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At least 775 records · Page 43

Modification of the continuous flow diffusion chamber for use in zero-gravity

The design philosophy and performance characteristics of the continuous flow diffusion chamber developed for use in ground-based simulation of some of the experiments planned for the atmospheric cloud physics laboratory during the first Spacelab flight are discussed. Topics covered include principle of operation, thermal control, temperature measurement, tem-powered heat exchangers, wettable metal surfaces, sample injection system, and control electronics.

Keyser, G.↗

Direct coupling of microbore HPLC columns to MS systems

A detailed investigation using electron microscopy was conducted which examined the conditions of materials used in the construction of stable, high performance microbore liquid chromatography (LC) columns. Small details proved to be important. The effects of temperature on the elution of several homologous series used as probe compounds was examined in reverse phase systems. They showed that accessible temperature changes provide roughly half the increase in solvent strength that would be obtained going from a 100% aqueous to a 100% organic mobile phase, which is sufficient to warrant their use in many analyses requiring the use of gradients. Air circulation temperature control systems provide the easiest means of obtaining rapid, wide range changes in column temperature. However, slow heat transfer from the gas leads to thermal nonuniformity in the column and a decrease in resolution as the temperature program progresses.

Mcnair, H. M.↗

Geoscience Laser Altimeter System (GLAS) Loop Heat Pipes: An Eventual First Year On-Orbit

Goddard Space Flight Center's Geoscience Laser Altimeter System (GLAS) is the sole scientific instrument on the Ice, Cloud and land Elevation Satellite (ICESat) that was launched on January 12, 2003 from Vandenberg AFB. A thermal control architecture based on propylene Loop Heat Pipe technology was developed to provide selectable/stable temperature control for the lasers and other electronics over the widely varying mission environment. Following a nominal LHP and instrument start-up, the mission was interrupted with the failure of the first laser after only 36 days of operation. During the 5-month failure investigation, the two GLAS LHPs and the electronics operated nominally, using heaters as a substitute for the laser heat load. Just prior to resuming the mission, following a seasonal spacecraft yaw maneuver, one of the LHPs deprimed and created a thermal runaway condition that resulted in an emergency shutdown of the GLAS instrument. This paper presents details of the LHP anomaly, the resulting investigation and recovery, along with on-orbit flight data during these critical events.

Grob, E.↗

Unitized Regenerative Fuel Cell System Model Development

A Unitized Regenerative Fuel Cell (URFC) Energy Storage System is being developed at the NASA Glenn Research Center. This URFC system is unique in that it uses the surface area of the hydrogen and oxygen storage tanks as radiating heat surfaces for overall thermal control of the system. The tank surfaces also play an important role in the temperature control of regenerative gas dryers/humidifiers used to dry the hydrogen and oxygen gases produced by electrolysis during the charging and also used to humidify the hydrogen and oxygen gases used by fuel cell during the discharging of the URFCS. A bi- directional pressure controller is used to control the pressure of the oxygen and hydrogen gas inside the URFC stack during both charging and discharging of the URFC system. A water storage accumulator is used to store water reactant and control water pressure inside the URFC stack.

Burke, Kenneth A.↗

System for Testing Thermal Insulation of Pipes

An apparatus and method have been developed for measuring the rates of leakage of heat into pipes carrying liquids, the purpose of the measurements being to quantify the thermal performance of the insulation system. The apparatus is designed primarily for testing pipes used to carry cryogenic liquids, but can also be used for measuring the thermal performance of other insulated pipes or piping systems. The basic measurement principle is straightforward: The outer surface of the pipe insulation is maintained at a fixed warmer temperature. The interior of the pipe is maintained in a narrow fixed lower-temperature range by means of a regular liquid (e.g., water) that is pumped through the pipe at a known flow rate or a cryogenic liquid (e.g., nitrogen) that is saturated at atmospheric pressure and replenished until steady-state conditions are achieved. In the case of water or another liquid pumped through, the inlet and outlet temperatures are measured and heat-leak power is calculated as the mass flow rate of the liquid multiplied by the specific heat of the liquid multiplied by the inlet-to-outlet temperature rise of the liquid. In the case of liquid nitrogen or another low-temperature boiling liquid, the heat-leak power is calculated as the rate of boil-off multiplied by the latent heat of vaporization of the liquid. Then the thermal-insulation performance of the pipe system can be calculated as a function of the measured heat-leak power, the inner and outer boundary temperatures, and the dimensions of the pipe. The apparatus can test as many as three pipes simultaneously. The pipes can have inner diameters up to .15 cm and outer diameters up to .20 cm. The lengths of the pipes may vary; typical lengths are of the order of 18 m. Two thermal guard boxes . one for each end of the pipe(s) under test . are used to make the inlet and outlet fluid connections to the pipe(s) (see figure). The connections include bellows that accommodate thermal expansion and contraction of the pipes. The guard boxes and pipe(s) are positioned so that the pipe(s) slope upward from the upstream to the downstream end at an angle of at least 2 . The upward slope allows vapor bubbles to accumulate at the downstream end. The thermal guard boxes keep the ends of the pipes at the lower interior temperature to prevent spurious lengthwise leakage of heat into the pipes. It is important to prevent this spurious heat leakage because, if it were allowed to occur, it could contribute a large error in the measured heat-leak power. The upstream thermal guard box includes a heat exchanger through which liquid flowing into the pipe(s) is subcooled to the saturation temperature corresponding to the ambient pressure. Conversely, this heat exchanger can also be used to warm the flowing liquid to a desired fixed temperature. The apparatus includes a temperature control device that is placed around each pipe under test. Each device is operated under thermostatic control to maintain the outer surface of the pipe insulation at the specified test temperature. All measurements are recorded on a portable data-acquisition system.

Fesmire, James E.↗

Removing Rotational Variations from Shoulder Thermocouples in Friction Stir Welding

Thick plate and lower temperature friction stir welding results in good post-weld properties by welding at very low tool rotational speeds. Low speeds cause large variations in the measured shoulder temperature, making temperature control difficult. This paper describes a computationally light method to correct for oscillating measured temperatures. Data is collected over the previous two revolutions and used to build a compensation table and calculate a derivative. In simulation, measured temperature variations are reduced by a factor of five to ten. Temperature data is preserved and not cornered, nor is any time delay induced by this method, unlike with filtering methods.

Friction Stir Welding, Temperature↗

Thermodynamics and dehydration/hydration behaviors of Na-sulfate, -borate, and -bicarbonate minerals

Here, detailed thermal experiments using relative humidity- (RH) and temperature-controlled X-ray diffraction (XRD) and H 2 O adsorption/desorption measurements were applied to understand the dehydration/hydration behaviors of thenardite/mirabilite (Na 2 SO 4 /Na 2 SO 4 ·10H 2 O), tincalconite/borax (Na 2 B 4 O 7 ·5H 2 O/Na 2 B 4 O 7 ·10H 2 O), nahcolite (NaHCO 3 ), and qilianshanite (NaH 4 (BO 3 ) (CO 3 )·2H 2 O or NaHCO 3 ·H 3 BO 3 ·2H 2 O). The thermal behaviors of thenardite/mirabilite and tincalconite/borax were evaluated at room temperature as a function of RH. Hydration of thenardite to mirabilite is very sluggish and does not begin until at least 85 % RH, whereas dehydration of mirabilite to thenardite occurs at ~76 % RH. The reactions are accessible in the solid state and were not completely reversible on the time scale of these measurements. Qilianshanite appears stable under room conditions, as long as the RH is >20 %, supported by 2.5 months of observation during exposure to room air of known RH. Qilianshanite persists metastably for at least two days when exposed to both wet and 0% RH atmospheres at room temperature, observed during environment-controlled XRD. Below 20 % RH, qilianshanite sluggishly reacts to form tincalconite and nahcolite. When heated, qilianshanite broke down at 70 °C based on XRD results, and thermogravimetric analysis (TGA) confirmed a dehydration temperature of ~75 °C. Tincalconite hydrated to borax at 80 % RH, and dehydration from borax to tincalconite occurred at 40–50 % RH, illustrating the effective reversibility of the reaction under room conditions. The minor phase nahcolite originally in qilianshanite remained in the residue of decomposed qilianshanite after heating to 125 °C, demonstrated by continuous XRD measurements, whereas nahcolite was largely dehydrated when heated to ~100 °C during TGA. The difference can be attributed to the slower reaction kinetics in the environmental XRD. These results shed considerable light on the behavior of these minerals in the environment, particularly in evaporite deposits in Antarctica, where all of these minerals are reacting with the atmosphere on a diurnal-to-seasonal basis.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Improving Thermal Model Prediction Through Statistical Analysis of Irradiation and Post-Irradiation Data from AGR Experiments

As part of the High Temperature Reactors (HTR) R&D program, a series of irradiation tests, designated as Advanced Gas-cooled Reactor (AGR), have been defined to support development and qualification of fuel design, fabrication process, and fuel performance under normal operation and accident conditions. The AGR tests employ fuel compacts placed in a graphite cylinder shrouded by a steel capsule and instrumented with thermocouples (TC) embedded in graphite blocks enabling temperature control. While not possible to obtain by direct measurements in the tests, crucial fuel conditions (e.g., temperature, neutron fast fluence, and burnup) are calculated using core physics and thermal modeling codes. This paper is focused on AGR test fuel temperature predicted by the ABAQUS code's finite element-based thermal models. The work follows up on a previous study, in which several statistical analysis methods were adapted, implemented in the NGNP Data Management and Analysis System (NDMAS), and applied for qualification of AGR-1 thermocouple data. Abnormal trends in measured data revealed by the statistical analysis are traced to either measuring instrument deterioration or physical mechanisms in capsules that may have shifted the system thermal response. The main thrust of this work is to exploit the variety of data obtained in irradiation and post-irradiation examination (PIE) for assessment of modeling assumptions. As an example, the uneven reduction of the control gas gap in Capsule 5 found in the capsule metrology measurements in PIE helps identify mechanisms other than TC drift causing the decrease in TC readings. This suggests a more physics-based modification of the thermal model that leads to a better fit with experimental data, thus reducing model uncertainty and increasing confidence in the calculated fuel temperatures of the AGR-1 test.

99 GENERAL AND MISCELLANEOUS↗

Thermoradiative energy conversion in infrared interband cascade InAs/GaSb/AlInSb/GaSb type-II superlattice diodes

Thermoradiative energy conversion presents a means for the direct conversion of thermal energy through radiative transfer to a cold scene. However, much of the study of thermoradiative principles has been based on theory and simulations, with only sparse reports on the experimental demonstration of the concept. This work studies thermoradiative energy conversion in InAs/GaSb/AlInSb/GaSb type-II superlattice cascade devices. The devices exhibit a cutoff wavelength of 3.2 μm at 300 K, corresponding to a bandgap of 0.39 eV. Testing under a temperature-controlled chamber and scene demonstrates a maximum power density of 2.9 mW/m2 at a cell temperature of 121 °C. It is consistent with expected values for device operation limited by Shockley–Read–Hall non-radiative recombination. This result is a significant step in providing an experimental demonstration of thermoradiative energy conversion and a means to characterize cell performance, providing a foundation for further development to achieve practical values for power generation.

Islam, Md Toriqul (ORCID:0000000249871320)↗

Long life reliability thermal control systems study

The results of a program undertaken to conceptually design and evaluate a passive, high reliability, long life thermal control system for space station application are presented. The program consisted of four steps: (1) investigate and select potential thermal system elements; (2) conceive, evaluate and select a thermal control system using these elements; (3) conduct a verification test of a prototype segment of the selected system; and (4) evaluate the utilization of waste heat from the power supply. The result of this project is a conceptual thermal control system design which employs heat pipes as primary components, both for heat transport and temperature control. The system, its evaluation, and the test results are described.

Scollon, T. R., Jr.↗

Space environmental effects on adhesives for the Galileo spacecraft

Requirements for the adhesives used on the Galileo Jovian probe are discussed, and the results of mechanical and radiation experiments for their qualification are presented. The five types of adhesives used for the Wide Field Camera, SXA Antenna, temperature control louvers, and structural bonds all passed the proton and electron tests and the low temperature radiation tests. Possible bond improvements through techniques including gamma ray radiation exposure and ion implantation are also considered.

Bouquet, F. L.↗

Activation and proliferation of lymphocytes and other mammalian cells in microgravity

The experimental findings reviewed in this chapter support the following conclusions: Proliferation. Human T-lymphocytes, associated with monocytes as accessory cells, show dramatic changes in the centrifuge, in the clinostat and in space. In free-floating cells the mitogenic response is depressed by 90% in microgravity, whereas in cells attached to a substratum activation is enhanced by 100% compared to 1-G ground and inflight controls. The duration of phase G1 of the mitotic cycle of HeLa cells is reduced in hypergravity, resulting in an increased proliferation rate. Other systems like Friend cells and WI38 human embryonic lung cells do not show significant changes. Genetic expression and signal transduction. T-lymphocytes and monocytes show important changes in the expression of cytokines like interleukin-1, interleukin-2, interferon-gamma and tumor necrosis factor. The data from space experiments in Spacelab, Space Shuttle mid-deck, and Biokosmos have helped to clarify certain aspects of the mechanism of T-cell activation. Epidermoid A431 cells show changes in the genetic expression of the proto-oncogenes c-fos and c-jun in the clinostat and in sounding rockets. Membrane function, in particular the binding of ligates as first messengers of a signal, is not changed in most of the cell systems in microgravity. Morphology and Mortility. Free cells, lymphocytes in particular, are able to move and form aggregates in microgravity, indicating that cell-cell contacts and cell communications do take place in microgravity. Dramatic morphological and ultrastructural changes are not detected in cells cultured in microgravity. Important experiments with single mammalian cells, including immune cells, were carried out recently in three Spacelab flights, (SL-J, D-2, and IML-2 in 1992, 1993, and 1994, respectively). The results of the D-2 mission have been published in ref. 75; those of the IML-2 mission in ref. 76. Finally, many cell biology experiments in space have suffered in the past from a lack of adequate controls (like 1-G centrifuges) and of proper experimental conditions (like well-controlled temperature). In this respect the availability of Biorack, outfitted with proper incubators with 1-G control centrifuge as well as a glovebox with a microscope, is a great advantage. It is also desirable that cell biology experiments in space are accompanied or even preceded by a program of ground-based investigations in the fast rotating clinostat and in the centrifuge, and that preparatory experiments be done in parabolic flights and sounding rockets, whenever possible. Proper publication of the results of space experiments is another important need. A great number of data have been published in proceedings and reports that are not available to the broad scientific community. To guarantee the credibility and the international recognition of space biology it is important that the results be published in international, peer reviewed journals.

manned↗

Interannual Variations and Trends in Global Land Surface Phenology Derived from Enhanced Vegetation Index During 1982-2010

Land swiace phenology is widely retrieved from satellite observations at regional and global scales, and its long-term record has been demonstmted to be a valuable tool for reconstructing past climate variations, monitoring the dynamics of terrestrial ecosystems in response to climate impacts, and predicting biological responses to future climate scenarios. This srudy detected global land surface phenology from the advanced very high resolution radiometer (AVHRR) and the Moderate Resolution Imaging Spectroradiometer (MODIS) data from 1982 to 2010. Based on daily enhanced vegetation index at a spatial resolution of 0.05 degrees, we simulated the seasonal vegetative trajectory for each individual pixel using piecewise logistic models, which was then used to detect the onset of greenness increase (OGI) and the length of vegetation growing season (GSL). Further, both overall interannual variations and pixel-based trends were examIned across Koeppen's climate regions for the periods of 1982-1999 and 2000-2010, respectively. The results show that OGI and OSL varied considerably during 1982-2010 across the globe. Generally, the interarmual variation could be more than a month in precipitation-controlled tropical and dry climates while it was mainly less than 15 days in temperature-controlled temperate, cold, and polar climates. OGI, overall, shifted early, and GSL was prolonged from 1982 to 2010 in most climate regions in North America and Asia while the consistently significant trends only occurred in cold climate and polar climate in North America. The overall trends in Europe were generally insignificant. Over South America, late OGI was consistent (particularly from 1982 to 1999) while either positive or negative OSL trends in a climate region were mostly reversed between the periods of 1982-1999 and 2000-2010. In the Northern Hemisphere of Africa, OGI trends were mostly insignificant, but prolonged GSL was evident over individual climate regions during the last 3 decades. OGI mainly showed late trends in the Southern Hemisphere of Africa while GSL was reversed from reduced GSL trends (1982-1999) to prolonged trends (2000-2010). In Australia, GSL exhibited considerable interannual variation, but the consistent trend lacked presence in most regions. Finally, the proportion of pixels with significant trends was less than I% in most of climate regions although it could be as large as 10%.

remote sensing↗

Investigating On-Orbit Attitude Determination Anomalies for the Solar Dynamics Observatory Mission

The Solar Dynamics Observatory (SDO) was launched on February 11, 2010 from Kennedy Space Center on an Atlas V launch vehicle into a geosynchronous transfer orbit. SDO carries a suite of three scientific instruments, whose observations are intended to promote a more complete understanding of the Sun and its effects on the Earth's environment. After a successful launch, separation, and initial Sun acquisition, the launch and flight operations teams dove into a commissioning campaign that included, among other things, checkout and calibration of the fine attitude sensors and checkout of the Kalman filter (KF) and the spacecraft s inertial pointing and science control modes. In addition, initial calibration of the science instruments was also accomplished. During that process of KF and controller checkout, several interesting observations were noticed and investigated. The SDO fine attitude sensors consist of one Adcole Digital Sun Sensor (DSS), two Galileo Avionica (GA) quaternion-output Star Trackers (STs), and three Kearfott Two-Axis Rate Assemblies (hereafter called inertial reference units, or IRUs). Initial checkout of the fine attitude sensors indicated that all sensors appeared to be functioning properly. Initial calibration maneuvers were planned and executed to update scale factors, drift rate biases, and alignments of the IRUs. After updating the IRU parameters, the KF was initialized and quickly reached convergence. Over the next few hours, it became apparent that there was an oscillation in the sensor residuals and the KF estimation of the IRU bias. A concentrated investigation ensued to determine the cause of the oscillations, their effect on mission requirements, and how to mitigate them. The ensuing analysis determined that the oscillations seen were, in fact, due to an oscillation in the IRU biases. The low frequencies of the oscillations passed through the KF, were well within the controller bandwidth, and therefore the spacecraft was actually following the oscillating biases, resulting in movement of the spacecraft on the order of plus or minus 20 arcsec. Though this level of error met the ACS attitude knowledge requirement of [35, 70, 70] arcsec, 3 sigma, the desire of the ACS and instrument teams was to remove as much of the oscillation as possible. The Kearfott IRUs have an internal temperature controller, designed to maintain the IRU temperature at a constant temperature of approximately 70 C, thus minimizing the change in the bias drift and scale factors of the mechanical gyros. During ground testing of the observatory, it was discovered that the 83-Hz control cycle of the IRU heaters put a tremendous amount of stress on the spacecraft battery. Analysis by the power systems team indicated that the constant charge/discharge on the battery due to the IRU thermal control cycle could potentially limit the life of the battery. After much analysis, the decision was made not to run the internal IRU heaters. Analysis of on orbit data revealed that the oscillations in the IRU bias had a connection to the temperature of the IRU; changes in IRU temperature resulted in changes in the amplitude and period of the IRU biases. Several mitigating solutions were investigated, the result of which was to tune the KF with larger IRU noise assumptions which allows the KF to follow and correct for the time-varying IRU biases.

Vess, Melissa F.↗

Reduced deuterium retention in simultaneously damaged and annealed tungsten

Deuterium (D) retention in polycrystalline tungsten (W) with copper (Cu) ion damage concurrently produced at elevated surface temperature is investigated in this paper. An in situ heated stage held W samples at a controlled temperature up to 1243 K, which were subjected to displacement damage produced by 3.4 MeV Cu ions. D retention is subsequently explored by exposure of the W samples held at 383 K to a D 2 plasma ion fluence of 10 24 D + /m 2 . Nuclear reaction analysis (NRA), utilizing the D( 3 He,p) 4 He nuclear reaction, is used to probe the D concentration in the near surface up to 6 μm. Thermal desorption spectroscopy (TDS) is used to measure outgassed HD and D 2 molecules to determine the bulk D concentration. Both NRA and TDS measure a significant reduction in D retention for samples damaged at elevated temperature. TDS quantitatively shows that the lowest energy trap remains largely unaffected while higher energy traps, induced by Cu ions, are annealed and approach intrinsic concentrations as the temperature during ion damage approaches 1243 K. Finally, analysis of TDS data yields an activation energy of (0.10 ± 0.02) eV for recovery of ion-damage induced traps at elevated temperature.

36 MATERIALS SCIENCE↗

Effects of Warming on Tree Species’ Recruitment in Deciduous Forests of the Eastern United States

Climate change is restructuring forests of the United States, although the details of this restructuring are currently uncertain. Rising temperatures of 2 to 8oC and associated changes in soil moisture will shift the competitive balance between species that compete for light and water, and so change their abilities to produce seed, germinate, grow, and survive. We have used large-scale experiments to determine the effects of warming on the most sensitive stage of species distributions, i.e., recruitment, in mixed deciduous forests in southern New England and in the Piedmont region of North Carolina. Two questions organized our research: (1) Might temperate tree species near the “warm” end of their range in the eastern United States decline in abundance during the coming century due to projected warming? and (2) Might trees near the “cool” end of their range in the eastern United States increase in abundance, or extend their range, during the coming 100 years because of projected warming? To explore these questions, we exposed seedlings to air and soil warming experiments in two eastern deciduous forest sites; one at the Harvard Forest (HF) in central Massachusetts, and the other at the Duke Forest (DF) in the Piedmont region of North Carolina. We focused on tree species common to both Harvard and Duke Forests (such as red, black, and white oaks), those near northern range limits (black oak, flowing dogwood, tulip poplar), and those near southern range limits (yellow birch, sugar maple, Virginia pine). At each site, we planted seeds and seedlings in common gardens established in temperature-controlled, open-top chambers. The experimental design was replicated and fully factorial and involved three temperature regimes (ambient, +3oC and +5oC) and two light regimes (closed forest canopy (low light) and gap conditions (high light)). Measured variables included Winter/Spring responses to temperature and mid-Summer responses to low soil moisture. This research will advance our understanding of how the abundances and geographic distributions of several important eastern tree species near the cool and warm ends of their ranges will change during the century because of projected warming. Warming-induced changes in eastern tree abundances and distributions have the potential to affect both the quality and quantity of goods and services provided by eastern forests, and will therefore be of importance to society.

59 BASIC BIOLOGICAL SCIENCES↗

Heat treatment procedure to increase ductility of degraded nickel alloy

Tests demonstrate the room temperature ductility of degraded Rene 41 can be increased to acceptable values by solution heat treatment at a temperature of 2050 degrees to 2150 degrees F /1 to 2 hours/ and cooling through a controlled temperature range followed by normal aging in air /16 hours at 1400 degrees F/.

Prager, M.↗

Heat pipe thermal control system concept for the space station.

A program was undertaken to design and evaluate a high reliability, long life thermal control system for Space Station application. The program consisted of three sequential steps including the investigation of many thermal control elements to select the most reliable. The elements are combined into several system concepts. The most desirable approach is then selected and its characteristics are determined. The result of this project is a conceptual thermal control system design that employs heat pipes as primary components, both for heat transport and variable temperature control.

Scollon, T. R., Jr.↗