The goal of Kitware’s work has been the study of a unified data-driven approach for programming applications and in situ analysis and visualization. We have especially focused on understanding the interplay between data-centric programming model requirements at extreme-scale and the overall impact of those requirements on the design, capabilities, flexibility, and implementation details for both applications and the supporting in situ infrastructure. We have successfully demonstrated the use of pipeline abstractions within Legion and developed a number of algorithms that were integrated within the Legion simulation framework. This report focuses on describing milestones, mainly those focusing on exploring pipeline abstractions in the context of the Legion programming model.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2020

Multivariate Regression of Pyrotechnic Igniter Output

Multivariate multiple regression models are applied to simplified pyrotechnic igniters for the first time to understand how changes in manufactured parameters can affect the output gas dynamic response and the timing of ignition events. The statistical modeling technique is applied to demonstrate quantification of the effects of a set of independent variables measured in the as-fabricated igniters on a set of responses experimentally measured from the functioned igniters. Two independent process variables were intentionally varied following a full factorial experimental design while several other independent variables varied within their normal manufacturing variability range. The four igniter performance responses consisted of the timing of sequential events during igniter function and visual gas dynamic output in the form of shock wave strength observed with high-speed schlieren imaging. Linear regression models built using the measurements throughout the manufacturing processes and the output variance provide insight into the critical device parameters that dominate performance

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗

DOE OSTI2020

Laser Transport System Vacuum Simulations and LED Atom Tracker

MAGIS-100 is an experiment using atom interferometry on strontium atoms in a 100m vacuum chamber. The laser travels through a laser transport system (LTS) before going down the chamber. Two projects were completed over the course of the internship. One project was conducting vacuum simulations on the LTS to ensure it meets the experimental pressure requirement of 10-11 torr. This was done by characterizing the pressure profile with variations in pump size, pump spacing, and orifice size. The initial design of the LTS included one 30 L/s ion pump in the high vacuum (HV) region, a lens mount with holes of diameter 0.788”, and three 150 L/s ion pumps in the ultra-high vacuum (UHV) region. After adjusting these variables, it was concluded that the lens mount holes could be reduced to 0.200” in diameter and one 150 L/s ion pump in the UHV could be removed and still meet the experimental requirements. The other project was to design an LED atom tracker that shows the position of the strontium atoms in the 100m shaft. This will help with public outreach by allowing visitors to have a visual of the experiment. An Arduino Uno and Arduino Due were programmed using classical physics formulas to direct the RGB LED strips to flash in sync with the falling atoms. The requirements for powering and connecting the hardware were calculated and recommendations for scaling the system to 100m were made.

43 PARTICLE ACCELERATORS↗

DOE OSTI2019

Energy Modeling in Urban Districts: Forecast of Multi-Sector Energy Use and GHG Emissions

This document reports the findings of the energy use and greenhouse gases (GHG) emissions model loosely based on three districts in the San Francisco Bay Area, District A, District B, and District C. Modeling platforms exist for city energy benchmarking, inventorying, and GHG emissions forecasting and planning. However, the wide variety and features of today’s tools, their focus on a sub-set or snapshot data from various energy generation and consumption sectors, and the fact that many of them are not open data models, create sub-optimal environments for the energy analysis districts are seeking to conduct. Hence, we have developed a new software tool with customized data and dynamic visualization; DEPICT (Decision-support and Emissions Prediction Interactive Cities Tool) to obtain energy and emissions forecasts at different stages of the districts’ build-out by varying selected design parameters. This report presents the methodology and framework we have developed to estimate whole district emissions and details the results by district, with the objective of finding insights into the main sources of emissions, and the available levers to reduce them efficiently. This document details the impact of each emissions mitigation measure investigated, along with the assumption and models that were used to reach these values

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2014

From Voxels to Knowledge: A Practical Guide to the Segmentation of Complex Electron Microscopy 3D-Data

Modern 3D electron microscopy approaches have recently allowed unprecedented insight into the 3D ultrastructural organization of cells and tissues, enabling the visualization of large macromolecular machines, such as adhesion complexes, as well as higher-order structures, such as the cytoskeleton and cellular organelles in their respective cell and tissue context. Given the inherent complexity of cellular volumes, it is essential to first extract the features of interest in order to allow visualization, quantification, and therefore comprehension of their 3D organization. Each data set is defined by distinct characteristics, e.g., signal-to-noise ratio, crispness (sharpness) of the data, heterogeneity of its features, crowdedness of features, presence or absence of characteristic shapes that allow for easy identification, and the percentage of the entire volume that a specific region of interest occupies. All these characteristics need to be considered when deciding on which approach to take for segmentation. The six different 3D ultrastructural data sets presented were obtained by three different imaging approaches: resin embedded stained electron tomography, focused ion beam- and serial block face- scanning electron microscopy (FIB-SEM, SBF-SEM) of mildly stained and heavily stained samples, respectively. For these data sets, four different segmentation approaches have been applied: (1) fully manual model building followed solely by visualization of the model, (2) manual tracing segmentation of the data followed by surface rendering, (3) semi-automated approaches followed by surface rendering, or (4) automated custom-designed segmentation algorithms followed by surface rendering and quantitative analysis. Depending on the combination of data set characteristics, it was found that typically one of these four categorical approaches outperforms the others, but depending on the exact sequence of criteria, more than one approach may be successful. Based on these data, we propose a triage scheme that categorizes both objective data set characteristics and subjective personal criteria for the analysis of the different data sets.

3D electron microscopy↗

DOE OSTI2021

SIR Glass Test Vehicle Designed to Characterize Process Materials

The exposure to harsh environments can result in reliability issues on highly dense electronic packages and circuit assemblies. One area of concern is electrochemical failure mechanisms caused by electrolytic corrosion, electrochemical migration (dendrites), and leakage currents under humid conditions. These no-fault and no-trouble found failure points are challenging to detect and to perform process control during the assembly process. The focus of this research centers on metallizing glass surface insulation resistance test vehicles to characterize materials on electronic packages and components that exhibit the highest risk of failure due to material interactions and process residues. Glass test vehicles provide a visual representation of materials when they are exposed to moisture content in the air. Harsh environments can cause material interactions resulting in morphology changes, opening, and release of active components. A transparent test vehicle is highly functional for environmental stress testing under temperature, humidity, and bias. The designed experiment will evaluate the effects of material and process residues that can undergo changes in behavior during application, which leads to local failures.

Capen, Bill↗