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At least 739 records · Page 41

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NASA NTRS1985

Analysis of vibronic transitions in titanium doped sapphire using the temperature of the fluorescence spectra

An analysis of the fluorescence spectra of titanium-doped sapphire crystals for temperatures ranging from 13 to 578 K is made. Zero- and multiphoton assisted electronic transitions are observed at temperatures below 125 K. Zero-phonon transition energies agree with previously reported measured and predicted values. Photon-assisted transitions suggest that two principle modes of lattice vibrations with energies of 220 and 260/cm are coupled to the electronic 2T2g state. A single phonon energy of 173/cm is observed to couple to the 2Eg electronic state. Crossover energy is estimated to be about 11,800/cm using a simple harmonic approximation. Lineshape analysis is performed. The fluorescence lifetime as measured to be a constant 3.9 microsec below 150 k decreasing to 2.9 microsec at 300 K.

Byvik, C. E.↗

NASA NTRS1985

Bonding and nondestructive evaluation of graphite/PEEK composite and titanium adherends with thermoplastic adhesives

Bonded single overlap shear specimens were fabricated from Graphite/PEEK (Polyetheretherketone) composite adherends and titanium adherends. Six advanced thermoplastic adhesives were used for the bonding. The specimens were bonded by an electromagnetic induction technique producing high heating rates and high-strength bonds in a few minutes. This contrasts with conventionally heated presses or autoclaves that take hours to process comparable quality bonds. The Graphite/PEEK composites were highly resistant to delamination during the testing. This allowed the specimen to fail exclusively through the bondline, even at very high shear loads. Nondestructive evaluation of bonded specimens was performed ultrasonically by energizing the entire thickness of the material through the bondline and measuring acoustic impedance parameters. Destructive testing confirmed the unique ultrasonic profiles of strong and weak bonds, establishing a standard for predicting relative bond strength in subsequent specimens.

Hodges, W. T.↗

NASA NTRS1986

Evaluation of a novel thermoplastic polyimide for bonding titanium

A novel hot-melt processable polyimide has been synthesized and characterized as an adhesive for a titanium alloy. This system shows potential for applications with service temperatures near 200 C. A bonding cycle was developed from preliminary processing studies. The bonded specimens were tested at room temperature, 177 C and 204 C both before and after aging in air at 204 C for times up to 1000 hours. There was no appreciable change in strength after aging. Bonded specimens were exposed to boiling water continuously for a 72 hour period. These specimens exhibited some loss in strength due to this rather severe exposure.

Progar, D. J.↗

NASA NTRS1986

A study of cumulative fatigue damage in titanium 6Al-4V alloy

Experimental data were obtained using titanium 6Al-4V alloy under stress ratios of -1, 0, and negative infinity. A study of cumulative fatigue damage using Miner's (1945) and Kramer's (1974) equations for stress ratios of -1 and 0 for low-high, low-high mixed, high-low, and high-low mixed stress sequences has revealed close agreement between the theoretical and experimental values of fatigue damage and fatigue life. Kramer's equation predicts less conservative and more realistic cumulative fatigue damage than does the popularly used Miner's rule.

Jeelani, S.↗

NASA NTRS1986

Electrochemical behavior of a titanium electrode in hydrazine solutions

The kinetics of the establishment of the oxidation-reduction potential of a titanium electrode upon contact with hydrazine was studied in different media: H2SO4, NaOH, and Na2SO4. It was found that the nature of the potential shift depends little on the medium. The initial potential determines the rate of potential displacement upon contact with hydrazine, which is explained by the different condition of the electrode's surface.

Levchenko, A. K.↗

NASA NTRS1987

Analysis and test of superplastically formed titanium hat-stiffened panels under compression

Four hat-stiffened titanium panels with two different stiffener configurations were fabricated by superplastic forming/weld brazing and tested under a moderately heavy compressive load. The panels had the same overall dimensions but differed in the shape of the hat-stiffener webs; three panels had stiffeners with flat webs and the other panel had stiffeners with beaded webs. Analysis indicated that the local buckling strain of the flat stiffener web was considerably lower than the general panel buckling strain or cap buckling strain. The analysis also showed that beading the webs of the hat stiffeners removed them as the critical element for local buckling and improved the buckling strain of the panels. The analytical extensional stiffness and failure loads compared very well with experimental results.

Davis, Randall C.↗

NASA NTRS1987

Titanium-doped sapphire laser research and design study

Three main topics were considered in this study: the fundamental laser parameters of titanium-doped sapphire, characterization of commercially grown material, and design of a tunable, narrow-linewidth laser. Fundamental parameters investigated included the gain cross section, upper-state lifetime as a function of temperature and the surface-damage threshold. Commercial material was found to vary widely in the level of absorption of the laser wavelength with the highest absorption in Czochralski-grown crystals. Several Yi:sapphire lasers were constructed, including a multimode laser with greater than 50mJ of output energy and a single-transverse-mode ring laser, whose spectral and temporal characteristics were completely characterized. A design for a narrow-linewidth (single-frequency) Ti:sapphire laser was developed, based on the results of the experimental work. The design involves the use of a single-frequency, quasi-cw master oscillator, employed as an injection source for a pulsed ring laser.

Moulton, Peter F.↗

NASA NTRS1987

Comparison of measured temperatures, thermal stresses and creep residues with predictions on a built-up titanium structure

Temperature, thermal stresses, and residual creep stresses were studied by comparing laboratory values measured on a built-up titanium structure with values calculated from finite-element models. Several such models were used to examine the relationship between computational thermal stresses and thermal stresses measured on a built-up structure. Element suitability, element density, and computational temperature discrepancies were studied to determine their impact on measured and calculated thermal stress. The optimum number of elements is established from a balance between element density and suitable safety margins, such that the answer is acceptably safe yet is economical from a computational viewpoint. It is noted that situations exist where relatively small excursions of calculated temperatures from measured values result in far more than proportional increases in thermal stress values. Measured residual stresses due to creep significantly exceeded the values computed by the piecewise linear elastic strain analogy approach. The most important element in the computation is the correct definition of the creep law. Computational methodology advances in predicting residual stresses due to creep require significantly more viscoelastic material characterization.

Jenkins, Jerald M.↗

NASA NTRS1988

Titanium carbide coatings for aerospace ball bearings

In conventional ball bearings, steel to steel contacts between the balls and the raceways are at the origin of microwelds which lead to material transfer, surface roughening, lubricant breakdown, and finally to a loss in the bearing performances. To minimize the microwelding tendencies of the contacting partners it is necessary to modify their surface materials; the solid to solid collisions themselves are difficult to avoid. The use of titanium carbide coated steel balls can bring spectacular improvements in the performances and lifetimes of both oil-grease lubricated and oil-grease free bearings in a series of severe applications.

Boving, Hans J.↗

NASA NTRS1990

Observations of fatigue crack initiation and damage growth in notched titanium matrix composites

The purpose was to characterize damage initiation and growth in notched titanium matrix composites at room temperature. Double edge notched or center open hole SCS-6/Ti-15-3 specimens containing 0 deg plies or containing both 0 and 90 deg plies were fatigued. The specimens were tested in the as-fabricated (ASF) and in heat-treated conditions. A local strain criterion using unnotched specimen fatigue data was successful in predicting fatigue damage initiation. The initiation stress level was accurately predicted for both a double edge notched unidirectional specimen and a cross-plied center hole specimen. The fatigue produced long multiple cracks growing from the notches. These fatigue cracks were only in the matrix material and did not break the fibers in their path. The combination of matrix cracking and fiber/matrix debonding appears to greatly reduce the stress concentration around the notches. The laminates that were heat treated showed a different crack growth pattern. In the ASF specimens, matrix cracks had a more tortuous path and showed considerable more crack branching. For the same specimen geometry and cyclic stress, the (0/90/0) laminate with a hole had far superior fatigue resistance than the matrix only specimen with a hole.

Naik, R. A.↗

NASA NTRS1990

Surface characterization of hydrogen charged and uncharged alpha-2 and gamma titanium aluminide alloys using AES and REELS

The surfaces of selected uncharged and hydrogen charged alpha-2 and gamma titanium aluminide alloys with Nb additions were characterized by Auger electron (AES) and reflected electron energy loss (REELS) spectroscopy. The alloy surfaces were cleaned before analysis at room temperature by ion sputtering. The low energy (500 eV) ion sputtering process preferentially sputtered the surface concentration. The surface concentrations were determined by comparing AES data from the alloys with corresponding data from elemental references. No differences were observed in the Ti or Nb Auger spectra for the uncharged and hydrogen charged alloys, even though the alpha-2 alloy had 33.4 atomic percent dissolved hydrogen. Also, no differences were observed in the AES spectra when hydrogen was adsorbed from the gas phase. Bulk plasmon energy shifts were observed in all alloys. The energy shifts were induced either by dissolved hydrogen (alpha-2 alloy) or hydrogen adsorbed from the gas phase (alpha-2 and gamma alloys). The adsorption induced plasmon energy shifts were greatest for the gamma alloy and cp-Ti metal.

Shanabarger, M. R.↗

NASA NTRS1990

Fatigue damage growth mechanisms in continuous fiber reinforced titanium matrix composites

The role of fiber/matrix interface strength, residual thermal stresses, and fiber and matrix properties on fatigue damage accumulation in continuous fiber metal matrix composites (MMC) is discussed. Results from titanium matrix silicon carbide fiber composites is the primary topic of discussion. Results were obtained from both notched and unnotched specimens at room and elevated temperatures. The stress in the 0 deg fibers was identified as the controlling factor in fatigue life. Fatigue of the notched specimens indicated that cracks can grow in the matrix materials without breaking fibers.

Johnson, W. S.↗

NASA NTRS1989

The effect of hydrogen on mechanical properties of oxygen-strengthened titanium

The effect of oxygen on the hydrogen embrittlement in titanium was investigated in two Ti-based alloys containing different amounts of oxygen: 0.064 and 0.154, in wt pct. Tensile, impact, and hardness tests were performed with and without prior hydrogenation of the specimens. Results show that, while the presence of hydrogen, even in relatively small amounts, will not affect the hardness or room-temperature tensile properties determined at relatively slow strain rates, hydrogen will reduce significantly the impact resistance, as determined by the Charpy V-notch test. This deleterious effect on the impact resistance was found to be exacerbated by an increase of oxygen in the alloy.

Wasz, M. L.↗

NASA NTRS1991

Thermal behavior of a titanium honeycomb-core sandwich panel

Finite element thermal stress analysis was performed on a rectangular titanium honecomb-core sandwich panel which is subjected to thermal load with a temperature gradient across its depth. The distributions of normal stresses in the face sheets and the face-sheet/sandwich-core interfacial shear stresses are presented. The thermal buckling of the heated face sheet was analyzed by assuming the face sheet to be resting on an elastic foundation representing the sandwich core. Thermal buckling curves and thermal buckling load surface are presented for setting the limit for temperature gradient across the panel depth.

Ko, William L.↗

NASA NTRS1989

Effect of grinding on the fatigue life of titanium alloy (5 Al-2.5 Sn) under dry and wet conditions

The principal factors in the performance of aerospace materials are strength-to-weight ratio, fatigue life, fracture toughness, survivability and, of course, reliability. Machining processes and, in particular, grinding under adverse conditions have been found to cause damage to surface integrity and affect the residual stress distribution in the surface and subsurface region. These effects have a direct bearing on the fatigue life. In this investigation the effects of grinding conditions on the fatigue life of Titanium 5 Al-2.5Sn were studied. This alloy is used in ground form in the manufacturing of some critical components in the space shuttle's main engine. It is essential that materials for such applications be properly characterized for use in severe service conditions. Flat sub-size specimens 0.1 inch thick were ground on a surface grinding machine equipped with a variable speed motor at speeds of 2000 to 6000 rpm using SiC wheels of grit sizes 60 and 120. The grinding parameters used in this investigation were chosen from a separate study. The ground specimens were then fatigued at a selected stress and the resulting lives were compared with that of the virgin material. The surfaces of the specimens were examined under a scanning electron microscope, and the roughness and hardness were measured using a standard profilometer and microhardness tester, respectively. The fatigue life of the ground specimens was found to decrease with the increase in speed for both dry and wet conditions. The fatigue life of specimens ground under wet conditions showed a significant increase at the wheel speed of 2000 rpm for both the grit sizes and thereafter decreased with increase profilometry, microhardness measurements and scanning electron microscopic examination.

Rangaswamy, Partha↗

NASA NTRS1990

Characterization of hydrogen interactions with the surface of alpha-2 titanium aluminide alloys

The interaction of hydrogen at the surface of alpha-2 titanium aluminide alloys with Nb additions has been investigated with Auger electron spectroscopy (AES) and reflected electron energy loss (REELS) spectroscopy. The hydrogen was either adsorbed onto the alloy surface from the gas phase or it was pre-charged into the alloy forming an alpha-2 hydride. No effect of either adsorbed or absorbed hydrogen was observed in the Auger spectra. A shift in the bulk plasmon loss energy (observed with REELS) was measured for both conditions. The potential significance of these results in relation to hydrogen interactions in this alloy is discussed.

Shanabarger, Mickey R.↗

NASA NTRS1991

Effect of grinding conditions on the fatigue life of titanium 5Al-2.5Sn alloy

An investigation into the effect of grinding conditions on the fatigue life of titanium 5Al-2.5Sn is presented. Damage to surface integrity and changes in the residual stresses distribution are studied to assess changes in fatigue life. A surface grinding machine, operating at speeds ranging from 2000 to 6000 fpm and using SiC wheels of grit sizes 60 and 120, was used to grind flat subsize specimens of 0.1-in. thickness. After grinding, the specimens were fatigued at a chosen stress and compared with the unadulterated material. A standard profilometer, a microhardness tester, and a scanning electron microscope were utilized to examine surface characteristics and measure roughness and hardness. Increased grinding speed in both wet and dry applications tended to decrease the fatigue life of the specimens. Fatigue life increased markedly at 2000 fpm under wet conditions, but then decreased at higher speeds. Grit size had no effect on the fatigue life.

Rangaswamy, P.↗

NASA NTRS1991

Effect of chromium and phosphorus on the physical properties of iron and titanium-based amorphous metallic alloy films

Amorphous iron and titanium-based alloys containing various amounts of chromium, phosphorus, and boron exhibit high corrosion resistance. Some physical properties of Fe and Ti-based metallic alloy films deposited on a glass substrate by a dc-magnetron sputtering technique are reported. The films were characterized using differential scanning calorimetry, stress analysis, SEM, XRD, SIMS, electron microprobe, and potentiodynamic polarization techniques.

Distefano, S.↗