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At least 739 records · Page 41
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Inhibition of Micro-pitting by Tribofilm-Forming ZrO 2 Nanocrystal Lubricant Additives: A Micro-pitting Rig and Transmission Electron Microscope Study

The drive to reduce fuel consumption in transportation has encouraged the emergence of low viscosity lubricants to reduce viscous losses in the engine, drivetrain, and other components. However, viscosity reduction increases the risk of surface damage, thus motivating the development of new anti-wear (AW) additives. Capped ZrO 2 nanocrystals (NCs) in base oils have been shown to form AW tribofilms within microscale sliding contacts. However, the potential of ZrO 2 NCs to protect surfaces subjected to rolling-sliding contact from macroscale damage, such as micro-pitting, remains unexplored. Here, we explore the ability of ZrO 2 NCs to form protective tribofilms under harsh conditions using a micro-pitting rig (MPR), consisting of a three ring-on-roller configuration. The experiments were conducted in polyalphaolephin (PAO) base oil, with and without 5 nm diameter ZrO 2 NCs, at two levels of slide-to-roll ratio (SRR) (30% and 0%) and at variable test durations up to long durations (119 h). MPR results showed the use of ZrO 2 NCs gives rise to the formation of a tribofilm covering the roller surfaces and decreases the initiation and propagation of micro-pits compared to tests in pure PAO base stock. Transmission electron microscopy (TEM) performed on focused ion beam (FIB) milled cross-sectional samples of the roller surfaces revealed the growth of dense and 50–100 nm thick ZrO 2 -based tribofilms independent of (SRR), indicating the potential for robust micro-pitting fatigue protection. Nevertheless, small cracks localized within the near surface region of the roller tested at the most severe conditions (30% SRR and 119 h) were observed. The initiation of these cracks was directly related to the presence of manganese sulphide (MnS) inclusions in the steel, revealed using TEM combined with energy dispersive spectroscopy (EDS). Furthermore, the results highlight the benefits of the protective tribofilms formed by ZrO 2 NCs and suggest approaches for further optimizing their use.

36 MATERIALS SCIENCE↗
NASA NTRS1983

Effect of crack curvature on stress intensity factors for ASTM standard compact tension specimens

The stress intensity factors (SIF) are calculated using the method of lines for the compact tension specimen in tensile and shear loading for curved crack fronts. For the purely elastic case, it was found that as the crack front curvature increases, the SIF value at the center of the specimen decreases while increasing at the surface. For the higher values of crack front curvatures, the maximum value of the SIF occurs at an interior point located adjacent to the surface. A thickness average SIF was computed for parabolically applied shear loading. These results were used to assess the requirements of ASTM standards E399-71 and E399-81 on the shape of crack fronts. The SIF is assumed to reflect the average stress environment near the crack edge.

Alam, J.↗
DOE OSTI2022

Stress-controlled fatigue of HfNbTaTiZr high-entropy alloy and associated deformation and fracture mechanisms

The stress-controlled fatigue tests are carried out at a stress ratio of 0.1 and a frequency of 10 Hz, and span both low-cycle and high-cycle regimes by varying the applied stress amplitudes. The high-cycle fatigue regime gives a fatigue strength of 497 MPa and a fatigue ratio of 0.44. At equivalent conditions, the alloy's fatigue strength is greater than all other high-entropy alloys (HEAs) with reported high-cycle fatigue data, dilute body-centered cubic alloys, and many structural alloys such as steels, titanium alloys, and aluminum alloys. Through in-depth analyses of crack-propagation trajectories, fracture-surface morphologies and deformation plasticity by means of various microstructural analysis techniques and theoretical frameworks, the alloy's remarkable fatigue resistance is attributed to delayed crack initiation in the high-cycle regime, which is achieved by retarding the formation of localized persistent slip bands, and its good resistance to crack propagation in the low-cycle regime, which is accomplished by intrinsic toughening backed up by extrinsic toughening. Additionally, the stochastic nature of the fatigue data is neatly captured with a 2-parameter Weibull model.

36 MATERIALS SCIENCE↗
NASA NTRS1976

Crack problems in cylindrical and spherical shells

Standard plate or shell theories were used as a starting point to study the fracture problems in thin-walled cylindrical and spherical shells, assuming that the plane of the crack is perpendicular to the surface of the sheet. Since recent studies have shown that local shell curvatures may have a rather considerable effect on the stress intensity factor, the crack problem was considered in conjunction with a shell rather than a plate theory. The material was assumed to be isotropic and homogeneous, so that approximate solutions may be obtained by approximating the local shell crack geometry with an ideal shell which has a solution, namely a spherical shell with a meridional crack, a cylindrical shell with a circumferential crack, or a cylindrical shell with an axial crack. A method of solution for the specially orthotropic shells containing a crack was described; symmetric and skew-symmetric problems are considered in cylindrical shells with an axial crack.

Erdogan, F.↗
NASA NTRS1981

Fracture and failure: Analyses, mechanisms and applications; Proceedings of the Symposium, Los Angeles, CA, March 17-20, 1980

Papers are presented on the application of fracture mechanics to spacecraft design, fracture control applications on the Space Shuttle reaction control thrusters, and an assessment of fatigue crack growth rate relationships for metallic airframe materials. Also considered are fracture mechanisms and microstructural relationships in Ni-base alloy systems, the use of surface deformation markings to determine crack propagation directions, case histories of metallurgical failures in the electronics industry, and a failure analysis of silica phenolic nozzle liners.

Tung, P. P.↗
NASA NTRS1993

NDE of PWA 1480 single crystal turbine blade material

Cantilever bending fatigue specimens were examined by fluorescent liquid penetrant and radioactive gas penetrant (Krypton) non-destructive evaluation (NDE) methods and tested. Specimens with cast, ground, or polished surface were evaluated to study the effect of surface condition on NDE and fatigue crack initiation. Fractographic and metallurgical analyses were performed to determine the nature of crack precursors. Preliminary results show that fatigue strength was lower for specimens with cast surfaces than for specimens with machined surfaces. The liquid penetrant and gas penetrant techniques both provided indications of a large population of defects on the cast surfaces. On ground or polished specimen surfaces, the gas penetrant appeared to estimate the actual number of voids more accurately than the liquid penetrant.

Klima, Stanley J.↗
NASA NTRS1993

NDE of PWA 1480 single crystal turbine blade material

Cantilever bending fatigue specimens were examined by fluorescent liquid penetrant and radioactive gas penetrant (Krypton) Nondestructive Evaluation (NDE) methods and tested. Specimens with cast, ground, or polished surfaces were evaluated to study the effect of surface condition on NDE and fatigue crack initiation. Fractographic and metallurgical analyses were performed to determine the nature of crack precursors. Preliminary results show that fatigue strength was lower for specimens with cast surfaces than for specimens with machined surfaces. The liquid penetrant and gas penetrant techniques both provided indications of a large population of defects on the cast surfaces. On ground or polished specimen surfaces, the gas penetrant appeared to estimate the actual number of voids more accurately than the liquid penetrant.

Klima, Stanley J.↗
DOE OSTI2025

Fatigue behavior of low-cost, non-spherical Ti-6Al-4V powder processed via laser powder bed fusion

Hydride-dehydride Ti-6Al-4V powder with particle size distribution of 75–175 μm were used to manufacture fatigue samples. Optimized processing parameters were used to maintain a relative density of >99.5% in the samples. Fatigue tests were carried out in R = σ min /σ max = -1 condition under stresses ranging from 150 to 500 MPa and the results were compared to samples that were additively manufactured using spherical powders. The fatigue lives were similar between the two types of powder; i.e., powder morphology has no effect on fatigue performance. However, the high surface roughness and martensitic microstructure resulting from the laser powder bed fusion process result in poor performance compared to samples machined from conventionally produced materials. In conclusion, crack initiation occurred consistently from surface defects because of high surface roughness of the additively manufactured parts.

36 MATERIALS SCIENCE↗
NASA NTRS1972

Cracking of the lunar soil

Rather than a pattern of cracks in an apparently flat surface, the Apollo 12 photographs suggest an irregular surface that consists of clods or fragments. The impression of flat tiles and crusting, obtained by monoscopic viewing, is an illusion. Instead, the lunar soil deforms and cracks in the same manner as homogeneous isotropic terrestrial soils of moderate bulk density, having a small amount of cohesion.

Jaffe, L. D.↗
NASA NTRS1993

Intrinsic fatigue crack growth rates for Al-Li-Cu-Mg alloys in vacuum

The influences of microstructure and deformation mode on inert environment intrinsic fatigue crack propagation were investigated for Al-Li-Cu-Mg alloys AA2090, AA8090, and X2095 compared to AA2024. The amount of coherent shearable delta-prime (Al3Li) precipitates and extent of localized planar slip deformation were reduced by composition (increased Cu/Li in X2095) and heat treatment (double aging of AA8090). Intrinsic growth rates, obtained at high constant K(max) to minimize crack closure and in vacuum to eliminate any environmental effect, were alloy dependent; da/dN varied up to tenfold based on applied Delta-K or Delta-K/E. When compared based on a crack tip cyclic strain or opening displacement parameter, growth rates were equivalent for all alloys except X2095-T8, which exhibited unique fatigue crack growth resistance. Tortuous fatigue crack profiles and large fracture surface facets were observed for each Al-Li alloy independent of the precipitates present, particularly delta-prime, and the localized slip deformation structure. Reduced fatigue crack propagation rates for X2095 in vacuum are not explained by either residual crack closure or slip reversibility arguments; the origin of apparent slip band facets in a homogeneous slip alloy is unclear.

Slavik, D. C.↗
NASA NTRS1992

An energy analysis of crack-initiation and arrest in epoxy

The objective of this work is to study fracture processes such as crack initiation and arrest in epoxy. A compact tension specimen with displacement-controlled loading is employed to observe multiple crack initiations and arrests. The energy release rate at crack initiation is significantly higher than that at crack arrest, as has been observed elsewhere. In this study, the difference between these energy release rates is found to depend on specimen size (scale effect), and is quantitatively related to the fracture surface morphology. The scale effect, similar to that in strength theory, is conventionally attributed to the statistics of defects which control the fracture process. Triangular shaped ripples, deltoids, are formed on the fracture surface of the epoxy during the slow sub-critical crack growth, prior to the smooth mirrorlike surface characteristic of fast cracks. The deltoids are complimentary on the two crack faces which excludes any inelastic deformation from consideration. The deltoids are analogous to the ripples created on a river surface downstream from a small obstacle. However, in spite of the expectation based on this analogy and the observed scale effect, there are no 'defects' at the apex of the deltoids detectable down to the 0.1 micron level. This suggests that the formation of deltoids during the slow process of subcritical crack growth is an intrinsic feature of the fracture process itself, triggered by inhomogeneity of material on a submicron scale. This inhomogeneity may be related to a fluctuation in the cross-link density of the epoxy.

Chudnovsky, A.↗
NASA NTRS1990

Thermomechanical testing techniques for high-temparature composites: TMF behavior of SiC(SCS-6)/Ti-15-3

Thermomechanical testing techniques recently developed for monolithic structural alloys were successfully extended to continuous fiber reinforced composite materials in plate form. The success of this adaptation was verified on a model metal matrix composite (MMC) material, namely SiC(SCS-6)/Ti-15V-3Cr-3Al-3Sn. Effects of heating system type and specimen preparation are also addressed. Cyclic lives determined under full thermo-mechanical conditions were shown to be significantly reduced from those obtained under comparable isothermal and in-phase bi-thermal conditions. Fractography and metallography from specimens subjected to isothermal, out-of-phase and in-phase conditions reveal distinct differences in damage-failure modes. Isothermal metallography revealed extensive matrix cracking associated with fiber damage throughout the entire cross-section of the specimen. Out-of-phase metallography revealed extensive matrix damage associated with minimal (if any) fiber cracking. However, the damage was located exclusively at surface and near-surface locations. In-phase conditions produced extensive fiber cracking throughout the entire cross-section, associated with minimal (if any) matrix damage.

Castelli, Michael G.↗
NASA NTRS1992

Thermomechanical testing of high-temperature composites - Thermomechanical fatigue (TMF) behavior of SiC(SCS-6)/Ti-15-3

Thermomechanical testing techniques recently developed for monolithic structural alloys were successfully extended to continuous fiber reinforced composite materials in plate form. The success of this adaptation was verified on a model metal matrix composite (MMC) material, namely SiC(SCS-6)/Ti-15V-3Cr-3Al-3Sn. Effects of heating system type and specimen preparation are also addressed. Cyclic lives determined under full thermomechanical conditions were shown to be significantly reduced from those obtained under comparable isothermal and in-phase bi-thermal conditions. Fractography and metallography from specimens subjected to isothermal, out-of-phase and in-phase conditions reveal distinct differences in damage-failure modes. Isothermal metallography revealed extensive matrix cracking associated with fiber damage throughout the entire cross-section of the specimen. Out-of-phase metallography revealed extensive matrix damage associated with minimal (if any) fiber cracking. However, the damage was located exclusively at surface and near-surface locations. In-phase conditions produced extensive fiber cracking throughout the entire cross-section, associated with minimal (if any) matrix damage.

Castelli, Michael G.↗
NASA NTRS1989

Treatment of singularities in cracked bodies

Three-dimensional finite-element analyses of middle-crack tension (M-T) and bend specimens subjected to mode I loadings were performed to study the stress singularity along the crack front. The specimen was modeled using 20-node isoparametric elements. The displacements and stresses from the analysis were used to estimate the power of singularities using a log-log regression analysis along the crack front. The analyses showed that finite-sized cracked bodies have two singular stress fields of the form rho = C sub o (theta, z) r to the -1/2 power + D sub o (theta, phi) R to the lambda rho power. The first term is the cylindrical singularity with the power -1/2 and is dominant over the middle 96 pct (for Poisson's ratio = 0.3) of the crack front and becomes nearly zero at the free surface. The second singularity is a vertex singularity with the vertex point located at the intersection of the crack front and the free surface. The second term is dominant at the free surface and becomes nearly zero away from the the boundary layer. The thickness of the boundary layer depends on Poisson's ratio of the material and is independent of the specimen type. The thickness of the boundary layer varied from 0 pct to about 5 pct of the total specimen thickness as Poisson's ratio varied from 0.0 to 0.45. Because there are two singular stress fields near the free surface, the strain energy release rate (G) is an appropriate parameter to measure the severity of the crack.

Shivakumar, K. N.↗
NASA NTRS1990

Treatment of singularities in cracked bodies

Three-dimensional finite-element analyses of middle-crack tension (M-T) and bend specimens subjected to mode I loadings were performed to study the stress singularity along the crack front. The specimen was modeled using 20-node isoparametric elements. The displacements and stresses from the analysis were used to estimate the power of singularities using a log-log regression analysis along the crack front. The analyses showed that finite-sized cracked bodies have two singular stress fields of the form rho = C sub o (theta, z) r to the -1/2 power + D sub o (theta, phi) R to the lambda rho power. The first term is the cylindrical singularity with the power -1/2 and is dominant over the middle 96 pct (for Poisson's ratio = 0.3) of the crack front and becomes nearly zero at the free surface. The second singularity is a vertex singularity with the vertex point located at the intersection of the crack front and the free surface. The second term is dominant at the free surface and becomes nearly zero away from the boundary layer. The thickness of the boundary layer depends on Poisson's ratio of the material and is independent of the specimen type. The thickness of the boundary layer varied from 0 pct to about 5 pct of the total specimen thickness as Poisson's ratio varied from 0.0 to 0.45. Because there are two singular stress fields near the free surface, the strain energy release rate (G) is an appropriate parameter to measure the severity of the crack.

Shivakumar, K. N.↗
DOE OSTI2025

Halide Vapor Phase Epitaxy of Ge from an Elemental Source

Halide vapor phase epitaxy shows promise for low-cost photovoltaic device manufacturing because of its high growth rates and lower cost elemental precursors but previously has not been used to deposit epitaxial Ge. Here, we demonstrate Ge deposition by generating GeCl 2 in situ from solid Ge and HCl in a N 2 ambient. To achieve Ge growth, we inject AsH 3 and PH 3 as sources of active hydrogen to the growth surface to create a driving force for growth. We do not observe Ge growth unless a supply of hydrogen is added, consistent with thermodynamic calculations. Furthermore, we show the hydrogen source must crack readily on the substrate surface to enable growth; relatively stable sources such as H 2 do not cause growth. Unintentional group V doping is one drawback of using AsH 3 and PH 3 to drive the Ge reaction. We observed As or P concentrations in the Ge films ranging from 4 x 10 17 to 1 x 10 18 atoms/cm 3 , concentrations that can drastically influence device characteristics. However, we note there are numerous other "helper molecule" options that can provide active hydrogen without doping or etching the material. This work provides a path forward for Ge deposition for optoelectronic devices from an elemental source.

14 SOLAR ENERGY↗
NASA NTRS1981

Cyclic plasticity models and application in fatigue analysis

An analytical procedure for prediction of the cyclic plasticity effects on both the structural fatigue life to crack initiation and the rate of crack growth is presented. The crack initiation criterion is based on the Coffin-Manson formulae extended for multiaxial stress state and for inclusion of the mean stress effect. This criterion is also applied for the accumulated damage ahead of the existing crack tip which is assumed to be related to the crack growth rate. Three cyclic plasticity models, based on the concept of combination of several yield surfaces, are employed for computing the crack growth rate of a crack plane stress panel under several cyclic loading conditions.

Kalev, I.↗