Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “laboratories”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 757 records · Page 42

Wetland Delineation Report for Middle Mortandad Mesa Adjacent to Technical Area 55 at Los Alamos National Laboratory

This report provides the results of a wetland delineation conducted to support operational logistics for construction of a high-pressure water line that is planned to occur near a wetland at Los Alamos National Laboratory (LANL). The wetland reach is on the mesa edge in Technical Area (TA)-55 above the Mortandad Canyon watershed. This area has not been previously delineated; however, it drains to a canyon bottom where LANL updated a delineation in 2017 for the wetland adjacent to Technical Areas (TAs) 25, 48, and 55.

54 ENVIRONMENTAL SCIENCES↗

An Overview of Argonne’s Advanced Mobility Technology Laboratory Vehicle Systems Instrumentation and Evaluation Methodology

This report will provide a general overview of the testing facilities, research equipment, and general testing methodologies Argonne utilizes to conduct vehicle technology evaluations of advanced technology research vehicles. Data is captured from vehicle evaluations that provide powertrain operation and corresponding energy consumption based on a combination of in-depth instrumentation and focused testing. This resulting dataset of hundreds of time-resolved vehicle signals provide a basis for direct analysis and model validation of vehicle specific technologies. Argonne has attempted to standardize the approach to vehicle instrumentation and testing at Argonne, but it should be noted that each vehicle, and the corresponding assessment, remains unique. It is suggested that the reader reference vehicle specific testing reports for an overview of the unique aspects for each test vehicle. Additionally, the datasets for research vehicles are made publicly available through the Advanced Mobility Technology Laboratory’s Downloadable Driving Database (D3) at www.anl.gov/d3.

33 ADVANCED PROPULSION SYSTEMS↗

Argonne National Laboratory Site Environmental Report (CY2020)

This report discusses the status and the accomplishments of the environmental protection program at Argonne National Laboratory for calendar year 2020. The status of Argonne environmental protection activities with respect to compliance with the various laws and regulations is discussed, along with environmental management, sustainability efforts, environmental corrective actions, and habitat restoration. To evaluate the effects of Argonne operations on the environment, samples of environmental media collected on the site, at the site boundary, and off the Argonne site were analyzed and compared with applicable guidelines and standards. A variety of radionuclides were measured in air, surface water, groundwater, and bottom sediment samples. In addition, chemical constituents in surface water, groundwater, and wastewater were analyzed. External penetrating radiation doses were measured, and the potential for radiation exposure to off site population groups was estimated. Results are interpreted with respect to the origin of the radioactive and chemical substances (i.e., natural, Argonne, and other) and are compared with applicable standards intended to protect human health and the environment. A U.S. Department of Energy (DOE) dose calculation methodology, based on International Commission on Radiological Protection (ICRP) recommendations and the U.S. Environmental Protection Agency’s (EPA) CAP 88 Version 4.1 computer code, was used in preparing this report.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Bat Survey for the Lawrence Livermore National Laboratory Experimental Test Site 300

Pursuant to Subcontract Number B644180 between ECORP Consulting, Inc. (ECORP) and Lawrence Livermore National Security, LLC. at Lawrence Livermore National Laboratory (LLNL), ECORP conducted focused bat surveys at LLNL’s Experimental Test Site (Site 300) during the spring of 2021. The surveys targeted two focal species including the Western red bat (Lasiurus blossevillii) and pallid bat (Antrozous pallidus) on the approximately 6,800-acre Site 300 in Alameda and San Joaquin Counties. The results of these surveys will provide supporting information for a Site-Wide Environmental Impact Statement.

54 ENVIRONMENTAL SCIENCES↗

Carnivore Survey Results for the Lawrence Livermore National Laboratory Site 300

ECORP Consulting, Inc. conducted a suite of carnivore surveys at the Lawrence Livermore National Laboratory’s (LLNL) Experimental Test Site (Site 300; project site). The project site is located east of the City of Livermore and southwest of the City of Tracy, Alameda and San Joaquin Counties, California. Mesocarnivore surveys were conducted on the project site in 2002 in preparation for the 2005 LLNL Site-Wide Environmental Impact Statement (SWEIS; Clark et al. 2003). The 2002 surveys included a combination of spotlighting, camera stations, and scat detection dog surveys. Additional scat detection dog surveys for San Joaquin kit fox (Vulpes macrotis mutica) were performed on Site 300 and the adjacent California Department of Fish and Wildlife’s (CDFW) Corral Hollow Ecological Reserve in 2018 and 2020 (Woollett 2019, 2021). A variety of species, including American badger (Taxidea taxus), coyote (Canis latrans), and bobcat (Lynx rufus), were detected during the previous surveys; however, no San Joaquin kit fox or mountain lion (Puma concolor) were detected. In support of the preparation of the new SWEIS, ECORP performed carnivore surveys to document the carnivores and other animals present on Site 300, with a focus on determining if the federally listed (endangered) and state listed (threatened) San Joaquin kit fox, CDFW Species of Special Concern (SSC) American badger, and/or mountain lion are present on Site 300. American badgers are known to occur on the property and there have been a few sporadic sightings of mountain lions, but San Joaquin kit fox have not been documented on Site 300. Although mountain lion were not detected during the 2002 survey, it has been added as a focal species for this survey because the southern and central coast evolutionary significant units of mountain lions were recently advanced by CDFW as a Candidate species for listing as “threatened” under the California Endangered Species Act.

54 ENVIRONMENTAL SCIENCES↗

Passerine Bird Surveys for the Lawrence Livermore National Laboratory Site 200

Pursuant to Subcontract Number B644180 between ECORP Consulting, Inc. (ECORP) and Lawrence Livermore National Security, LLC. (LLNS) at Lawrence Livermore National Laboratory (LLNL), ECORP conducted passerine bird and waterfowl surveys at LLNL Livermore Site 200 (Site 200) during the spring and summer of 2021. While the point-count surveys were considered passerine and waterfowl surveys, other non-passerine species (e.g. raptors, doves, woodpeckers, hummingbirds) were surveyed for as well. LLNL conducts annual monitoring for nesting raptors at the Livermore Site 200. Because of this, raptors were not included as target species in this scope of work. The purpose of the surveys was to document the presence and abundance of all avian species in support of a Site-wide Environmental Impact Statement. Particular focus of the survey was on special status bird species.

54 ENVIRONMENTAL SCIENCES↗

Avian Surveys Report for the Lawrence Livermore National Laboratory Arroyo Mocho Pumping Station

Pursuant to Subcontract Number B644180 between ECORP Consulting, Inc. and Lawrence Livermore National Security, LLC. at Lawrence Livermore National Laboratory (LLNL), ECORP conducted passerine bird and raptor surveys at the Arroyo Mocho pumping station site during the spring and summer of 2021. While the point-count survey was considered a passerine survey, other non-passerine species (e.g. doves, woodpeckers, hummingbirds) were surveyed for as well. The purpose of the surveys was to document the presence and abundance of all avian species within the survey area in support of a Site-wide Environmental Impact Statement. Particular focus of the survey was on special status bird species.

54 ENVIRONMENTAL SCIENCES↗

Final Reports of the 2021 Los Alamos National Laboratory Computational Physics Student Summer Workshop

Since 2011, the Los Alamos National Laboratory Computational Physics Student Summer Workshop has been bringing together a highly talented and diverse group of students every summer. Students work in teams of two, alongside typically two mentors, on research projects reflecting a broad range of topics within computational physics. In addition, students attend a series of lectures on topics within computational physics, facility tours, and networking events. The program lasts ten weeks, with this year’s workshop running from June 7 to August 13. At the end of the summer, students give a final presentation, along with a written report. Those reports are what make up the remaining sections of this document. Admission to the workshop is by a competitive process, with the mentors forming the selection committee. One of the important accomplishments of the workshop has been to create a student pipeline from diverse schools that sometimes are not normally tapped by LANL recruiting. Many workshop students maintain a continuing relationship with LANL, returning as student interns, post-doctoral researchers, and staff members. Additionally, workshop alumni act as ambassadors for LANL. The result is a wider awareness both of LANL as a potential employer, and of the technical work that happens at LANL. This year, the workshop was once again in an off-site, virtual format. Students worked on LANL virtual desktop systems remotely, also accessing LANL HPC resources. In order to facilitate communication, student were given accounts on both Webex, a video teleconferencing platform, and Mattermost, an online team collaboration and chat platform, similar to Slack. Daily communication between students and mentors was primarily on Mattermost, with Webex conferencing as needed. The lectures were all done on Webex. Given the difficulty of the virtual format, and a concern that students might have video teleconferencing burn-out, all lectures were optional this year. In spite of this, the attendance was generally high. Lecturers were asked to try to move to a more high-level, ”What is it?,” format. Once again, the students did a tremendous job. Over the course of ten weeks, they did important research across a staggering array of disciplines. The following pages contain the final report for each team’s research efforts. Enjoy!

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗

Site Environmental Report for 2020, Sandia National Laboratories, California

Sandia National Laboratories, California (SNL/CA) is a Department of Energy (DOE) facility. The management and operations of the facility are under a contract with the DOE's National Nuclear Security Administration (NNSA). On May 1, 2017, the name of the management and operating contractor changed from Sandia Corporation to National Technology & Engineering Solutions of Sandia, LLC (NTESS). The DOE, NNSA, Sandia Field Office administers the contract and oversees contractor operations at the site. DOE and its management and operating contractor for Sandia are committed to safeguarding environmental protection, compliance, and sustainability and to ensuring the validity and accuracy of the monitoring data presented in this Annual Site Environmental Report. This Site Environmental Report for 2020 was prepared in accordance with DOE Order 231.1B, Environment, Safety and Health Reporting (DOE 2012). The report provides a summary of environmental monitoring information and compliance activities that occurred at SNL/CA during calendar year 2020, unless noted otherwise. General site and environmental program information is also included.

54 ENVIRONMENTAL SCIENCES↗

Pacific Northwest National Laboratory Annual Site Environmental Report for Calendar Year 2020. Final Report

The U.S. Department of Energy requires that all its site facilities develop an annual site environmental report to comply with DOE Order 231.1B, Chg 1, and DOE Order 458.1, Admin Chg 4. This report provides a synopsis of calendar year 2020 information related to environmental management performance and compliance efforts at Pacific Northwest National Laboratory. It summarizes site compliance with federal, state, and local environmental laws, regulations, policies, directives, permits, and Orders, and provides environmental management performance benchmarks and their status to the public, regulatory agencies, community officials, Native American tribes, and public interest groups.

54 ENVIRONMENTAL SCIENCES↗

Accelerated Aging of Fast Pyrolysis Bio-Oil Using Carbonyl Titration: Laboratory Analytical Procedure (LAP)

This laboratory analytical procedure covers the accelerated aging of fast pyrolysis bio-oils. Bio-oils undergo reactions that result in physical and chemical changes over time. These changes typically result in an increase in molecular weight, decrease in some functional groups such as carbonyls, and an increase in viscosity; additionally, the aging process often leads to phase separation. Studies have shown that accelerated aging of bio-oils using this method closely mimics room temperature aging for long periods of time (over 3 years). This procedure has been developed for the accelerated aging of fast pyrolysis bio-oils only. Fast pyrolysis bio-oils are more reactive than other bio-oils (e.g., catalytic fast pyrolysis) and undergo aging much more rapidly. Therefore, this procedure should only be used for fast pyrolysis bio-oil samples.

09 BIOMASS FUELS↗

Determination of Carbon, Hydrogen, Nitrogen, and Oxygen in Bio-Oils: Laboratory Analytical Procedure (LAP)

The determination of total carbon, hydrogen, and nitrogen in bio-oils is important as these values can be used to track the carbon balance of production processes as well as calculate total oxygen content by difference. Oxygen content of bio-oils is a key metric for production and upgrading strategies as these are typically aimed at reducing oxygen. Oxygenates in bio-oils contribute to poor hydrocarbon miscibility, high acidity, high viscosity, and poor stability. Upgrading of bio-oils via deoxygenation produces hydrocarbons which can be used to generate feedstocks for renewable fuels and chemicals. In this Laboratory Analytical Procedure (LAP), combustion-based ultimate analysis is used to determine the weight percent (wt%) of C, H, and N in bio-oils and upgraded products. Ultimate analysis uses high temperatures and a pure oxygen environment to completely combust organic samples to carbon dioxide (CO 2 ), water (H 2 O), and nitrogen oxides (NO x ). In this procedure the amount of C and H in the sample are quantified by measuring resultant CO 2 and H 2 O with Fourier-transform infrared spectroscopy (FTIR). For N, NO x is reduced to nitrogen (N 2 ) which is measured with a thermal conductivity detector (TCD), providing total N content.

09 BIOMASS FUELS↗

Determination of Water Content in Bio-Oils by Volumetric Karl Fischer Titration: Laboratory Analytical Procedure (LAP)

The water content of bio-oils is a key metric for several reasons. Water is typically the most concentrated single component of fast pyrolysis oils, though this will be much lower in catalytic fast pyrolysis and upgraded products. Reduced water content is preferable in bio-oil as water can contribute to phase separation, corrosivity, and instability. Additionally, lower water is beneficial for physical properties such as energy density. The percentage of water can also be used to correct the calculation for organic oxygen when determining total oxygen content of bio-oils via combustion-based ultimate analysis. The procedure described here is specifically written for the analysis of bio-oils, and is based on ASTM E203, Standard Test Method for Water Using Volumetric Karl Fischer Titration. This standard test method is specified for measuring the mass % water in pyrolysis liquid biofuels in ASTM D7544, Standard Specification for Pyrolysis Liquid Biofuel. Although the standard method is prescribed for the analysis of pyrolysis liquids for use in industrial and commercial burners, the method is not specifically written for this product. The method described with this Laboratory Analytical Procedure (LAP) provides specific guidance for the analysis of bio-oils. Both organic and aqueous phases can be measured with this technique.

09 BIOMASS FUELS↗

Determination of Carbon Functional Groups in Pyrolysis Bio-Oils using 13 C NMR: Laboratory Analytical Procedure (LAP)

Pyrolysis is a process that can be used to convert biomass to solid, liquid and gaseous products for use as renewable chemicals and fuels. The liquid fraction, known as “bio-oil” is complex and challenging to characterize, particularly by means of GC/MS, GPC, LC and FT-IR. NMR is capable of analyzing whole bio-oil samples and can provide quantitative results to characterize different functional groups or types of carbon present in bio-oil. This Laboratory Analytical Procedure (LAP) quantifies different carbon functional groups in whole bio-oil samples. This information can be used for comparisons between different pyrolysis experimental conditions or different upgrading processes and catalysts, and also allow for comparisons between bio-oils produced at different facilities.

09 BIOMASS FUELS↗

Natural Resource Management Plan for Brookhaven National Laboratory

The purpose of the Natural Resource Management Plan (NRMP) is to provide management guidance, promote stewardship of the natural resources found at BNL, and to sustainably integrate their protection with pursuit of the Laboratory’s mission. The philosophy or guiding principles of the NRMP include stewardship, sustainability, adaptive ecosystem management, compliance, integration with other plans and requirements, and the incorporation of community involvement, where applicable. The NRMP is reviewed and updated every five years. The body of this plan establishes the management goals and actions necessary for managing the natural resources at BNL in a sustainable manner. The appendices provide specific management requirements for threatened and endangered species documented on site (Appendices A, B and C).

54 ENVIRONMENTAL SCIENCES↗

Triad ST&E Committee Meeting - Laboratory Update [Slides]

My ultimate responsibility is to make sure the people of this Laboratory are safe. Impacts of the mandate are manageable and not a significant deviation from historical attrition. We will be communicating with employees on vacation/LWOP about important dates and the criteria for returning to work.

99 GENERAL AND MISCELLANEOUS↗

Engineering Space Mission Support at Los Alamos National Laboratory [Slides]

This talk focuses on engineering space mission support at Los Alamos National Laboratory (LANL). In many cases, LANL is one of many participants on a particular space mission. There are many other space activities at institutions and government agencies worldwide, some of which are closely related to the ones describe in this talk.

42 ENGINEERING↗

Laboratory Evaluation to Increase Effectiveness of Field-Scale Soil Flushing in the Hanford 100 Areas

This laboratory study was initiated to develop an improved technical understanding of the key controlling geochemical and physical processes of mobilizing residual Cr(VI) in Hanford sediments to provide increased effectiveness in soil flushing activities planned for Hanford 100 Areas. This was accomplished by (1) quantifying Cr mass, release rate, and surface phase changes as Cr is leached from different Hanford sediments; (2) maximizing Cr leaching during soil flushing by evaluating different leach solutions and leach strategies; and (3) minimizing leaching of remaining residual Cr after soil flushing ends. To quantify geochemical controls on Cr leaching from sediments, sequential liquid extractions were used to identify aqueous, adsorbed, and solid Cr surface phases (precipitates or Cr incorporated into other phases) before and after water-saturated and unsaturated leach experiments with pH 8 artificial groundwater and with other amendment solutions. Changes in the Cr release rate from sediments were also correlated to changes in Cr surface phases. During unsaturated infiltration, water advection occurs primarily through larger pores, with less movement through smaller grain layers leading to a slower release of Cr trapped in smaller pores next to smaller grains. To quantify these physical controls on Cr leaching from sediments, 10 ft high 1-D infiltration experiments were conducted at differing leach solution application rates, and Cr leaching during application and subsequent residual water flow was quantified. Qualitative 2-D experiments were also conducted to evaluate surfactant addition to increase flow in low-permeability zones. Cr-contaminated Hanford sediments from the 100-H, 100-K, 100-D, and 200 East Areas exhibited a wide variety of leach behavior from rapid release of a small amount of Cr to fast (i.e., minutes) and slow (i.e., hours or more) release of high Cr. Sediments with low labile Cr (< 0.2 µg/g) exhibited fast Cr release but less overall release, and most (>95%) leached from the sediments within a few pore volumes in water-saturated columns. With nearly no sorption of chromate, aqueous and sorbed Cr (as chromate) were released quickly from sediment within the first few pore volumes, resulting in high leach concentrations, fast initial Cr release rates, and changes in pre- and post-leach extractions. In contrast, sediments with high labile Cr (0.2 to 20 µg/g) exhibited a combination of fast and slow Cr release due to multiple Cr surface phases contributing to Cr release from the sediment at different rates with greater overall release. This resulted in elevated Cr effluent concentrations even after dozens of pore volumes were leached. In addition, the Cr release rate decreased with increasing time during leaching. A decrease in labile Cr (aqueous Cr, adsorbed Cr, pH 5 acetate dissolved precipitates) in post-leach extractions compared to pre-leach extractions showed initial aqueous and adsorbed Cr release, followed by dissolution of high-solubility precipitates such as CaCrO 4 (if present), then slow dissolution of calcite that may contain some chromate and possibly BaCrO 4 . The labile Cr in all sediments correlated well with the Cr release rate (r 2 = 0.81). Labile Cr also correlated well with the leached mass in water-saturated columns (r 2 = 0.98), and therefore can be used for prediction of potential removal with flushing applications.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗