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At least 793 records · Page 44

An upgraded frequency-selectable laser source (FLS) calibrator for CMB bandpass characterization

One of the biggest challenges for Cosmic Microwave Background (CMB) experiments comes from the uncertainty in instrument bandpass calibration. Uncertainties in bandpass can limit foreground removal and spectral fitting, which are critical for inflationary and galaxy cluster measurements. CMB experiments currently use Fourier Transform Spectrometers (FTSes) to measure instrument bandpasses. However, FTS systems are currently systematics-limited, so significant improvements in bandpass measurements require novel calibrators. To this end, we developed a Frequency-selectable Laser Source (FLS) calibrator, which uses a laser with adjustable frequency coupled to a system that allows for laser power attenuation. Following initial testing with the first FLS prototype, we developed an upgraded version of the calibrator with improved performance. We present the upgrades to the FLS calibrator, the characterization of the upgraded calibrator and new laser source, and plans for testing with microwave instruments in the field.

Saunders, Lauren J. [Fermilab] (ORCID:000000016367↗

A new time calibration method for switched-capacitor-array-based waveform samplers

Here we have developed a new time calibration method for the DRS4 waveform sampler that enables us to precisely measure the non-uniform sampling interval inherent in the switched-capacitor cells of the DRS4. The method uses the proportionality between the differential amplitude and sampling interval of adjacent switched-capacitor cells responding to a sawtooth-shape pulse. In the experiment, a sawtooth-shape pulse with a 40 ns period generated by a Tektronix AWG7102 is fed to a DRS4 evaluation board for calibrating the sampling intervals of all 1024 cells individually. The electronic time resolution of the DRS4 evaluation board with the new time calibration is measured to be ~2.4 ps RMS by using two simultaneous Gaussian pulses with 2.35 ns full-width at half-maximum and applying a Gaussian fit. The time resolution dependencies on the time difference with the new time calibration are measured and compared to results obtained by another method. Ultimately, the new method could be applicable for other switched-capacitor-array technology-based waveform samplers for precise time calibration.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

MO-D-BRD-04: NIST Air-Kerma Standard for Electronic Brachytherapy Calibrations

Electronic brachytherapy (eBT) has seen an insurgence of manufacturers entering the US market for use in radiation therapy. In addition to the established interstitial, intraluminary, and intracavitary applications of eBT, many centers are now using eBT to treat skin lesions. It is important for medical physicists working with electronic brachytherapy sources to understand the basic physics principles of the sources themselves as well as the variety of applications for which they are being used. The calibration of the sources is different from vendor to vendor and the traceability of calibrations has evolved as new sources came to market. In 2014, a new air-kerma based standard was introduced by the National Institute of Standards and Technology (NIST) to measure the output of an eBT source. Eventually commercial treatment planning systems should accommodate this new standard and provide NIST traceability to the end user. The calibration and commissioning of an eBT system is unique to its application and typically entails a list of procedural recommendations by the manufacturer. Commissioning measurements are performed using a variety of methods, some of which are modifications of existing AAPM Task Group protocols. A medical physicist should be familiar with the different AAPM Task Group recommendations for applicability to eBT and how to properly adapt them to their needs. In addition to the physical characteristics of an eBT source, the photon energy is substantially lower than from HDR Ir-192 sources. Consequently, tissue-specific dosimetry and radiobiological considerations are necessary when comparing these brachytherapy modalities and when making clinical decisions as a radiation therapy team. In this session, the physical characteristics and calibration methodologies of eBt sources will be presented as well as radiobiology considerations and other important clinical considerations. Learning Objectives: To understand the basic principles of electronic brachytherapy and the various applications for which it is being used. To understand the physics of the calibration and commissioning for electronic brachytherapy sources To understand the unique radiobiology and clinical implementation of electronic brachytherapy systems for skin and IORT techniques Xoft, Inc. contributed funding toward development of the NIST electronic brachytherapy facility (Michael Mitch).The University of Wisconsin (Wesley Culberson) has received research support funding from Xoft, Inc. Zoubir Ouhib has received partial funding from Elekta Esteya.

60 APPLIED LIFE SCIENCES↗

2016 NIST (133Xe) and Transfer (131mXe, 133mXe, 135Xe) Calibration Report

A significantly improved calibration of the High Purity Germanium detectors used by the Idaho National Laboratory Noble Gas Laboratory was performed during the annual NIST calibration. New sample spacers provide reproducible and secure support of samples at distances of 4, 12, 24, 50 and 100 cm. Bean, 15mL and 50mL Schlenk tube geometries were calibrated. Also included in this year’s calibration was a correlation of detector dead-time with sample activity that can be used to predict the schedule of counting the samples at each distance for each geometry. This schedule prediction will help staff members set calendar reminders so that collection of calibration data at each geometry will not be missed. This report also correlates the counting efficiencies between detectors, so that if the counting efficiency on one detector is not known, it can be estimated from the same geometry on another detector.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

PV Reference Cells for Outdoor Use: An Investigation of Calibration Factors

Reference cells are widely used in the photovoltaic (PV) industry to measure irradiance. For field applications and outdoor use, a variety of products are on the market, and they are often perceived as a low-cost alternative to thermopile radiometers. But reference cell characteristics differ substantially from the latter, therefore measurements made by one category of instrument cannot be substituted for or directly compared with the other. The National Renewable Energy Laboratory's (NREL's) Solar Radiation Research Laboratory is currently in a multiyear effort to develop guidance and recommendations for the design and use of outdoor reference cells, with a view to reducing inconsistencies and measurement uncertainty. The core of this effort is the long-term deployment of 39 units of 10 distinct types made by 6 manufacturers. This report compares the calibration factors provided by manufacturers - which most users rely upon - to those measured at a high level of accuracy by NREL's Cell Lab. It also reports on the application of the Broadband Outdoor Radiometer Calibration (BORCAL) method to reference cells. As a group, the factory calibrations for the crystalline silicon cells showed a small positive bias of +0.7%, with a tight distribution around this value. This is a very good result for the manufacturers. The two World Photovoltaic Scale cells constituted outliers, with a mean deviation of -0.8%, which is still within the reported uncertainty ranges. The data collected during the BORCAL procedures show a strong and systematic fluctuation of the apparent responsivity of the reference cells over the course of a day, which was anticipated. Consequently, the standard BORCAL R@45 calibration factors underestimated the reference cell responsivities by 1%-4%. An alternate responsivity indicator was developed, R'@30, incorporating adjustments for temperature response, spectral response, and directional response. This reduced the mean deviation to -0.4% compared to the Cell Lab. Further, two independent BORCAL sessions were able to produce the same values to within ±0.2%. This could be a viable approach for verifying reference cells using existing BORCAL infrastructure, for example, to evaluate their long-term stability. The daily profiles of responsivity obtained during the BORCAL sessions (provided in Appendix A) show clear patterns of differences between models, which provides evidence that their directional responses differ from each other; thus, two sensors that are calibrated correctly might give the same reading at 30° zenith angle but systematically different readings at 60°. The impact of these inconsistencies in field operation will be quantified using the long-term observations started in 2020.

14 SOLAR ENERGY↗

Status of the MODIS Level 1B Algorithms and Calibration Tables

The Moderate Resolution Imaging Spectroradiometer (MODIS) makes observations using 36 spectral bands with wavelengths from 0.41 to 14.4 m and nadir spatial resolutions of 0.25km, 0.5km, and 1km. It is currently operating onboard the NASA Earth Observing System (EOS) Terra and Aqua satellites, launched in December 1999 and May 2002, respectively. The MODIS Level 1B (L1B) program converts the sensor's on-orbit responses in digital numbers to radiometrically calibrated and geo-located data products for the duration of each mission. Its primary data products are top of the atmosphere (TOA) reflectance factors for the sensor's reflective solar bands (RSB) and TOA spectral radiances for the thermal emissive bands (TEB). The L1B algorithms perform the TEB calibration on a scan-by-scan basis using the sensor's response to the on-board blackbody (BB) and other parameters which are stored in Lookup Tables (LUTs). The RSB calibration coefficients are processed offline and regularly updated through LUTs. In this paper we provide a brief description of the MODIS L1B calibration algorithms and associated LUTs with emphasis on their recent improvements and updates developed for the MODIS collection 5 processing. We will also discuss sensor on-orbit calibration and performance issues that are critical to maintaining L1B data product quality, such as changes in the sensor's response versus scan-angle.

MODIS LEVEL 1B ALGORITHMS↗

Error Budget for a Calibration Demonstration System for the Reflected Solar Instrument for the Climate Absolute Radiance and Refractivity Observatory

A goal of the Climate Absolute Radiance and Refractivity Observatory (CLARREO) mission is to observe highaccuracy, long-term climate change trends over decadal time scales. The key to such a goal is to improving the accuracy of SI traceable absolute calibration across infrared and reflected solar wavelengths allowing climate change to be separated from the limit of natural variability. The advances required to reach on-orbit absolute accuracy to allow climate change observations to survive data gaps exist at NIST in the laboratory, but still need demonstration that the advances can move successfully from to NASA and/or instrument vendor capabilities for spaceborne instruments. The current work describes the radiometric calibration error budget for the Solar, Lunar for Absolute Reflectance Imaging Spectroradiometer (SOLARIS) which is the calibration demonstration system (CDS) for the reflected solar portion of CLARREO. The goal of the CDS is to allow the testing and evaluation of calibration approaches, alternate design and/or implementation approaches and components for the CLARREO mission. SOLARIS also provides a test-bed for detector technologies, non-linearity determination and uncertainties, and application of future technology developments and suggested spacecraft instrument design modifications. The resulting SI-traceable error budget for reflectance retrieval using solar irradiance as a reference and methods for laboratory-based, absolute calibration suitable for climatequality data collections is given. Key components in the error budget are geometry differences between the solar and earth views, knowledge of attenuator behavior when viewing the sun, and sensor behavior such as detector linearity and noise behavior. Methods for demonstrating this error budget are also presented.

radiometric calibration↗

Stability Assessment of OCO-2 Radiometric Calibration Using Aqua MODIS as a Reference

With three imaging grating spectrometers, the Orbiting Carbon Observatory-2 (OCO-2)measures high spectral resolution spectra (λ/∆λ≈19,000) of reflected solar radiation within the molecular oxygen (O2) A-band at 0.765 μm and two carbon dioxide (CO2) bands at 1.61 and 2.06 μm. OCO-2 uses onboard lamps with a reflective diffuser, solar observations through a transmissive diffuser, lunar measurements, and surface targets for radiometric calibration and validation. Separating calibrator aging from instrument degradation poses a challenge to OCO-2. Here we present a methodology for trending the OCO-2 Build 8R radiometric calibration using OCO-2 nadir observations over eight desert sites and nearly simultaneous observations from Moderate Resolution Imaging Spectroradiometer (MODIS) with sensor viewing zenith angles of 15 ± 0.5°. For the O2 A-band, this methodology is able to quantify a drift of−0.8 ± 0.1% per year and capture a small error in correcting the aging of the solar calibrator. For the other two OCO-2 bands, no measurable changes were seen, indicating less than 0.1% and less than 0.3% per year drift in the radiometric calibration of Band 2 and Band 3, respectively.

radiometric calibration↗

Evaluation of vicarious calibration for airborne sensors using RadCalNet

Vicarious calibration approaches using in-situ measurements are key techniques applied to on-orbit remote sensors. The in-situ measurements have advantages in terms of traceability and quantifiable accuracy that make them ideal for inter-consistency studies of on-orbit sensors. The Committee on Earth Observation Satellites Working Group on Calibration and Validation Infrared Visible Optical Sensors initiated the Radiometric Calibration Network (RadCalNet) to provide automated surface and top-of-atmosphere (TOA) reflectance data from multiple participating ground sites to the worldwide user community. RadCalNet standardizes protocols for collecting data, processes TOA reflectance, and provides International System of Units traceable uncertainty budgets for the five currently operating sites. RadCalNet data from the Railroad Valley Playa, Nevada, site was used to provide an SI-traceable, absolute radiometric calibration of the Enhanced MODIS Airborne Simulator as part of an overflight of opportunity during the FIREX-AQ campaign. The results shown here demonstrate the utility of RadCalNet data for absolute radiometric calibration of airborne imagers making flights of opportunity without the need for coordination with a field validation team.

Sensors↗

Bayesian Calibration of Stochastic Agent Based Model via Random Forest

Agent-based models (ABM) provide an excellent framework for modeling outbreaks and interventions in epidemiology by explicitly accounting for diverse individual interactions and environments. However, these models are usually stochastic and highly parametrized, requiring precise calibration for predictive performance. When considering realistic numbers of agents and properly accounting for stochasticity, this high-dimensional calibration can be computationally prohibitive. This paper presents a random forest-based surrogate modeling technique to accelerate the evaluation of ABMs and demonstrates its use to calibrate an epidemiological ABM named CityCOVID via Markov chain Monte Carlo (MCMC). The technique is first outlined in the context of CityCOVID's quantities of interest, namely hospitalizations and deaths, by exploring dimensionality reduction via temporal decomposition with principal component analysis (PCA) and via sensitivity analysis. The calibration problem is then presented, and samples are generated to best match COVID-19 hospitalization and death numbers in Chicago from March to June in 2020. Further, these results are compared with previous approximate Bayesian calibration (IMABC) results, and their predictive performance is analyzed, showing improved performance with a reduction in computation.

60 APPLIED LIFE SCIENCES↗

Clusters of Monoisotopic Elements for Calibration in (TOF) Mass Spectrometry

Precise calibration in TOF MS requires suitable and reliable standards, which are not always available for high masses. We evaluated inorganic clusters of the monoisotopic elements gold and phosphorus (Au{sub n}{sup +}/Au{sub n}{sup -} and P{sub n}{sup +}/P{sub n}{sup -}) as an alternative to peptides or proteins for the external and internal calibration of mass spectra in various experimental and instrumental scenarios. Monoisotopic gold or phosphorus clusters can be easily generated in situ from suitable precursors by laser desorption/ionization (LDI) or matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS). Their use offers numerous advantages, including simplicity of preparation, biological inertness, and exact mass determination even at lower mass resolution. We used citrate-stabilized gold nanoparticles to generate gold calibration clusters, and red phosphorus powder to generate phosphorus clusters. Both elements can be added to samples to perform internal calibration up to mass-to-charge (m/z) 10–15,000 without significantly interfering with the analyte. We demonstrated the use of the gold and phosphorous clusters in the MS analysis of complex biological samples, including microbial standards and total extracts of mouse embryonic fibroblasts. We believe that clusters of monoisotopic elements could be used as generally applicable calibrants for complex biological samples. .

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Iodine-Containing Mass-Defect-Tuned Dendrimers for Use as Internal Mass Spectrometry Calibrants

Calibrants based on synthetic dendrimers have been recently proposed as a versatile alternative to peptides and proteins for both MALDI and ESI mass spectrometry calibration. Because of their modular synthetic platform, dendrimer calibrants are particularly amenable to tailoring for specific applications. Utilizing this versatility, a set of dendrimers has been designed as an internal calibrant with a tailored mass defect to differentiate them from the majority of natural peptide analytes. This was achieved by incorporating a tris-iodinated aromatic core as an initiator for the dendrimer synthesis, thereby affording multiple calibration points (m/z range 600–2300) with an optimized mass-defect offset relative to all peptides composed of the 20 most common proteinogenic amino acids. .

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Validation of Calibration Parameters for Trapped Ion Mobility Spectrometry

Using contemporary theory for ion mobility spectrometry (IMS), gas-phase ion mobilities within a trapped ion mobility-mass spectrometer (TIMS) are not easily deduced using first principle equations due to non-linear pressure changes and consequently variations in E/N. It is for this reason that prior literature values have traditionally been used for TIMS calibration. Additionally, given that verified mobility standards currently do not exist and the that the exact conditions used to measure reported literature values may not always represent the environment within the TIMS, a direct approach to validating the behavior of the TIMS system is warranted. A calibration procedure is presented where an ambient pressure, ambient temperature, two-gate, printed circuit board drift-tube IMS (PCBIMS) is coupled to the front of a TIMS allowing reduced mobilities to be directly measured on the same instrument as the TIMS. These measured mobilities were used to evaluate the TIMS calibration procedure which correlates reduced mobility and TIMS elution voltages with literature values. When using the measured PCBIMS-reduced mobilities of tetraalkyl ammonium salts and tune mix for TIMS calibration of the alkyltrimethyl ammonium salts, the percent error is less than 1% as compared with using the reported literature K{sub 0} values where the percent error approaches 5%. This method provides a way to obtain accurate reference mobilities for ion mobility techniques that require a calibration step (i.e., TIMS and TWAVE). .

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Calibration of parallel bond parameters in bonded particle models via physics-informed adaptive moment optimisation

This study proposes an automated calibration procedure for bond parameters in bonded discrete element modelling. By exploring the underlying physical correlations between microscopic parameters of bonds and macroscopic strength parameters of the continuum to be modelled, the microscopic shear strength and tensile strength are identified as independent variables for calibration purpose. Then a physics-informed iterative scheme is proposed to automatically approximate the bond parameters by viewing the micro-macro relation as an implicitly defined mathematical mapping function. As a result of highly non-convex features of this implicit mapping, the adaptive moment estimation (Adam), which is especially suitable for problems with noisy gradients, is adopted as the basic iterative scheme, in conjunction with other numerical techniques to approximately evaluate the partial derivatives involved. The whole procedure offers a simple and effective framework for bond parameter calibration. Finally, a numerical example of SiC ceramic is provided for validation. By compared with some existing calibration methods, the proposed method shows significant advantages in terms of calibration efficiency and accuracy.

42 ENGINEERING↗

A calibration method for overconstrained spatial translational parallel manipulators

A calibration method for overconstrained spatial translational parallel mechanisms is proposed. The calibration of a Tri-pyramid overconstrained parallel robot is used as a vehicle to demonstrate the methodology and verify its feasibility. The proposed methodology consists of transforming the overconstrained mechanism of the robot into a non-overconstrained mechanism by replacing its redundant constraints with generalized forces (couples). The kinematic model of the non-overconstrained mechanism is derived using vector loops while its mechanical model is established by the energy method. An integrated kinematic model of the original overconstrained parallel robot is subsequently established by expressing the actual position of the end effector as the sum of the position derived by the kinematic model of the non-overconstrained mechanism and of the force-induced deformations at the end effector derived from the mechanical model. To assess the feasibility and the attainable improvements in accuracy through calibration, the positions of the end effector of the Tri-pyramid robot were measured by a method that uses a Double Ball Bar (DBB) and a 3-axes linear stage with micrometers. Based on the integrated kinematic model of the robot and the measured data, its structural parameters were identified by the Newton–Raphson iteration and least squares methods to complete the calibration. The calibration result shows that accuracy improvements on the order of 90% are achievable.

42 ENGINEERING↗

A gain series method for accurate EMCCD calibration

Abstract Calibration of the gain and digital conversion factor of an EMCCD is necessary for accurate photon counting. We present a new method to quickly calibrate multiple gain settings of an EMCCD camera. Acquiring gain-series calibration data and analyzing the resulting images with the EMCCD noise model more accurately estimates the gain response of the camera. Furthermore, we develop a method to compare the results from different calibration approaches. Gain-series calibration outperforms all other methods in this self-consistency test.

36 MATERIALS SCIENCE↗

Robotic calibration of the motional Stark effect diagnostic on Alcator C-Mod

The capability to calibrate diagnostics, such as the Motional Stark Effect (MSE) diagnostic, without using plasma or beam-into-gas discharges will become increasingly important on next step fusion facilities due to machine availability and operational constraints. A robotic calibration system consisting of a motorized three-axis positioning system and a polarization light source capable of generating arbitrary polarization states with a linear polarization angle accuracy of <0.05° has been constructed and has been used to calibrate the MSE diagnostic deployed on Alcator C-Mod. The polarization response of the complex diagnostic is shown to be fully captured using a Fourier expansion of the detector signals in terms of even harmonics of the input polarization angle. The system's high precision robotic control of position and orientation allow it to be used also to calibrate the geometry of the instrument's view. Combined with careful measurements of the narrow bandpass spectral filters, this system fully calibrates the diagnostic without any plasma discharges. The system's high repeatability, flexibility, and speed has been exploited to quantify several systematics in the MSE diagnostic response, providing a more complete understanding of the diagnostic performance.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Fast wavelength calibration method for spectrometers based on waveguide comb optical filter

A novel fast wavelength calibration method for spectrometers based on a standard spectrometer and a double metal-cladding waveguide comb optical filter (WCOF) is proposed and demonstrated. By using the WCOF device, a wide-spectrum beam is comb-filtered, which is very suitable for spectrometer wavelength calibration. The influence of waveguide filter’s structural parameters and the beam incident angle on the comb absorption peaks’ wavelength and its bandwidth are also discussed. The verification experiments were carried out in the wavelength range of 200–1100 nm with satisfactory results. Comparing with the traditional wavelength calibration method based on discrete sparse atomic emission or absorption lines, the new method has some advantages: sufficient calibration data, high accuracy, short calibration time, fit for produce process, stability, etc.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗