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At least 775 records · Page 43

Material interactions with the Low Earth Orbital (LEO) environment: Accurate reaction rate measurements

To resolve uncertainties in estimated LEO atomic oxygen fluence and provide reaction product composition data for comparison to data obtained in ground-based simulation laboratories, a flight experiment has been proposed for the space shuttle which utilizes an ion-neutral mass spectrometer to obtain in-situ ambient density measurements and identify reaction products from modeled polymers exposed to the atomic oxygen environment. An overview of this experiment is presented and the methodology of calibrating the flight mass spectrometer in a neutral beam facility prior to its use on the space shuttle is established. The experiment, designated EOIM-3 (Evaluation of Oxygen Interactions with Materials, third series), will provide a reliable materials interaction data base for future spacecraft design and will furnish insight into the basic chemical mechanisms leading to atomic oxygen interactions with surfaces.

Visentine, James T.↗

Electron beam fluorescence measurements in the Boeing hypersonic shock tunnel

The Calspan electron beam fluorescence (EBF) measurement system is described along with the results of measurements made in hypersonic flow. Numerous self-emitting metallic species were identified, many of which may be associated with an aging/erosion process within the B30HST. Because there were only 16 tunnel runs, it was only possible to obtain spectral measurements over a limited range of wavelengths and time sampling periods. Many spectral features of the flow remain uninvestigated. Because flow self-emission is important to all optical diagnostic techniques, it is recommended that additional spectral studies by performed. The three electron beam-excited species that were identified are nitrogen, helium, and nitric oxide. The high metallic radiation background interfered with attempts to obtain the time-wise variation of N2 density and He radiation with the optical fiber/PMT channels. In the case of the N2 density measurements the result of interference was increased uncertainty. Unfortunately, the interference caused the time-wise He measurements to fail completely. It is recommended that the electron beam be modulated to provide discrimination against the background radiation in future N2 density measurements. Careful data reduction produced useful measurements of N2 vibrational temperature, even though the high background from metallic species significantly increased measurement uncertainty. Perhaps the recommended additional spectral studies would reveal N2(+) First Negative System band-pair regions having less background. Detection of the He arrival was easily accomplished with the spectrometer/array detector system. Because of this, it is recommended that this means of detecting He arrival be used in the future. With proper calibrations of the system an He number density could be obtained. Although the flow conditions were out of limits for the run in which the NO spectrum was recorded, the usefulness of the NO spectrum for determination of free-stream rotational temperature was demonstrated and should be exploited in future experiments. Indeed, based on the strong NO signals, it is recommended that lower resolution NO spectra be obtained to provide a measure of NO vibrational temperature in the same manner that the N2 temperature was obtained.

Price, Linwood L.↗

A non-intrusive optical (NIO) approach to characterize heliostats in utility-scale power tower plants: Sensitivity study

Power towers, a type of concentrating power tower technology, use a large number of heliostats to concentrate sunlight and produce renewable energy. Optical errors of heliostats can cause drastic losses in the efficiency of power-tower plants. Accurately measuring optical errors is crucial to assessing and improving plant performance. This analysis discusses an innovate non-intrusive optical (NIO) approach to measure slope, canting, and tracking errors by detecting distortions in the reflected tower structure in heliostat images. Further in this work a sensitivity study is carefully conducted to determine the uncertainty requirements to allow the method to calculate slope errors with an accuracy of 0.25 mrad. Measurement uncertainty sources include camera resolution and position uncertainty, tower position uncertainty, and number of collected images. Each uncertainty source is investigated to determine its impact on the accuracy of the slope-error calculation. A combination of theoretical results and experimental results obtained from data collected on a heliostat at Sandia National Laboratories is used to determine and validate uncertainty requirements. The analysis shows that a measurement uncertainty of 0.25 mrad can be realized by realistically controlling uncertainty sources when implementing the NIO method. It demonstrates the superior performance of NIO in performing in-situ optical characterization.

14 SOLAR ENERGY↗

Pressure-Driven Fiber-Optic Sensor for Online Corrosion Monitoring

For many industrial applications, corrosion is a life-limiting phenomenon and therefore requires careful consideration and rigorous experimental testing before structural materials can be reliably deployed, particularly in harsh chemical environments. The traditional approach to measuring corrosion requires exposing many samples to the intended environment and then extracting them individually at discrete intervals for postexposure characterization. This approach does not provide a high degree of temporal resolution, nor does it provide any real-time information regarding dynamic changes in corrosion rates. Additionally, developing an online corrosion monitor capable of surviving harsh chemical environments could provide valuable information regarding the structural health of components and changing process conditions that could accelerate corrosion. To this end, a corrosion sensor was developed based on a pressure-driven Fabry-Pérot cavity (FPC). This sensor uses a pressure control system to internally pressurize the FPC formed between the sensor’s housing and a metal-embedded singlemode optical fiber. Simultaneous measurement of the change in FPC length using low-coherence interferometry and the applied pressure enables the calculation of the relative changes in the sensor’s diaphragm thickness due to corrosion on its outer surface. Measurements were made in situ while actively corroding the sensor and were validated against surveillance specimens that were corroded simultaneously. The uncertainties in the measured corrosion were analyzed using error propagation of the uncertainties in the measured pressures and displacements and were found to be <1% of the initial diaphragm thickness.

42 ENGINEERING↗

Heat capacity of microgram oxide samples by fast scanning calorimetry

Quantitative scanning calorimetry on microgram-sized samples opens a broad, new range of opportunities for studying the thermodynamic properties of quantity-limited materials, including those produced under extreme conditions or found as rare accessory minerals in nature. We calibrated the Mettler Toledo Flash DSC 2+ calorimeter to obtain quantitative heat capacities in the range 200–350 °C, using samples weighing between 2 and 11.5 μg. Our technique is applied to a new set of oxide materials to which it has never been used before, without the need for melting, glass transitions, or phase transformations. Heat capacity data were obtained for silica in the high pressure stishovite (rutile) structure, dense post-stishovite glass, standard fused quartz, and for TiO2 rutile. These heat capacities agree within 5%–15% with the literature values reported for rutile, stishovite, and fused SiO2 glass. The heat capacity of post-stishovite glass, made by heating stishovite to 1000 °C, is a newly reported value. After accurate calibrations, measured heat capacities were then used to calculate masses for samples in the microgram range, a substantial improvement over measurement in conventional microbalances, which have uncertainties approaching 50%–100% for such small samples. Since the typical uncertainty of heat capacities measured on 10–100 mg samples in conventional differential scanning calorimetry is typically 7% (1%–5% with careful work), flash differential scanning calorimetry, using samples a factor of 1000 smaller, increases the uncertainty of heat capacity measurements by a factor of <3, opening the door for meaningful measurements on ultra-small, high-pressure samples and other quantity-limited materials.

Instruments & Instrumentation↗

Effective UV radiation from model calculations and measurements

Model calculations have been made to simulate the effect of atmospheric ozone and geographical as well as meteorological parameters on solar UV radiation reaching the ground. Total ozone values as measured by Dobson spectrophotometer and Brewer spectrometer as well as turbidity were used as input to the model calculation. The performance of the model was tested by spectroradiometric measurements of solar global UV radiation at Potsdam. There are small differences that can be explained by the uncertainty of the measurements, by the uncertainty of input data to the model and by the uncertainty of the radiative transfer algorithms of the model itself. Some effects of solar radiation to the biosphere and to air chemistry are discussed. Model calculations and spectroradiometric measurements can be used to study variations of the effective radiation in space in space time. The comparability of action spectra and their uncertainties are also addressed.

Feister, Uwe↗

Stastically determined experimental uncertainties in photon Doppler velocimetry (PDV) measurements

Shock-ramp experiments place high demands on the precision, accuracy, and temporal resolution of transformed velocimetry signals. To minimize uncertainty after total propagation of a shockramp experiment, ideally multiple PDV traces are used. However, each trace has some uncertainty that is a function of the PDV system and analysis of the velocimetry data. In order to determine a reasonable experimental estimate of minimum uncertainty, we calculate observed uncertainties in as-fielded PDV systems using multiple channels to sample the velocity on each shot. We also calculate the uncertainty’s sensitivity to choice of analysis methods.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

An intercomparison of aircraft instrumentation for tropospheric measurements of sulfur dioxide

As part of the NASA Tropospheric Chemistry Program, a series of field intercomparisons have been conducted to evaluate the state-of-the art for measuring key tropospheric species. One of the objectives of the third intercomparison campaign in this series, Chemical Instrumentation Test and Evaluation 3 (CITE 3), was to evaluate instrumentation for making reliable tropospheric aircraft measurements of sulfur dioxide, dimethyl sulfide, hydrogen sulfide, carbon disulfide, and carbonyl sulfide. This paper reports the results of the intercomparisons of five sulfur dioxide measurement methods ranging from filter techniques, in which samples collected in flight are returned to the laboratory for analyses (chemiluminescent or ion chromatographic), to near real-time, in-flight measurements via gas chromatographic, mass spectrometric, and chemiluminescent techniques. All techniques showed some tendency to track sizeable changes in ambient SO2 such as those associated with altitude changes. For SO2 mixing ratios in the range of 200 pptv to a few ppbv, agreement among the techniques varies from about 30% to several orders of magnitude, depending upon the pair of measurements intercompared. For SO2 mixing ratios less than 200 pptv, measurements from the techniques are uncorrelated. In general, observed differences in the measurement of standards do not account for the flight results. The CITE 3 results do not unambiguously identify one or more of the measurement techniques as providing valid or invalid SO2 measurements, but identify the range of 'potential' uncertainty in SO2 measurements reported by currently available instrumentation and as measured under realistic aircraft environments.

Gregory, Gerald L.↗

Velocity Measurements in the Wake of the Swept Wing Flow Test Model at the National Transonic Facility

Femtosecond laser electronic excitation tagging (FLEET) was applied to obtain flowfield velocity data for the Swept Wing Flow Test (SWiFT) at the NASA Langley Research Center National Transonic Facility (NTF). Despite numerous challenges associated with performing flow velocimetry measurements within a large-scale cryogenic wind tunnel facility, the experimental campaign was conducted under various conditions, including dry air at 320 K, cool nitrogen at 240 K, and Mach numbers of 0.2 and 0.8. FLEET velocimetry measurements were performed in the downstream wake of the SWiFT model, providing a quantitative dataset. This dataset includes one-dimensional velocity profiles and two-dimensional velocity maps acquired at different angles of attack and Reynolds numbers. The two-dimensional single component velocity maps indicate relatively uniform flow across the 120-mm wide wake flow survey suggesting that the main flow features can be represented by single-position linear velocity profiles. The measured instantaneous velocity profiles at variable angles of attack are compared to model lift coefficient information obtained at Mach 0.2. At high Reynolds numbers, a sudden velocity decrease was observed in the FLEET measurements at the same time as stall in lift coefficient was observed. At a low Reynolds number, both the velocity profiles and the lift coefficient show a smoother transition, without a sudden stall. Furthermore, the two-dimensional, one component velocity map reveals a velocity deficit region at Mach 0.8 at various angles of attack. Both single shot and mean velocity measurements were acquired allowing assessment of flowfield fluctuations and measurement precisions. The uncertainties are within 4 m/s in mean measurements based on repeatability data and about 5 m/s in instantaneous single-shot measurements. Measurements are reported with ~4.8 mm spatial resolution with 32-pixel averaging used to reduce measurement errors.

femtosecond↗

Velocity Measurements in the Wake of the Swept Wing Flow Test (SWIFT) Model at the National Transonic Facility

Femtosecond laser electronic excitation tagging (FLEET) was applied to obtain flowfield velocity data for the Swept Wing Flow Test (SWiFT) at the NASA Langley Research Center National Transonic Facility (NTF). Despite numerous challenges associated with performing flow velocimetry measurements within a large-scale cryogenic wind tunnel facility, the experimental campaign was conducted under various conditions, including dry air at 320 K, cool nitrogen at 240 K, and Mach numbers of 0.2 and 0.8. FLEET velocimetry measurements were performed in the downstream wake of the SWiFT model, providing a quantitative dataset. This dataset includes one-dimensional velocity profiles and two-dimensional velocity maps acquired at different angles of attack and Reynolds numbers. The two-dimensional single component velocity maps indicate relatively uniform flow across the 120-mm wide wake flow survey suggesting that the main flow features can be represented by single-position linear velocity profiles. The measured instantaneous velocity profiles at variable angles of attack are compared to model lift coefficient information obtained at Mach 0.2. At high Reynolds numbers, a sudden velocity decrease was observed in the FLEET measurements at the same time as stall in lift coefficient was observed. At a low Reynolds number, both the velocity profiles and the lift coefficient show a smoother transition, without a sudden stall. Furthermore, the two-dimensional, one component velocity map reveals a velocity deficit region at Mach 0.8 at various angles of attack. Both single shot and mean velocity measurements were acquired allowing assessment of flowfield fluctuations and measurement precisions. The uncertainties are within 4 m/s in mean measurements based on repeatability data and about 5 m/s in instantaneous single-shot measurements. Measurements are reported with ~4.8 mm spatial resolution with 32-pixel averaging used to reduce measurement errors.

Transonic↗

Impact of Interaction Uncertainties on Neutrino-Nucleus Cross Section Measurements

Accelerator-based neutrino facilities represent forefront scientific endeavors, employing state-of-the-art techniques to investigate the properties of neutrinos and unveil signals of physics beyond the standard model. Neutrino-nucleus interactions constitute one of the biggest systematics in these experiments. As neutrino-nucleus cross section measurement statistics have started to surge in recent years, it's becoming vital to control systematics in these measurements. This presentation explores the pivotal role of neutrino interaction uncertainties, including nuclear effects and modeling approximations, in achieving precise neutrino cross-section measurements.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

HZETRN Radiation Transport Validation Using Balloon-Based Experimental Data

The deterministic radiation transport code HZETRN (High charge (Z) and Energy TRaNsport) was developed by NASA to study the effects of cosmic radiation on astronauts and instrumentation shielded by various materials. This work presents an analysis of computed differential flux from HZETRN compared with measurement data from three balloon-based experiments over a range of atmospheric depths, particle types, and energies. Model uncertainties were quantified using an interval-based validation metric that takes into account measurement uncertainty both in the flux and the energy at which it was measured. Average uncertainty metrics were computed for the entire dataset as well as subsets of the measurements (by experiment, particle type, energy, etc.) to reveal any specific trends of systematic over- or under-prediction by HZETRN. The distribution of individual model uncertainties was also investigated to study the range and dispersion of errors beyond just single scalar and interval metrics. The differential fluxes from HZETRN were generally well-correlated with balloon-based measurements; the median relative model difference across the entire dataset was determined to be 30%. The distribution of model uncertainties, however, revealed that the range of errors was relatively broad, with approximately 30% of the uncertainties exceeding ± 40%. The distribution also indicated that HZETRN systematically under-predicts the measurement dataset as a whole, with approximately 80% of the relative uncertainties having negative values. Instances of systematic bias for subsets of the data were also observed, including a significant underestimation of alpha particles and protons for energies below 2.5 GeV/u. Muons were found to be systematically over-predicted at atmospheric depths deeper than 50 g/cm(sup 2) but under-predicted for shallower depths. Furthermore, a systematic under-prediction of alpha particles and protons was observed below the geomagnetic cutoff, suggesting that improvements to the light ion production cross sections in HZETRN should be investigated.

James E Warner↗

High precision 5 MeV Mott polarimeter

We report on the design and performance of a Mott polarimeter optimized for a nominal 5-MeV electron beam from the Continuous Electron Beam Accelerator Facility (CEBAF) injector. The rf time structure of this beam allows the use of time of flight in the scattered electron detection, making it possible to cleanly isolate those detected electrons that originate from the scattering foil, and resulting in measured scattering asymmetries which are exceptionally stable over a broad range of beam conditions, beam currents, and foil thicknesses. In two separate series of measurements from two different photocathode electron sources, we have measured the Mott scattering asymmetries produced by an approximately 86% transversely polarized electron beam incident on ten gold foils with nominal thicknesses between 50 and 1000 nm. The statistical uncertainty of the measured asymmetry from each foil is below 0.25%. Within this statistical precision, the measured asymmetry was unaffected by ±1-mm shifts in the beam position on the target foil, and by beam current changes and dead-time effects over a wide range of beam currents. The overall uncertainty of our beam polarization measurement, arising from the uncertainty in the value of the scattering asymmetry at zero foil thickness as determined from our fits to the measured asymmetries versus scattering foil thicknesses, the estimated systematic effects, and the (dominant) uncertainty from the calculation of the theoretical Sherman function, is 0.61%. A simulation of the polarimeter using geant4 has confirmed that double scattering in the target foil is the sole source of the dependence of the measured asymmetry on foil thickness, and gives a result for the asymmetry versus foil thickness in good agreement with both our measurements and a simple calculation. Future measurements at different beam energies and with target foils of different atomic numbers will seek to bound uncertainties from small effects such as radiative corrections to the calculation of the polarimeter analyzing power. A simultaneous high-precision measurement of the beam polarization with a different polarimeter, AESOP (Accurate Electron Spin Optical Polarimeter), under development at the University of Nebraska, clearly possible at the CEBAF accelerator, will allow a high-precision comparison of our measured asymmetries with theoretical calculations of the Mott analyzing power. Finally, the improved precision of the current Mott polarimeter along with similar improvements to other Jefferson Lab polarimeters warrants another precision comparison of all of these polarimeters when measuring a beam of the same polarization.

Grames, J. M. (ORCID:0000000193908752)↗

Water-vapor absorption line measurements in the 940-nm band by using a Raman-shifted dye laser

We report water-vapor absorption line measurements that are made by using the first Stokes radiation (930-982 nm) with HWHM 0.015/cm generated by a narrow-linewidth, tunable dye laser. Forty-five absorption line strengths are measured with an uncertainty of 6 percent and among them are fourteen strong lines that are compared with previous measurements for the assessment of spectral purity of the light source. Thirty air-broadened linewidths are measured with 8 percent uncertainty at ambient atmospheric pressure with an average of 0.101/cm. The lines are selected for the purpose of temperature-sensitive or temperature-insensitive lidar measurements. Results for these line strengths and linewidths are corrected for broadband radiation and finite laser linewidth broadening effects and compared with the high-resolution transmission molecular absorption.

Chu, Zhiping↗

Understanding Type Ia Supernova Distance Biases by Simulating Spectral Variations

In the next decade, transient searches from the Vera C. Rubin Observatory and the Nancy Grace Roman Space Telescope will increase the sample of known Type Ia supernovae (SNe Ia) from ~10 3 to 10 5 . With this reduction of statistical uncertainties on cosmological measurements, new methods are needed to reduce systematic uncertainties. Here, characterizing the underlying spectroscopic evolution of SN Ia remains a major systematic uncertainty in current cosmological analyses, motivating a new simulation tool for the next era of SN Ia cosmology: Build Your Own Spectral Energy Distribution (byosed). byosed is used within the SNANA framework to simulate light curves by applying spectral variations to model SEDs, enabling flexible testing of possible systematic shifts in SN Ia distance measurements. We test the framework by comparing a nominal Roman SN Ia survey simulation using a baseline SED model to simulations using SEDs perturbed with byosed, and investigating the impact of ignoring specific SED features in the analysis. These features include semiempirical models of two possible, predicted relationships: between SN ejecta velocity and light-curve observables, and a redshift-dependent relationship between SN Hubble residuals and host-galaxy mass. We analyze each byosed simulation using the SALT2 and BEAMS with Bias Corrections framework, and estimate changes in the measured value of the dark-energy equation-of-state parameter, w. We find a difference of Δw = –0.023 for SN velocity and Δw = 0.021 for redshift-evolving host mass when compared to simulations without these features. By using byosed for SN Ia cosmology simulations, future analyses (e.g., the Rubin and Roman SN Ia samples) will have greater flexibility to constrain or reduce such SN Ia modeling uncertainties.

79 ASTRONOMY AND ASTROPHYSICS↗

Uncertainties in Predicting Rice Yield by Current Crop Models Under a Wide Range of Climatic Conditions

Predicting rice (Oryza sativa) productivity under future climates is important for global food security. Ecophysiological crop models in combination with climate model outputs are commonly used in yield prediction, but uncertainties associated with crop models remain largely unquantified. We evaluated 13 rice models against multi-year experimental yield data at four sites with diverse climatic conditions in Asia and examined whether different modeling approaches on major physiological processes attribute to the uncertainties of prediction to field measured yields and to the uncertainties of sensitivity to changes in temperature and CO2 concentration [CO2]. We also examined whether a use of an ensemble of crop models can reduce the uncertainties. Individual models did not consistently reproduce both experimental and regional yields well, and uncertainty was larger at the warmest and coolest sites. The variation in yield projections was larger among crop models than variation resulting from 16 global climate model-based scenarios. However, the mean of predictions of all crop models reproduced experimental data, with an uncertainty of less than 10 percent of measured yields. Using an ensemble of eight models calibrated only for phenology or five models calibrated in detail resulted in the uncertainty equivalent to that of the measured yield in well-controlled agronomic field experiments. Sensitivity analysis indicates the necessity to improve the accuracy in predicting both biomass and harvest index in response to increasing [CO2] and temperature.

crop-model ensembles↗

Experiments at Sandia to Measure the Effect of Temperature on Critical Systems

Estimation of the uncertainty in a critical experiment attributable to uncertainties in the measured experiment temperature is done by calculating the variation of the eigenvalue of a benchmark configuration as a function of temperature. In the low-enriched water-moderated critical experiments performed at Sandia, this is done by 1) estimating the effects of changing the water temperature while holding the UO 2 fuel temperature constant, 2) estimating the effects of changing the UO 2 temperature while holding the water temperature constant, and 3) combining the two results. This assumes that the two effects are separable. The results of such an analysis are nonintuitive and need experimental verification. Critical experiments are being planned at Sandia National Laboratories (Sandia) to measure the effect of temperature on critical systems and will serve to test the methods used in estimating the temperature effects in critical experiments.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

Improving air leakage prediction of buildings using the fan pressurization method with the Weighted Line of Organic Correlation

In many countries, the fan pressurization method is the most frequently chosen approach for measuring the air leakage of houses. The measurements are usually performed at pressures that far exceed pressures to which buildings are exposed to under normal conditions. A fit of these tests to the power-law formulation allows an extrapolation to data points outside the measured pressure range. With the Ordinary Least Square (OLS) fitting method, the pressure exponent and flow coefficient can be determined. However, the measurement results are highly sensitive to uncertainties induced by external factors like changing wind conditions during the tests, which is neglected by OLS. This may lead to errors in the prediction of flows at lower pressures. The Weighted Line of Organic Correlation (WLOC) is an alternative approach and takes measurement uncertainty into account. In this paper, a statistical analysis of an extensive data set of pressurization measurements has been performed. Both regression techniques have been compared for almost 7500 fan pressurization measurements of six houses in 109 different house leak configurations. The variability in predicting pressure exponent and flow coefficient for both WLOC and OLS regression was analyzed using probability density functions. It was found that the Weighted Line of Organic Correlation significantly decreases the uncertainty in predicting pressure exponent, flow coefficient, and other low-pressure air leakage metrics compared to the Ordinary Least Square fitting. Here, the authors highly recommend the implementation of WLOC in current measurement standards and test equipment.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗