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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 757 records · Page 42
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NASA NTRS2001

PiVoT GPS Receiver

NASA Goddard Space Flight Center has built an open architecture, 24 channel spaceflight Global Positioning System (GPS) receiver. The compact PCI PiVoT GPS receiver card is based on the Mitel/GEC Plessey Builder 2 board. PiVoT uses two Plessey 2021 correlators to allow tracking of up to 24 separate GPS SV's on unique channels. Its four front ends can support four independent antennas, making it a useful card for hosting GPS attitude determination algorithms. It has been built using space quality, radiation tolerant parts. The PiVoT card works at a lower signal to noise ratio than the original Builder 2 board. It also hosts an improved clock oscillator. The PiVoT software is based on the original Piessey Builder 2 software ported to the Linux operating system. The software is posix compliant and can be easily converted to other posix operating systems. The software is open source to anyone with a licensing agreement with Plessey. Additional tasks can be added to the software to support GPS science experiments or attitude determination algorithms. The next generation PiVoT receiver will be a single radiation hardened compact PCI card containing the microprocessor and the GPS receiver optimized for use above the GPS constellation.

Wennersten, Miriam↗
NASA NTRS2002

ISS Material Science Research Rack HWIL Interface Simulation

In this paper, the first Material Science Research Rack (MSRR-1) hardware-in-the-loop (HWIL) interface simulation is described. Dynamic Concepts developed this HWIL simulation system with funding and management provided by the Flight Software group (ED14) of NASA-MSFC's Avionics Department. The HWIL system has been used both as a flight software development environment and as a software qualification tool. To fulfill these roles, the HWIL simulator accurately models the system dynamics of many MSRR-1 subsystems and emulates most of the internal interface signals. The modeled subsystems include the Experiment Modules, the Thermal Environment Control System, the Vacuum Access System, the Solid State Power Controller Module, and the Active Rack Isolation Systems. The emulated signals reside on three separate MIL-STD-1553B digital communication buses, the ISS Medium Rate Data Link, and several analog controller and sensor signals. To enhance the range of testing, it was necessary to simulate several off-nominal conditions that may occur in the interfacing subsystems.

Williams, Philip J.↗
NASA NTRSDate not supplied

Coupling CFD and Material Response for Analysis of Mars Entry

In computing the response of an ablating thermal protection system during atmospheric entry, the aerothermal environment and material response are generally computed separately with a blowing correction term in the material response model to account for the blowing of char and pyrolysis gases [1]. In this work, we apply a coupled approach in which pyrolysis blowing gases, computed in the PATO material response code [2], are used with a blowing boundary condition in the DPLR hypersonic CFD code [3]. This leads to an iterative method in which blowing products from PATO are input into DPLR to update surface heating estimates. The full iterative method, with the addition of radiative heating estimates using the NEQAIR radiation solver [4], is shown in Fig. 1. The method is demonstrated on a sphere case with the environment and material properties based on the Mars Science Laboratory entry. Future work includes utilizing this method in computing full 3D material response during the Mars 2020 entry.

Heat Transfer↗
NASA NTRSDate not supplied

Thermal Protection System Design of Aerocapture Systems for Uranus Orbiters

The National Academies Planetary Science and Astrobiology Decadal Survey recently identified Uranus and Neptune - called Ice Giants - as the priority destinations for science[1]. The survey assessed both a mission to Uranus through the Uranus Orbiter and Probe (UOP) concept, and Neptune through the Neptune-Triton Odyssey concept and determined that Uranus is the highest priority for a Flagship class mission. The UOP mission will deliver an in situ probe and conduct a multi-year orbital tour of the system to meet the science objectives. While the Uranus mission is currently viable with launch windows starting in 2031 using existing launch vehicles, the mission has a long cruise time to destination (between 12 and 15 years) and would require more than half of its weight in fuel propellant to achieve the change in velocity necessary for orbital insertion. Aerocapture is a method of orbital control that uses aerodynamic forces generated on a vehicle by the planet’s atmosphere to modulate a spacecraft’s trajectory, allowing mission designers to target the final orbital state. For the Uranus mission, using aerocapture for orbital insertion can decrease not only the cruise time to the destination by 2 - 3 years, but the propellant required to achieve orbital insertion (by more than 40%) which would, in turn, increase the available science payload and reduce the timeline for retrieving data vital to the mission’s science objectives[2]. Achieving orbital insertion via aerocapture requires novel algorithms for Guidance, Navigation and Control[3], and mass-efficient Thermal Protection Systems (TPS) performing in a new atmosphere. This paper will focus on the selection and tailoring of the Thermal Protection Systems for the forebody and aftbody heatshields of an aerocapture mission to Uranus. While preliminary results indicate that multiple systems in NASA’s repertoire are capable of performing in the predicted aerothermal environment there are unique aspects like the inert environment that affect ablation efficiency, and the heatload for aerocapture trajectories to the outer planets are among the highest of any mission to-date[4]. These two factors may impose operational requirements to heatshield separation in order to minimize thermal soak to the payload, and may demand TPS thickness and configurations that have not yet been demonstrated. This paper will discuss the updated maturity, manufacturing, and performance capabilities of candidate thermal protection systems, with specific areas of need highlighted to make thermal protection systems viable for use in the recommended Uranus Orbiter and Probe mission.

Uranus↗
NASA NTRS2003

Validation of ADAR System 5500 Digital Imagery: Delivery Task Order #1, Task Request #857 - Brookings, SD

This work was performed under NASA's Verification and Validation Program as an independent check of data supplied by Positive Systems, Inc. through the Earth Science Enterprise's Scientific Data Purchase (SDP) Program. This document serves as the basis for reporting results associated with validation of multispectral imagery according to the specifications of contract NAS 13-98049. The validation was performed under the Positive Systems Imaging System Validation Work Instruction CRSP-WI-28: Spectral registration, spatial resolution, endlaps, sidelaps, and image quality were evaluated. The validation was proceded by Shipment Verification, as described in the Work Instruction CRSP-WI-22: Every image was passed through an automatic ingest verification and thumbnail review process to identify omissions, problems with media integrity, and gross errors in data quality. Validation of metadata files is not within the scope of this report, but it was performed separately.

Blonski, Slawomir↗
NASA NTRS1992

Something is wrong with climate theory

We frequently forget that there is more to science than the making of a more precise measurement or a more elaborate calculation. It is even more than applying to new problems the methods that worked on old problems. These activities, which keep most of us busy most of the time, are important, but the new and unexpected discoveries are more important. And many radically new discoveries arise from scientific puzzles, the "anomalies." We believe that studies of past climates have exposed an anomaly that deserves attention and that may result in a fundamentally new understanding of the climate system. The poles have been much warmer throughout much of Earth's history than they are now. Ice-age episodes with durations of millions of years have been separated by periods of hundreds of millions of years that have left little or no evidence of polar ice sheets. The data are best for the most recent of these ice-free episodes so we will concentrate on the Eocene.

Non-NASA Center↗
NASA NTRS2005

A Simple, Powerful Method for Optimal Guidance of Spacecraft Formations

One of the most interesting and challenging aspects of formation guidance law design is the coupling of the orbit design and the science return. The analyst s role is more complicated than simply to design the formation geometry and evolution. He or she is also involved in designing a significant portion of the science instrument itself. The effectiveness of the formation as a science instrument is intimately coupled with the relative geoniet,ry and evolution of the collection of spacecraft. Therefore, the science return can be maximized by optimizing the orbit design according to a performance metric relevant to the science mission goals. In this work, we present a simple method for optimal formation guidance that is applicable to missions whose performance metric, requirements, and constraints can be cast as functions that are explicitly dependent upon the orbit states and spacecraft relative positions and velocities. We present a general form for the cost and constraint functions, and derive their semi-analytic gradients with respect to the formation initial conditions. The gradients are broken down into two types. The first type are gradients of the mission specific performance metric with respect to formation geometry. The second type are derivatives of the formation geometry with respect to the orbit initial conditions. The fact that these two types of derivatives appear separately allows us to derive and implement a general framework that requires minimal modification to be applied to different missions or mission phases. To illustrate the applicability of the approach, we conclude with applications to twc missims: the Magnetospheric Mu!tiscale mission (MMS), a,nd the TJaser Interferometer Space Antenna (LISA).

Hughes, Steven P.↗
NASA NTRS2006

A Simple, Powerful Method for Optimal Guidance of Spacecraft Formations

One of the most interesting and challenging aspects of formation guidance law design is the coupling of the orbit design and the science return. The analyst's role is more complicated than simply to design the formation geometry and evolution. He or she is also involved in designing a significant portion of the science instrument itself. The effectiveness of the formation as a science instrument is intimately coupled with the relative geometry and evolution of the collection of spacecraft. Therefore, the science return can be maximized by optimizing the orbit design according to a performance metric relevant to the science mission goals. In this work, we present a simple method for optimal formation guidance that is applicable to missions whose performance metric, requirements, and constraints can be cast as functions that are explicitly dependent upon the orbit states and spacecraft relative positions and velocities. We present a general form for the cost and constraint functions, and derive their semi-analytic gradients with respect to the formation initial conditions. The gradients are broken down into two types. The first type are gradients of the mission specific performance metric with respect to formation geometry. The second type are derivatives of the formation geometry with respect to the orbit initial conditions. The fact that these two types of derivatives appear separately allows us to derive and implement a general framework that requires minimal modification to be applied to different missions or mission phases. To illustrate the applicability of the approach, we conclude with applications to two missions: the Magnetospheric Multiscale mission (MMS) , and the Laser Interferometer Space Antenna (LISA).

Hughes, Steven P.↗
NASA NTRS2020

Spitzer Follow-up of Extremely Cold Brown Dwarfs Discovered by the Backyard Worlds: Planet 9 Citizen Science Project

We present Spitzer follow-up imaging of 95 candidate extremely cold brown dwarfs discovered by the Backyard Worlds: Planet 9 citizen science project, which uses visually perceived motion in multi epoch Wide-field Infrared Survey Explorer(WISE)images to identify previously unrecognized substellar neighbors to the Sun. We measure Spitzer[3.6]–[4.5]color to photo type our brown dwarf candidates, with an emphasis on pinpointing the coldest and closest Y dwarfs within our sample. The combination of WISE and Spitzer astrometry provides quantitative confirmation of the transverse motion of 75 of our discoveries. Nine of our motion-confirmed objects have best-fit linear motions larger than 1′′yr−1; our fastest-moving discovery is WISEA J155349.96+693355.2(μ≈215 yr−1),a possible T-type sub dwarf. We also report a newly discovered wide-separation(∼400 au)T8 comoving companion to the white dwarf LSPM J0055+5948(the fourth such system to be found), plus a candidate late T companion to the white dwarf LSR J0002+6357 at 55 projected separation(∼8700 au if associated). Among our motion-confirmed targets, five have Spitzer colors most consistent with spectral type Y. Four of these five have exceptionally red Spitzer colors suggesting types of Y1 or later, adding considerably to the small sample of known objects in this especially valuable low-temperature regime. Our Y dwarf candidates begin bridging the gap between the bulk of the Y dwarf population and the coldest known brown dwarf.

Y dwarfs↗
NASA NTRS2011

Lunabotics Mining Competition: Inspiration Through Accomplishment

NASA's Lunabotics Mining Competition is designed to promote the development of interest in space activities and STEM (Science, Technology, Engineering, and Mathematics) fields. The competition uses excavation, a necessary first step towards extracting resources from the regolith and building bases on the moon. The unique physical properties of lunar regolith and the reduced 1/6th gravity, vacuum environment make excavation a difficult technical challenge. Advances in lunar regolith mining have the potential to significantly contribute to our nation's space vision and NASA space exploration operations. The competition is conducted annually by NASA at the Kennedy Space Center Visitor Complex. The teams that can use telerobotic or autonomous operation to excavate a lunar regolith geotechnical simulant, herein after referred to as Black Point-1 (or BP-1) and score the most points (calculated as an average of two separate 10-minute timed competition attempts) will eam points towards the Joe Kosmo Award for Excellence and the scores will reflect ranking in the on-site mining category of the competition. The minimum excavation requirement is 10.0 kg during each competition attempt and the robotic excavator, referred to as the "Lunabot", must meet all specifications. This paper will review the achievements of the Lunabotics Mining Competition in 2010 and 2011, and present the new rules for 2012. By providing a framework for robotic design and fabrication, which culminates in a live competition event, university students have been able to produce sophisticated lunabots which are tele-operated. Multi-disciplinary teams are encouraged and the extreme sense of accomplishment provides a unique source of inspiration to the participating students, which has been shown to translate into increased interest in STEM careers. Our industrial sponsors (Caterpillar, Newmont Mining, Harris, Honeybee Robotics) have all stated that there is a strong need for skills in the workforce related to robotics and automated machines. In 2010, 22 United States (US) universities competed, and in May 2011 the competition was opened to international participation, with 46 Universities attending. There were 12 international teams and 34 US teams. This combined total directly inspired an estimated 544 university students. More students and the public were engaged via internet broadcasting and social networking media. This is expected to be of value for actual future space missions, as knowledge is gained from testing many innovative prototypes in simulated lunar regolith. More information is available at www.nasa.gov/lunabotics/.

Mueller, Robert P.↗
NASA NTRS2000

The Pascal Discovery Mission: A Mars Climate Network Mission

The climate of Mars is a major focus of Mars exploration. With the loss of MCO, however, it remains uncertain how it will be achieved. We argue that a truly dedicated climate mission to Mars should have both orbital and landed components, and that these should operate simultaneously for at least 1 Mars year if not longer. Pascal is a Discovery mission that emphasizes the landed component. Its principal goal is to establish a network of 24 small weather stations on the surface of Mars that will operate for 2 Mars years, with an extended mission option for an additional 8 Mars years bringing the total mission lifetime up to 10 Mars years. The stations will collect hourly measurements of pressure, temperature, and optical depth. After delivering the probes to Mars, Pascal's carrier spacecraft will go into an elliptical orbit which will serve as a relay for the landers, and a platform for synoptic imaging. These simultaneous measurements from the surface and from orbit will allow us to characterize the planet's general circulation and its interaction with the dust, water, and CO2 cycles. During entry, descent, and landing, each of Pascal's 24 probes will also measure the temperature structure of the atmosphere and acquire images of the surface. These data will allow us to determine the global structure of the atmosphere between 15 and 130 km, and characterize the local terrain to help interpret the landed data. The descent images are part of Pascal's outreach program, as the probe camera system will be developed by faculty-supervised student project. The intent is to generate enthusiasm for the Pascal mission by directly involving students. Pascal will be launched on a Delta II-7925 in August of 2005. A type I trajectory will deliver Pascal to Mars in January of 2006. On approach, the three-axis stabilized carrier spacecraft will spring deploy the Pascal probes in 4 separate salvo's of 6 each. Global coverage is achieved with small time-of-arrival adjustments in between each salvo. Pascal's probes utilize an aeroshell, parachute, and crushable material for entry, descent and landing. On the surface, their long life and global coverage is enabled by a Micro Thermal Power Source with demonstrated heritage. After all probes are released, the carrier spacecraft will execute a small burn for insertion into an elliptical orbit. The long lifetime of the Pascal network was chosen in part to maximize the chances that orbital sounding, like that planned with MCO, would occur at some point during the mission. If Pascal is selected for launch in '05, this could occur if MCO-like science is reflown in the '05 opportunity or, if it is reflown in '03, the mission is extended to overlap with Pascal. The combination of temperature sounding from orbit, and surface pressure mapping from the surface will allow a direct determination of the full 3-D wind field for the first time.

Haberle, R. M.↗
NASA NTRS2000

The Pascal Discovery Mission: A Mars Climate Network Mission

The climate of Mars is a major focus of Mars exploration. With the loss of MCO, however, it remains uncertain how it will be achieved. We argue that a truly dedicated climate mission to Mars should have both orbital and landed components, and that these should operate simultaneously for at least I Mars year if not longer. Pascal is Discovery mission that emphasizes the landed component. Its principal goal is to establish a network of 24 small weather stations on the surface of Mars that will operate for 2 Mars years, with an extended mission option for an additional 8 Mars years bringing the total mission lifetime up to 10 Mars years. The stations will collect hourly measurements of pressure, temperature, and optical depth. After delivering the probes to Mars, Pascal's carrier spacecraft will go into an elliptical orbit which will serve as a relay for the landers, and a platform for synoptic imaging. These simultaneous measurements from the surface and from orbit will allow us to characterize the planet's general circulation and its interaction with the dust, water, and CO2 cycles. During entry, descent, and landing, each of Pascal's 24 probes will also measure the temperature structure of the atmosphere and acquire images of the surface. These data will allow us to determine the global structure of the atmosphere between 15 and 130 km, and characterize the local terrain to help interpret the landed data. The descent images are part of Pascal's outreach program, as the probe camera system will be developed by faculty-supervised student project. The intent is to generate enthusiasm for the Pascal mission by directly involving students. Pascal will be launched on a Delta 11-7925 in August of 2005. A type I trajectory will deliver Pascal to Mars in January of 2006. On approach, the three-axis stabilized carrier spacecraft will spring deploy the Pascal probes in 4 separate salvo's of 6 each. Global coverage is achieved with small time-of-arrival adjustments in between each salvo. Pascal's probes utilize an aeroshell, parachute, and crushable material for entry, descent and landing. On the surface, their long life and global coverage is enabled by a Micro Thermal Power Source with demonstrated heritage. After all probes are released, the carrier spacecraft will execute a small bum for insertion into an elliptical orbit. The long lifetime of the Pascal network was chosen in part to maximize the chances that orbital sounding, like that planned with MCO, would occur at some point during the mission. If Pascal is selected for launch in -05, this could occur if MCO-like science is reflown in the '05 opportunity or, if it is reflown in '03, the mission is extended to overlap with Pascal. The combination of temperature sounding from orbit, and surface pressure mapping from the surface will allow a direct determination of the full 3-D wind field for the first time.

Haberle, Robert M.↗
NASA NTRS2016

Community-Wide Validation of Geospace Model Local K-Index Predictions to Support Model Transition to Operations

We present the latest result of a community-wide space weather model validation effort coordinated among the Community Coordinated Modeling Center (CCMC), NOAA Space Weather Prediction Center (SWPC), model developers, and the broader science community. Validation of geospace models is a critical activity for both building confidence in the science results produced by the models and in assessing the suitability of the models for transition to operations. Indeed, a primary motivation of this work is supporting NOAA/SWPCs effort to select a model or models to be transitioned into operations. Our validation efforts focus on the ability of the models to reproduce a regional index of geomagnetic disturbance, the local K-index. Our analysis includes six events representing a range of geomagnetic activity conditions and six geomagnetic observatories representing midlatitude and high-latitude locations. Contingency tables, skill scores, and distribution metrics are used for the quantitative analysis of model performance. We consider model performance on an event-by-event basis, aggregated over events, at specific station locations, and separated into high-latitude and midlatitude domains. A summary of results is presented in this report, and an online tool for detailed analysis is available at the CCMC.

Glocer, A.↗
NASA NTRS2020

Non-linear Least Square Fitting Technique for the Determination of Field Line Resonance Frequency in Ground Magnetometer Data: Application to Remote Sensing of Plasmaspheric Mass Density

The accurate determination of the Field Line Resonance (FLR) frequency of a resonating geomagnetic field line is necessary to remotely monitor the plasmaspheric mass density during geomagnetic storms and quiet times alike. Under certain assumptions the plasmaspheric mass density at the equator is inversely proportional to the square of the FLR frequency. The most common techniques to determine the FLR frequency from ground magnetometer measurements are the amplitude ratio and phase difference techniques, both based on geomagnetic field observations at two latitudinally separated ground stations along the same magnetic meridian. Previously developed automated techniques have used statistical methods to pinpoint the FLR frequency using the amplitude ratio and phase difference calculations. We now introduce a physics-based automated technique, using non-linear least square fitting of the ground magnetometer data to the analytical resonant wave equations, that reproduces the wave characteristics on the ground, and from those determine the FLR frequency. One of the advantages of the new technique is the estimation of physics-based errors of the FLR frequency, and as a result of the equatorial plasmaspheric mass density. We present analytical results of the new technique, and test it using data from the Inner-Magnetospheric Array for Geospace Science (iMAGS) ground magnetometer chain along the coast of Chile and the east coast of the United States. We compare the results with the results of previously published statistical automated techniques.

A. Boudouridis↗
NASA NTRS1996

National Aeronautics and Space Administration (NASA)/American Society for Engineering Education (ASEE) Summer Faculty Fellowship Program: 1995

The objectives of the JSC NASA/ASEE Summer Faculty Fellowship Program, which began nationally in 1964 and at JSC in 1965, are (1) to further the professional knowledge of qualified engineering and science faculty members; (2) to stimulate an exchange of ideas between participants and NASA; (3) to enrich and refresh the research and teaching activities of the participants' institutions; and (4) to contribute to the research objectives of the NASA centers. Each faculty fellow spent at least 10 weeks at JSC engaged in a research project in collaboration with a NASA/JSC colleague. In addition to the faculty participants, the 1995 program included five students. This document is a compilation of the first fifteen of twenty-seven final reports on the research projects completed by the faculty fellows and visiting students during the summer of 1995. The reports of two of the students are integral with that of the respective fellow. Three students wrote separate reports included in Volume 2.

Hyman, William A.↗
NASA NTRS2004

Global Land Ice Measurements from Space

The NSIDC at the University of Colorado has successfully completed the tasks outlined in its proposal 0999.08.1216B, the 'Global Land Ice Measurements from Space' grant funded by NASA under NAG5-9722. The Global Land Ice Measurements from Space (GLIMS) grant reported on here is one of the first completed elements of the overall GLIMS project that continues with separate funding from NASA, the United States Geological Survey (USGS), and internationally by many national agencies and universities. The primary goals of GLIMS are to survey significant numbers of the world's 160,000 glaciers with data collected by the ASTER (Advanced Spaceborne Thermal Emission and reflection Radiometer) instrument aboard the EOS Terra spacecraft, and Landsat ETM+ (Enhanced Thematic Mapper Plus) and to make these data available to users in a common and easily usable format. GLIMS participants include: NSIDC as developer of the GLIMS database, USGS Flagstaff as the GLIMS Coordination Center, USGS EROS Data Center (EDC) as the archive for satellite imagery used in GLIMS analyses (NASA funding for GLIMS also includes the Flagstaff group and EDC through the related ASTER Science Team and Land Processes Distributed Active Archive Center [LP DAAC] activities), and approximately twenty two Regional Centers (RCs). RCs are funded by the national agencies of participating countries to analyze satellite imagery for a specified set of glaciological parameters and provide the results to NSIDC for archive and distribution to the public.

Scharfen, Gregory R.↗
NASA NTRSDate not supplied

Early Assessments of Crew Timelines for the Lunar Surface Habitat

As NASA progresses towards sustained crewed space missions, crew timelines will become increasingly important to achieving mission goals. While it is desirable to spend as much time as possible during crewed space missions on science activities and experiments, there are a large number of activities that crew members must perform each day in order to maintain both crew and vehicle health and safety. The time available for science activities in space is highly dependent on mandatory tasks required for crew and vehicle health and safety. The different crewed activities need to be planned accordingly long before the start of a mission in order to optimize crew time for science. To begin assessing the potential crew time for available for science, an understanding of the requirements to maintain crew and vehicle health and safety is needed. These additional activities may include sleep, exercise, vehicle maintenance, logistics handling, crew personal time, as well as many other tasks. The remaining time outside of these required tasks, within a reasonable crew work schedule, can be dedicated to science operations. This paper will detail a collaborative effort to analyzing crew times for sustained spaceflight missions and how the results of that analysis are applied to the crew timeline for the proposed Lunar Surface Habitat (SH).To determine the crew time for all of these required activities, an analysis was conducted utilizing defined agency requirements and historical crewed mission data. Predicted crew activity times were integrated into a daily schedule in order to optimize the crew’s time during the mission. This methodology was utilized to produce expected crew timelines for NASA’s proposed Artemis Base Camp (ABC) missions. The current plans for the ABC contain two different sustained habitats, the Pressurized Rover (PR) and the Surface Habitat (SH). While the crew are separated between the two habitats, the timelines for each element are dependent on the other element’s operations, so the two element timelines are formed in conjunction with one another. The results described in this paper, however, will focus solely on the crew timeline in the SH. This paper will explain the methodology behind predicting the required crew time spent in the SH for each activity, and the process of incorporating these predicted crew times into a coherent schedule.

Crew Time↗
NASA NTRS1999

Microfabricated capillary electrophoresis amino acid chirality analyzer for extraterrestrial exploration

Chiral separations of fluorescein isothiocyanate-labeled amino acids have been performed on a microfabricated capillary electrophoresis chip to explore the feasibility of using such devices to analyze for extinct or extant life signs in extraterrestrial environments. The test system consists of a folded electrophoresis channel (19.0 cm long x 150 microns wide x 20 microns deep) that was photolithographically fabricated in a 10-cm-diameter glass wafer sandwich, coupled to a laser-excited confocal fluorescence detection apparatus providing subattomole sensitivity. Using a sodium dodecyl sulfate/gamma-cyclodextrin pH 10.0 carbonate electrophoresis buffer and a separation voltage of 550 V/cm at 10 degrees C, baseline resolution was observed for Val, Ala, Glu, and Asp enantiomers and Gly in only 4 min. Enantiomeric ratios were determined for amino acids extracted from the Murchison meteorite, and these values closely matched values determined by HPLC. These results demonstrate the feasibility of using microfabricated lab-on-a-chip systems to analyze extraterrestrial samples for amino acids.

NASA Discipline Life Sciences Technologies↗