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NASA NTRS1996

Design of an Improved Heater Array to Measure Microscale Wall Heat Transfer

An improved array of microscale heaters is being developed to measure the heat transfer coefficient at many points underneath individual bubbles during boiling as a function of space and time. This heater array enables the local heat transfer from a surface during the bubble growth and departure process to be measured with very high temporal and spatial resolution, and should allow better understanding of the boiling heat transfer mechanisms by pin-pointing when and where in the bubble departure cycle large amounts of wall heat transfer occur. Such information can provide much needed data regarding the important heat transfer mechanisms during the bubble departure cycle, and can serve as benchmarks to validate many of the analytical and numerical models used to simulate boiling. The improvements to the heater array include using a silicon-on-quartz substrate to reduce thermal cross-talk between the heaters, decreased space between the heaters, increased pad sizes on the heaters, and progressive heater sizes. Some results using the present heater array are discussed.

Kim, Jungho↗

NASA NTRS1959

Preliminary Study of a Piston Pump for Cryogenic Fluids

Preliminary data are presented covering the performance of a low-speed, five-cylinder piston pump designed for handling boiling hydrogen. This pump was designed for a flow of 55 gallons per minute at 240 rpm with a discharge pressure of 135 pounds per square inch. Tests were made using JP-4 fuel, liquid nitrogen, and liquid hydrogen. Pump delivery and endurance characteristics were satisfactory for the range of operation covered. In connection with the foregoing pump development, the cavitation characteristics of a preliminary visual model, glass-cylinder pump and of a simple reciprocating disk were studied. Subcooling of approximately 0.60 F was obtained from the cavitation produced by reciprocating a disk in boiling nitrogen and in boiling water. The subcooling obtained in a similar manner with liquid hydrogen was somewhat less.

Biermann, Arnold E.↗

NASA NTRS2002

Multipurpose Thermal Insulation Test Apparatus

A multi-purpose thermal insulation test apparatus is used for testing insulation materials, or other components. The test apparatus is a fluid boil-off calorimeter system for calibrated measurement of the apparent thermal conductivity (k-value) of a specimen material at a fixed vacuum level. The apparatus includes an inner vessel for receiving a fluid with a normal boiling point below ambient temperature, such as liquid nitrogen, enclosed within a vacuum chamber. A cold mass assembly, including the inner vessel and thermal guards, is suspended from the top of the vacuum chamber. Handling tools attach to the cold mass assembly for convenient manipulation of the assembly and for the installation or wrapping of insulation test materials. Liquid nitrogen is typically supplied to the inner vessel using a fill tube with funnel. A single port through the top of the vacuum chamber facilitates both filling and venting. Aerogel composite stacks with reflective films are fastened to the top and the bottom of the inner vessel as thermal guards. The comparative k-value of the insulation material is determined by measuring the boil-off flow rate of gas, the temperature differential across the insulation thickness, and the dimensions (length and diameters) of the test specimen.

Fesmire, James E.↗

NASA NTRS1999

Design of Transpiration Cooled Thermal Protection Systems

This study explored three approaches for the utilization of transpiration cooling in thermal protection systems. One model uses an impermeable wall with boiling water heat transfer at the backface (Model I). A second model uses a permeable wall with a boiling water backface and additional heat transfer to the water vapor as it flows in channels toward the exposed surface (Model II). The third model also uses a permeable wall, but maintains a boiling condition at the exposed surface of the material (Model III). The governing equations for the models were developed in non-dimensional form and a comprehensive parametric investigation of the effects of the independent variables on the important dependent variables was performed. In addition, detailed analyses were performed for selected materials to evaluate the practical limitations of the results of the parametric study.

Callens, E. Eugene, Jr.↗

NASA NTRS1994

A comparison of iron extraction methods for the determination of degree of pyritisation and the recognition of iron-limited pyrite formation

Measurements of degree of pyritisation require an estimate of sediment iron which is capable of reaction with dissolved sulphide to form pyrite, either directly or indirectly via iron monosulphide precursors. Three dissolution techniques (buffered dithionite, cold 1 M HCl, boiling 12 M HCl) were examined for their capacity to extract iron from a variety of iron minerals, and iron-bearing sediments, as a function of different extraction times and different grain sizes. All the iron oxides studied are quantitatively extracted by dithionite and boiling HCl (but not by cold HCl). Both HCl techniques extract more iron from silicates than does dithionite but probably about the same amounts as are potentially capable of sulphidation. Modern sediment studies indicate that most sedimentary pyrite is formed rapidly from iron oxides, with smaller amounts formed more slowly from iron silicates (if sufficient geologic time is available). It is therefore recommended that the degree of pyritisation be defined with respect to the dithionite-extractable (mainly iron oxide) pool and/or the boiling HCl-extractable pool (which includes some silicate iron) for the recognition of iron-limited pyritisation.

NASA Discipline Exobiology↗

NASA NTRS2001

Growth and Morphology of Supercritical Fluids, a Fluid Physics Experiment Conducted on Mir, Complete

The Growth and Morphology of Supercritical Fluids (GMSF) is an international experiment facilitated by the NASA Glenn Research Center and under the guidance of U.S. principal investor Professor Hegseth of the University of New Orleans and three French coinvestigators: Daniel Beysens, Yves Garrabos, and Carole Chabot. The GMSF experiments were concluded in early 1999 on the Russian space station Mir. The experiments spanned the three science themes of near-critical phase separation rates, interface dynamics in near-critical boiling, and measurement of the spectrum of density fluctuation length scales very close to the critical point. The fluids used were pure CO2 or SF6. Three of the five thermostats used could adjust the sample volume with the scheduled crew time. Such a volume adjustment enabled variable sample densities around the critical density as well as pressure steps (as distinct from the usual temperature steps) applied to the sample. The French-built ALICE II facility was used for these experiments. It allows tightly thermostated (left photograph) samples (right photograph) to be controlled and viewed/measured. Its diagnostics include interferometry, shadowgraph, high-speed pressure measurements, and microscopy. Data were logged on DAT tapes, and PCMCIA cards and were returned to Earth only after the mission was over. The ground-breaking near critical boiling experiment has yielded the most results with a paper published in Physical Review Letters (ref. 1). The boiling work also received press in Science Magazine (ref. 2). This work showed that, in very compressible near-critical two-phase pure fluids, a vapor bubble was induced to temporarily overheat during a rapid heating of the sample wall. The temperature rise in the vapor was 23-percent higher than the rise in the driving container wall. The effect is due to adiabatic compression of the vapor bubble by the rapid expansion of fluid near the boundary during heatup. Thermal diffusivity is low near the critical point, so getting heat out of the compressed bubble is observably slow. This gives the appearance of a backward heat flow, or heat flow from a cold surface to a warm fluid.

Wilkinson, R. Allen↗

NASA NTRS2008

Active Co-Storage of Cryogenic Propellants for Lunar Explortation

Long-term storage of cryogenic propellants is a critical requirement for NASA's effort to return to the moon. Liquid hydrogen and liquid oxygen provide the highest specific impulse of any practical chemical propulsion system, and thus provides the greatest payload mass per unit of launch mass. Future manned missions will require vehicles with the flexibility to remain in orbit for months, necessitating long-term storage of these cryogenic liquids. For decades cryogenic scientific satellites have used dual cryogens with different temperatures to cool instruments. This technology utilizes a higher temperature cryogen to provide a stage that efficiently intercepts a large fraction of the heat that would otherwise be incident on the lower temperature cryogen. This interception reduces the boil-off of the lower temperature cryogen and increasing the overall life-time of the mission. The Active Co-Storage concept is implemented similarly; the 101 K liquid oxygen thermally shields the 24 K liquid hydrogen. A thermal radiation shield that is linked to the liquid oxygen tank shrouds the liquid hydrogen tank, thereby preventing the liquid hydrogen tank from being directly exposed to the 300 K external environment. Modern cryocooler technology can eliminate the liquid oxygen boil-off and also cool the thermal radiation shield thereby reducing the liquid hydrogen boil-off to a small fraction of the unshielded rate. The thermal radiation shield can be a simple conductive shroud or a more sophisticated but lighter Broad Area Cooling (BAC) shroud. The paper describes the design impact of an active co-storage system for the Altair Descent Vehicle. This paper also compares the spacecraft-level impacts of the conductive shroud and the BAC shroud active co-storage concepts with a passive storage option in the context of the different scales of spacecraft that will be used for the lunar exploration effort - the Altair Ascent and Descent Vehicles, the Orion, and the Ares V Earth Departure Stage. The paper also reports on a subscale test of this active co-storage configuration. The test tank is 0.7 m in diameter, approximately one-third the dimension of tanks that would be needed in a lunar ascent module. A thin-walled fiberglass skirt supports and isolates the tank from a 100 K stage. A similar thin-walled skirt supports the lOOK stage from the ambient temperature structure. An aluminum shield with a heavy MLI blanket surrounds the tank and is attached at the 100 K stage. In this initial phase of the project, there is no tank on the 100 K stage, but it is actively cooled by a single-stage cryocooler similar in design to the one used on the RHESSI mission. The test configuration includes a number of innovative elements, including a helical support heat exchanger and an external thermodynamic vent/heat interception system. To avoid the complexity of an explosive gas handling system, testing will be done with liquid helium and liquid neon as simulant fluids. The properties of these fluids bracket the properties of liquid hydrogen. Instrumentation allows tank temperature and shield temperature profiles, tank liquid levels, and pressure drops through the flow lines, to be measured.

Mustafi, S.↗

NASA NTRS2009

Gauging Systems Monitor Cryogenic Liquids

Rocket fuel needs to stay cool - super cool, in fact. The ability to store gas propellants like liquid hydrogen and oxygen at cryogenic temperatures (below -243 F) is crucial for space missions in order to reduce their volumes and allow their storage in smaller (and therefore, less costly) tanks. The Agency has used these cryogenic fluids for vehicle propellants, reactants, and life support systems since 1962 with the Centaur upper stage rocket, which was powered with liquid oxygen and liquid hydrogen. During proposed long-duration missions, super-cooled fluids will also be used in space power systems, spaceports, and lunar habitation systems. In the next generation of launch vehicles, gaseous propellants will be cooled to and stored for extended periods at even colder temperatures than currently employed via a process called densification. Densification sub-cools liquids to temperatures even closer to absolute zero (-459 F), increasing the fluid s density and shrinking its volume beyond common cryogenics. Sub-cooling cryogenic liquid hydrogen, for instance, from 20 K (-423 F) to 15 K (-432.4 F) reduces its mass by 10 percent. These densified liquid gases can provide more cost savings from reduced payload volume. In order to benefit from this cost savings, the Agency is working with private industry to prevent evaporation, leakage, and other inadvertent loss of liquids and gases in payloads - requiring new cryogenic systems to prevent 98 percent (or more) of boil-off loss. Boil-off occurs when cryogenic or densified liquids evaporate, and is a concern during launch pad holds. Accurate sensing of propellants aboard space vehicles is also critical for proper engine shutdown and re-ignition after launch, and zero boil-off fuel systems are also in development for the Altair lunar lander.

Source record↗

NASA NTRS2010

Insulation-Testing Cryostat With Lifting Mechanism

The figure depicts selected aspects of an apparatus for testing thermal-insulation materials for cryogenic systems at temperatures and under vacuum or atmospheric conditions representative of those encountered in use. This apparatus, called "Cryostat-100," is based on the established cryogen-boil-off calorimeter method, according to which the amount of heat that passes through an insulation specimen to a cryogenic fluid in a container, and thus the effective thermal conductance of the specimen, is taken to be proportional to the amount of the cryogenic fluid that boils off from the container. The design of Cryostat-100 is based partly on, and incorporates improvements over, the design of a similar prior apparatus called "Cryostat-1" described in "Improved Methods of Testing Cryogenic Insulation Materials" (KSC-12107 & KSC- 12108), NASA Tech Briefs, Vol. 24, No. 12 (December 2000), page 46. The design of Cryostat-100 also incorporates the best features of two other similar prior apparatuses called "Cryostat-2" (also described in the cited prior article) and "Cryostat- 4." Notable among the improvements in Cryostat-100 is the addition of a lifting mechanism that enables safe, rapid, reliable insertion and removal of insulation specimens and facilitates maintenance operations that involve lifting. As in Cryostat-1, the cold mass is a vertical stainless-steel cylindrical vessel subdivided into a larger measurement vessel with smaller thermal-guard vessels at both ends. During operation, all three vessels are kept filled with liquid nitrogen near saturation at ambient pressure (temperature .77.4 K). The cold mass of Cryostat-100 has a length of 1 m and diameter of 168 mm. Each specimen has a corresponding nominal length and inner diameter and a nominal thickness of 25.4 mm. Specimens that are shorter and have thicknesses between 0 and 50 mm are also acceptable. Bulk-fill, foam, clam-shell, multilayer insulation, and layered materials can be tested over a very wide range of thermal transmission: apparent thermal conductivity from 0.01 to 60 mW/m-K and heat flux from 0.1 to 500 W/sq m. A test in Cryostat-100 can be conducted at any desired gas pressure between ambient atmospheric pressure at one extreme and a vacuum with residual pressure <10(exp -5) torr (<1.33 10(exp -3) Pa) at the other extreme. The residual gas (and purge gas) is typically nitrogen, but can be any suitable purge gas (e.g., helium, argon, or carbon dioxide). Usually, the temperature on the warm boundary of the insulation specimen is maintained near the ambient value (approximately 293 K), while the boiling of liquid nitrogen at atmospheric pressure in the cold mass maintains the temperature on the cold boundary of the specimen at approximately 77 K.

Fesmire, James↗

NASA NTRS2010

Cryogenic Fluid Management Technology for Moon and Mars Missions

In support of the U.S. Space Exploration Policy, focused cryogenic fluid management technology efforts are underway within the National Aeronautics and Space Administration. Under the auspices of the Exploration Technology Development Program, cryogenic fluid management technology efforts are being conducted by the Cryogenic Fluid Management Project. Cryogenic Fluid Management Project objectives are to develop storage, transfer, and handling technologies for cryogens to support high performance demands of lunar, and ultimately, Mars missions in the application areas of propulsion, surface systems, and Earth-based ground operations. The targeted use of cryogens and cryogenic technologies for these application areas is anticipated to significantly reduce propellant launch mass and required on-orbit margins, to reduce and even eliminate storage tank boil-off losses for long term missions, to economize ground pad storage and transfer operations, and to expand operational and architectural operations at destination. This paper organizes Cryogenic Fluid Management Project technology efforts according to Exploration Architecture target areas, and discusses the scope of trade studies, analytical modeling, and test efforts presently underway, as well as future plans, to address those target areas. The target areas are: liquid methane/liquid oxygen for propelling the Altair Lander Ascent Stage, liquid hydrogen/liquid oxygen for propelling the Altair Lander Descent Stage and Ares V Earth Departure Stage, liquefaction, zero boil-off, and propellant scavenging for Lunar Surface Systems, cold helium and zero boil-off technologies for Earth-Based Ground Operations, and architecture definition studies for long term storage and on-orbit transfer and pressurization of LH2, cryogenic Mars landing and ascent vehicles, and cryogenic production via in situ resource utilization on Mars.

Doherty, Michael P.↗

NASA NTRS2003

Electric Field Effect on Bubble Detachment in Variable Gravity Environment

The subject of the present study, the process of bubble detachment from an orifice in a plane surface, shows some resemblance to bubble departure in boiling. Because of the high heat transfer coefficients associated with phase change processes, boiling is utilized in many industrial operations and is an attractive solution to cooling problems in aerospace engineering. In terrestrial conditions, buoyancy is responsible for bubble removal from the surface. In space, the gravity level being orders of magnitude smaller than on earth, bubbles formed during boiling remain attached at the surface. As a result, the amount of heat removed from the heated surface can decrease considerably. The use of electric fields is proposed to control bubble behavior and help bubble removal from the surface on which they form. The objective of the study is to investigate the behavior of individual air bubbles injected through an orifice into an electrically insulating liquid under the influence of a static electric field. Bubble cycle life were visualized in terrestrial conditions and for several reduced gravity levels. Bubble volume, dimensions and contact angle at detachment were measured and analyzed for different parameters as gravity level and electric field magnitude. Situations were considered with uniform or non-uni form electric field. Results show that these parameters significantly affect bubble behavior, shape, volume and dimensions.

Iacona, Estelle↗

NASA NTRS2005

Apparatus for Testing Flat Specimens of Thermal Insulation

An apparatus has been developed to implement an improved method of testing flat-plate specimens of thermal-insulation materials for cryogenic application. The method includes testing under realistic use conditions that could include vacuum and mechanical loading at a pressure up to 70 psi (=0.48 MPa). The apparatus can accommodate a rigid or flexible specimen having thickness up to 1.25 in. (=3.2 cm) and diameters between 6 and 10 in. (about 15.2 and 25.4 cm, respectively). Typical test conditions include boundary temperatures between 77 K and 373 K and vacuum/interstitial gas filling at a pressure between 10(exp -6) torr (=1.3 x 10(exp -4) Pa) and 760 torr (atmospheric pressure =0.1 MPa). The interstitial gas could be N2, He, CO2, or any other suitable gas to which the insulation is expected to be exposed in use. Relative to prior apparatuses and testing methods, this apparatus and the testing method that it implements offer advantages of relative simplicity and ease of use. The basic principle of operation of the apparatus is that of boil-off calorimetry, using liquid nitrogen or any other suitable liquid that boils at a desired temperature below ambient temperature. Comparative rates of flow of heat through the thicknesses of the specimens (heat-leak rates) and apparent-thermal-conductivity values are obtained from tests of specimens. Absolute values of heat-leak rates and apparent thermal conductivities are computed from a combination of (1) the aforementioned comparative values and (2) calibration factors obtained by testing reference specimens of materials that have known thermal-insulation properties. The apparatus includes a full complement of temperature sensors, a vacuum pump and chamber, a monitoring and control system, and tools and fixtures that enable rapid and reliable installation and removal of specimens. A specimen is installed at the bottom of the vacuum chamber, and a cold-mass assembly that includes a tank is lowered into position above and around the specimen (see figure). A spring-based compensating fixture helps to ensure adequate thermal contact with possibly irregular specimen surfaces. For a high-compression test, the springs can be replaced with spacers. A flat circular load cell at the bottom of the chamber measures the compressive load on the specimen. Once the desired compressive-load, temperature, and vacuum/gas-filling conditions are established, testing begins. During a test, all measurements are recorded by use of a portable data-acquisition system and a computer. The total heat-leak rate is measured and calculated as the boil-off flow rate multiplied by the latent heat of vaporization. The parasitic heat leak (to the side of the specimen and to the top and side of the cold-mass tank) is reduced to a small fraction of the total heat leak by use of a combination of multilayer-insulation (MLI) shield rings, reflective film, a fiberglass/epoxy centering ring, and a bulk fill of aerogel beads. This combination eliminates the need for a cryogenic guard chamber used in a typical prior apparatus to reduce the parasitic heat leak.

Fesmire, James E.↗

NASA NTRS2011

An Active Broad Area Cooling Model of a Cryogenic Propellant Tank with a Single Stage Reverse Turbo-Brayton Cycle Cryocooler

As focus shifts towards long-duration space exploration missions, an increased interest in active thermal control of cryogenic propellants to achieve zero boil-off of cryogens has emerged. An active thermal control concept of considerable merit is the integration of a broad area cooling system for a cryogenic propellant tank with a combined cryocooler and circulator system that can be used to reduce or even eliminate liquid cryogen boil-off. One prospective cryocooler and circulator combination is the reverse turbo-Brayton cycle cryocooler. This system is unique in that it has the ability to both cool and circulate the coolant gas efficiently in the same loop as the broad area cooling lines, allowing for a single cooling gas loop, with the primary heat rejection occurring by way of a radiator and/or aftercooler. Currently few modeling tools exist that can size and characterize an integrated reverse turbo-Brayton cycle cryocooler in combination with a broad area cooling design. This paper addresses efforts to create such a tool to assist in gaining a broader understanding of these systems, and investigate their performance in potential space missions. The model uses conventional engineering and thermodynamic relationships to predict the preliminary design parameters, including input power requirements, pressure drops, flow rate, cycle performance, cooling lift, broad area cooler line sizing, and component operating temperatures and pressures given the cooling load operating temperature, heat rejection temperature, compressor inlet pressure, compressor rotational speed, and cryogenic tank geometry. In addition, the model allows for the preliminary design analysis of the broad area cooling tubing, to determine the effect of tube sizing on the reverse turbo-Brayton cycle system performance. At the time this paper was written, the model was verified to match existing theoretical documentation within a reasonable margin. While further experimental data is needed for full validation, this tool has already made significant steps towards giving a clearer understanding of the performance of a reverse turbo-Brayton cycle cryocooler integrated with broad area cooling technology for zero boil-off active thermal control.

Guzik, Monica C.↗

NASA NTRS2012

Measuring Air Leaks into the Vacuum Space of Large Liquid Hydrogen Tanks

Large cryogenic liquid hydrogen tanks are composed of inner and outer shells. The outer shell is exposed to the ambient environment while the inner shell holds the liquid hydrogen. The region between these two shells is evacuated and typically filled with a powderlike insulation to minimize radiative coupling between the two shells. A technique was developed for detecting the presence of an air leak from the outside environment into this evacuated region. These tanks are roughly 70 ft (approx. equal 21 m) in diameter (outer shell) and the inner shell is roughly 62 ft (approx. equal 19 m) in diameter, so the evacuated region is about 4 ft (approx. equal 1 m) wide. A small leak's primary effect is to increase the boil-off of the tank. It was preferable to install a more accurate fill level sensor than to implement a boil-off meter. The fill level sensor would be composed of an accurate pair of pressure transducers that would essentially weigh the remaining liquid hydrogen. This upgrade, allowing boil-off data to be obtained weekly instead of over several months, is ongoing, and will then provide a relatively rapid indication of the presence of a leak.

Youngquist, Robert↗

NASA NTRS2013

Experimental Investigation of Flow Condensation in Microgravity

Future manned missions to Mars are expected to greatly increase the space vehicle's size, weight, and heat dissipation requirements. An effective means to reducing both size and weight is to replace single-phase thermal management systems with two-phase counterparts that capitalize upon both latent and sensible heat of the coolant rather than sensible heat alone. This shift is expected to yield orders of magnitude enhancements in flow boiling and condensation heat transfer coefficients. A major challenge to this shift is a lack of reliable tools for accurate prediction of two-phase pressure drop and heat transfer coefficient in reduced gravity. Developing such tools will require a sophisticated experimental facility to enable investigators to perform both flow boiling and condensation experiments in microgravity in pursuit of reliable databases. This study will discuss the development of the Flow Boiling and Condensation Experiment (FBCE) for the International Space Station (ISS), which was initiated in 2012 in collaboration between Purdue University and NASA Glenn Research Center. This facility was recently tested in parabolic flight to acquire condensation data for FC-72 in microgravity, aided by high-speed video analysis of interfacial structure of the condensation film. The condensation is achieved by rejecting heat to a counter flow of water, and experiments were performed at different mass velocities of FC-72 and water and different FC-72 inlet qualities. It is shown that the film flow varies from smooth-laminar to wavy-laminar and ultimately turbulent with increasing FC-72 mass velocity. The heat transfer coefficient is highest near the inlet of the condensation tube, where the film is thinnest, and decreases monotonically along the tube, except for high FC-72 mass velocities, where the heat transfer coefficient is enhanced downstream. This enhancement is attributed to both turbulence and increased interfacial waviness. One-ge correlations are shown to predict the average condensation heat transfer coefficient with varying degrees of success, and a recent correlation is identified for its superior predictive capability, evidenced by a mean absolute error of 21.7%.

microgravity↗

NASA NTRS2015

Numerical Simulation of Liquid Nitrogen Chilldown of a Vertical Tube

This paper presents the results of a one-dimensional numerical simulation of the transient chilldown of a vertical stainless steel tube with liquid nitrogen. The direction of flow is downward (with gravity) through the tube. Heat transfer correlations for film, transition, and nucleate boiling, as well as critical heat flux, rewetting temperature, and the temperature at the onset of nucleate boiling were used to model the convection to the tube wall. Chilldown curves from the simulations were compared with data from 55 recent liquid nitrogen chilldown experiments. With these new correlations the simulation is able to predict the time to rewetting temperature and time to onset of nucleate boiling to within 25% for mass fluxes ranging from 61.2 to 1150 kg/(sq m s), inlet pressures from 175 to 817 kPa, and subcooled inlet temperatures from 0 to 14 K below the saturation temperature.

GFSSP↗

NASA NTRS2015

Cryogenic Fluid Management Technology Development for Nuclear Thermal Propulsion

The purpose of this paper is to investigate, facilitate a discussion and determine a path forward for technology development of cryogenic fluid management technology that is necessary for long duration deep space missions utilizing nuclear thermal propulsion systems. There are a number of challenges in managing cryogenic liquids that must be addressed before long durations missions into deep space, such as a trip to Mars can be successful. The leakage rate of hydrogen from pressure vessels, seals, lines and valves is a critical factor that must be controlled and minimized. For long duration missions, hydrogen leakage amounts to large increases in hydrogen and therefore vehicle mass. The size of a deep space vehicle, such as a mars transfer vehicle, must be kept small to control cost and the logistics of a multi launch, assembled in orbit vehicle. The boil off control of the cryogenic fluid is an additional obstacle to long duration missions. The boil off caused by heat absorption results in the growth of the propellant needs of the vehicle and therefore vehicle mass. This is a significant problem for a vehicle using nuclear (fission) propulsion systems. Radiation from the engines deposits large quantities of heat into the cryogenic fluid, greatly increasing boil off beyond that caused by environmental heat leakage. Addressing and resolving these challenges is critical to successful long duration space exploration. This paper discusses the state of the technology needed to address these challenges and discuss the path forward needed in technology development.

Taylor, Brian↗

NASA NTRS2016

Development of Advanced ISS-WPA Catalysts for Organic Oxidation at Reduced Pressure/Temperature

The Water Processor Assembly (WPA) at International Space Station (ISS) processes a waste stream via multi-filtration beds, where inorganic and non-volatile organic contaminants are removed, and a catalytic reactor, where low molecular weight organics not removed by the adsorption process are oxidized at elevated pressure in the presence of oxygen and elevated temperature above the normal water boiling point. Operation at an elevated pressure requires a more complex system design compared to a reactor that could operate at ambient pressure. However, catalysts currently available have insufficient activity to achieve complete oxidation of the organic load at a temperature less than the water boiling point and ambient pressure. Therefore, it is highly desirable to develop a more active and efficient catalyst at ambient pressure and a moderate temperature that is less than water boiling temperature. This paper describes our efforts in developing high efficiency water processing catalysts. Different catalyst support structures and coating metals were investigated in subscale reactors and results were compared against the flight WPA catalyst. Detailed improvements achieved on alternate metal catalysts at ambient pressure and 200 F will also be presented in the paper.

Yu, Ping↗