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Results for “Diffraction optics”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 739 records · Page 41
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

(NH 4 ) 2 [UO 2 Cl 4 ]·2H 2 O, a new uranyl tetrachloride with ammonium charge-balancing cations

A new uranyl tetrachloride salt with chemical formula, (NH 4 ) 2 [UO 2 Cl 4 ]·2H 2 O, namely, diammonium uranyl tetrachloride dihydrate, 1 , was prepared and crystallized via slow evaporation from a solution of 2 M hydrochloric acid. As confirmed by powder X-ray diffraction, the title compound crystallizes with an ammonium chloride impurity that formed as a result of the breakdown of a triazine precursor. The (UO 2 Cl 4 ) 2− dianion is charge balanced by ammonium cations, while an extensive hydrogen-bond network donated from structural water molecules stabilize the overall assembly. Compound 1 adds to the extensive collection of actinyl tetrachloride salts, but it represents the first without an alkali cation for purely inorganic compounds. Diffuse reflectance and luminescence spectra show typical absorption and emission behavior, respectively, of uranyl materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2026

Development of PNNL’s Plutonium Metallography Capability

The goal of this project was to develop plutonium metallography capabilities and establish workflows for characterization at PNNL’s Radiological Processing Facility (RPL). Developing and expanding on this capability opens more opportunities for PNNL to better support science through collaborations with other labs, plants, and sites withing the Department of Energy Complex and through programs within the National Nuclear Security Administration. This project established metallography equipment in an air glovebox, polishing protocols, as well as radiological and facility controls and procedures so that gram quantities of plutonium metal could be analyzed on multiple characterization tools. Data was collected and analyzed on two different delta phase plutonium - Gallium samples and a calciothermically reduced alpha plutonium metal using a combination of optical and electron microscopy, powder X-ray diffraction, and atom probe tomography. This report highlights the metallography capabilities, some preliminary data collections, and plans at PNNL to support plutonium material science.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Effect of Composition on the Phase Structure and Magnetic Properties of Ball-Milled LaFe11.71-xMnxSi1.29H1.6 Magnetocaloric Powders

Magnetocaloric alloys are an important class of materials that enable non-vapor compression cycles. One promising candidate for magnetocaloric systems is LaFeMnSi, thanks to a combination of factors including low-cost constituents and a useful curie temperature, although control of the constituents’ phase distribution can be challenging. In this paper, the effects of composition and high energy ball milling on the particle morphology and phase stability of LaFe11.71-xMnxSi1.29H1.6 magnetocaloric powders were investigated. The powders were characterized with optical microscopy, dynamic light scattering, X-ray diffraction (XRD), and differential scanning calorimetry (DSC). It was found that the powders retained most of their original magnetocaloric phase during milling, although milling reduced the degree of crystallinity in the powder. Furthermore, some oxide phases (<1 weight percent) were present in the as-received and milled powders, which indicates that no significant contamination of the powders occurred during milling. Finally, the results indicated that the Curie temperature drops as Fe content decreases (Mn content increases). In all of the powders, milling led to an increase in the Curie temperature of ~3–6 °C.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1967

Impact glass in the Cachari eucrite.

Preatmospheric hypervelocity impact black glass in Cachari eucrite studied by optical microscopy, electron microprobe and X-ray diffraction

VITREOUS MATERIAL↗
NASA NTRS1969

A survey of laser display

Laser display systems, discussing mechanical, diffractive and refractive beam deflection techniques, electro-optical polarization devices, holographic displays, etc

Devaney, A. J.↗
NASA NTRS1973

Automated thematic mapping and change detection of ERTS-1 images, part A

The author has identified the following significant results. Automatic and accurate image processing techniques are essential to full utilization of ERTS-1 photography. In pursuit of this, terrain types in the ERTS-1 photography will be classified by spatial signatures. Diffraction patterns from selected ERTS-1 images have been developed optically and are being analyzed to identify unique signatures for various terrain types. Spatial signatures have been definitely identified for cultivated land and certain urban areas. A Fourier plane mask has been developed that greatly facilitates the analysis of the diffraction patterns.

Gramenopoulos, N.↗
NASA NTRS1974

Lunar sample contracts

The major scientific accomplishments through 1971 are reported for the particle track studies of lunar samples. Results are discussed of nuclear track measurements by optical and electron microscopy, thermoluminescence, X-ray diffraction, and differential thermal analysis.

Walker, R. M.↗
NASA NTRS1974

Skylab program payload integration. TO27 sample array

The objective of the TO27 sample array was to determine the change in optical properties of various transmissive windows, mirrors, and diffraction gratings caused by the deposition of contaminants found about the orbital assembly. The expected information to be obtained from the total TO27 sample array program is as follows: (1) effect of space contaminants on transmittance, reflectance, grating efficiency, and polarization; (2) variations in deposition of contaminants due to substrate, solar radiation, period of exposure, direction of exposure, and geometry effects; (3) identification of contaminants and source of evolution; (4) time of contaminant evolution and lingering time; and (5) guidelines for a model of spacecraft contamination.

Muscari, J. A.↗
NASA NTRS1975

Evaluation of silicon ribbon material for solar cell fabrication

Optical microscopy, electron microscopy, and X-ray diffraction were utilized to characterize silicon ribbon structure. Complex twin formation was observed in nearly all ribbons examined. Twins formed in the 110-plane 112-line ribbon orientation appear stable, and this orientation may be preferable when the ribbon is utilized for solar cells. In addition to twinning, grain boundaries and other structural defects were observed in the ribbon material. Hall effect, resistivity, spreading resistance, surface photovoltage, and solar cell electrical/optical measurements were performed on ribbon samples and correlated with structural and ribbon growth characteristics. Only those ribbon samples with either single-crystal structure or with 'parallel' twin formations were capable of solar-cell performance approaching that of Czochralski material.

Leipold, M.↗
NASA NTRS1988

Correlation lifetimes of quiet and magnetic granulation from the SOUP instrument on Spacelab 2

The time sequences of diffraction limited granulation images obtained by the Solar Optical Universal Polarimeter on Spacelab 2 are presented. The uncorrection autocorrelation limetime in magnetic regions is dominated by the 5-min oscillation. The removal of this oscillation causes the autocorrelation lifetime to increase by more than a factor of 2. The results suggest that a significant fraction of granule lifetimes are terminated by nearby explosions. Horizontal displacements and transverse velocities in the intensity field are measured. Lower limits to the lifetime in the quiet and magnetic sun are set at 440 s and 950 s, respectively.

Title, A.↗
NASA NTRS1989

Mechanical alloying, characterization and consolidation of Ti-Al-Ni alloys

Mechanical alloying is being investigated as a processing route for the production of aluminide intermetallics. This program involves powder production and characterization, consolidation and thermal treatments and determination of microstructure-property relationships. An attritor mill is being used to produce powder in lots up to 1000 grams and the processing parameters are being systematically varied to establish the optimum milling conditions. The mill is being instrumented to generate data related to the processing to provide a basis for theoretical modeling. Powder is being characterized using thermal analysis, optical and electron microscopy and X-ray diffraction. Particle size distributions and powder density are being determined. Consolidation of the powder is being approached in several different ways including, cold isostatic pressing, sintering, extrusion and hot pressing. The results of the program so far will be presented and future directions discussed.

Nash, P.↗
NASA NTRS1990

Space optics for studying extra-solar planetary systems

The sharp imaging of telescopes in space will improve the ability to see faint objects near bright ones. One exciting application is the search for planets around other stars. However, because a planet is, at best, 10 exp 9 times fainter than a star in visible light, specialized optical systems are required. Using apodization to remove diffracted light, the limiting source of noise is the intensity of starlight scattered by mirror figure errors. Based on the prelaunch metrology of the HST mirrors, and considering only photonstatistics, months of integration would be needed for HST to detect Jupiter next to the sun at a distance of 5 pc. The integration times will be shorter for future telescopes in space with smoother mirrors and/or larger apertures.

Brown, Robert A.↗
NASA NTRS1993

Direct 75 milliarcsecond images from the Multiple Mirror Telescope with adaptive optics

We report results from an adaptive optics system designed to provide imaging at the diffraction limit of resolution in the near-infrared at the Multiple Mirror Telescope (MMT). For the present experiment, the aperture consisted of five of the six primary mirrors of the MMT, operating as a coherently phased array. The largest components of the atmospherically induced wave-front aberration are the fluctuations in mean phase between the segments. These errors were derived in real time from the Fourier transform of short-exposure stellar images at 2.2 microns and corrected at an image of the telescope pupil with piston motion from a segmented adaptive mirror. At a correction rate of 43 Hz, this level of adaptive control resulted in an integrated image with a clear diffraction-limited component of 0.075 arcsec FWHM. This stabilized component is present directly in the light arriving at the detector and is not the result of postprocessing. We discuss future improvements to our adaptive wave-front control and its application to astronomical observations.

Lloyd-Hart, M.↗
NASA NTRS1993

An in-depth analysis and modelling of the Shuttle to MILA S-band telemetry link

The S-Band radio frequency (RF) link between the Merritt Island (MILA) Tracking Station and the Space Shuttle launch pads is a critical communication path for prelaunch and launch operations. The proposed siting of the Center for Space Education (CSE) at the Visitor Center required a study to avoid RF line-of-sight blockage and reflection paths. The study revealed the trees near MILA's 9-meter (9-M) antennas are obstructing the optical line-of-sight. The studies found diffraction is the main propagation mechanism. This paper describes a link model based on the Geometric Theory of Diffraction.

Caroglanian, Armen↗
NASA NTRS1995

Novel solutions to low-frequency problems with geometrically designed beam-waveguide systems

The poor low-frequency performance of geometrically designed beam-waveguide (BWG) antennas is shown to be caused by the diffraction phase centers being far from the geometrical optics mirror focus, resulting in substantial spillover and defocusing loss. Two novel solutions are proposed: (1) reposition the mirrors to focus low frequencies and redesign the high frequencies to utilize the new mirror positions, and (2) redesign the input feed system to provide an optimum solution for the low frequency. A novel use of the conjugate phase-matching technique is utilized to design the optimum low-frequency feed system, and the new feed system has been implemented in the JPL research and development BWG as part of a dual S-/X-band (2.3 GHz/8.45 GHz) feed system. The new S-band feed system is shown to perform significantly better than the original geometrically designed system.

Imbriale, W. A.↗
NASA NTRS2000

Poster Presentation: Optical Test of NGST Developmental Mirrors

An Optical Testing System (OTS) has been developed to measure the figure and radius of curvature of NGST developmental mirrors in the vacuum, cryogenic environment of the X-Ray Calibration Facility (XRCF) at Marshall Space Flight Center (MSFC). The OTS consists of a WaveScope Shack-Hartmann sensor from Adaptive Optics Associates as the main instrument, a Point Diffraction Interferometer (PDI), a Point Spread Function (PSF) imager, an alignment system, a Leica Disto Pro distance measurement instrument, and a laser source palette (632.8 nm wavelength) that is fiber-coupled to the sensor instruments. All of the instruments except the laser source palette are located on a single breadboard known as the Wavefront Sensor Pallet (WSP). The WSP is located on top of a 5-DOF motion system located at the center of curvature of the test mirror. Two PC's are used to control the OTS. The error in the figure measurement is dominated by the WaveScope's measurement error. An analysis using the absolute wavefront gradient error of 1/50 wave P-V (at 0.6328 microns) provided by the manufacturer leads to a total surface figure measurement error of approximately 1/100 wave rms. This easily meets the requirement of 1/10 wave P-V. The error in radius of curvature is dominated by the Leica's absolute measurement error of VI.5 mm and the focus setting error of Vi.4 mm, giving an overall error of V2 mm. The OTS is currently being used to test the NGST Mirror System Demonstrators (NMSD's) and the Subscale Beryllium Mirror Demonstrator (SBNM).

Hadaway, James B.↗
NASA NTRS2021

Active Wide-Field Sky Simulator Design for the JPL Astrometry Testbed

Exoplanet detection through astrometry will provide mass measurements that are key to our understanding of exoplanet demographics. Astrometric surveys are also critical pre-cursor observations for identifying targets for future direct imaging missions, such as the HabEx and LUVOIR mission concepts. However, Earth-mass planets orbiting Sun-like stars within 10 pc only cause a 0.3 uas astrometric signal, which is about two orders of magnitude smaller than the current state-of-the-art. In order to advance the technologies needed for future astrometry instruments, a testbed capable of simulating and measuring equivalent Earth-like exoplanet astrometric signals was created. The testbed has a stable light source that simulates a field of stars and can introduce a sub-uas astrometric signal onto a central artificial target star. This is done by illuminating an array of pinholes lithographically printed onto a glass substrate and translating, with picometer resolution, a target-star pinhole located on a centrally cut flexure feature. To detect this motion, a diffractive pupil is used to calibrate the limiting optical distortions of an Offner relay. Presented in this paper are the requirements, design, and implementation of the wide-field astrometry testbed’s light source.

Bendek, Eduardo↗