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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 721 records · Page 40
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Incommensurate magnetic orders and topological Hall effect in the square-net centrosymmetric EuGa 2 Al 2 system

Neutron diffraction on the centrosymmetric square-net magnet EuGa 2 Al 2 reveals multiple incommensurate magnetic states (AFM1, 2, 3) in zero field. In applied field, a new magnetic phase (A) is identified from magnetization and transport measurements, bounded by two of the μ 0 H=0 incommensurate magnetic phases (AFM1, helical, and AFM3, cycloidal) with different moment orientations. Moreover, magnetotransport measurements indicate the presence of a topological Hall effect, with maximum values centered in the A phase. Together, these results render EuGa 2 Al 2 a material with noncoplanar or topological spin texture in applied field. X-ray diffraction reveals an out-of-plane (OOP) charge density wave (CDW) below T CDW ~50 K while the magnetic propagation vector lies in plane below T N =19.5 K. Together these data point to a new route to realizing in-plane noncollinear spin textures through an OOP CDW. In turn, these noncollinear spin textures may be unstable against the formation of topological spin textures in an applied field.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Epitaxial growth of hexagonal BaNi O 3–δ thin films on SrTi O 3 (111) substrates

Transition metal oxides containing nickel species in oxidation states higher than 3+ often exhibit high catalytic activity, which makes them promising for applications as advanced electrocatalysts for water splitting and fuel cells. Here, we examine the structure and properties of BaNiO 3 (BNO) thin films, containing formally Ni 4+ , grown on SrTiO 3 (111) substrates using oxygen-plasma–assisted molecular beam epitaxy. X-ray diffraction and scanning transmission electron microscopy measurements reveal that BNO films have a hexagonal structure with $c$- and $a$-axes of mixed textures showing epitaxial relationships BNO (0001) ∥ SrTiO 3 (111) and BNO (10$\overline{1}$0) ∥ SrTi O 3 (111), respectively. The formation of the $a$-axis texture is dominant due to the smaller lattice mismatch with the substrate. Here, density functional theory calculations confirm that the hexagonal BNO film with the $a$-axis texture is energetically more favorable than the competing $c$-axis texture. Detailed spectroscopy data analysis indicates that hexagonal BNO films contain mixtures of Ni 2+ , Ni 3+ , and Ni 4+ species, with Ni 4+ being dominant. Our study provides insights into stabilizing Ni 4+ in complex oxides, which is important for further exploration of the potential of materials containing Ni 4+ .

36 MATERIALS SCIENCE↗
DOE OSTI2024

Differential Organic Carbon Mineralization Responses to Soil Moisture in Three Different Soil Orders Under Mixed Forested System: Supporting Data

This data contains data from 90-day long incubation study which aimed to look at the soil moisture-texture relationship on soil organic carbon (SOC) cycling. Soils were collected from three distinct soil textures from mixed forests in 2017: sandy (Georgia, 2017-05-01), loamy (Missouri, 2017-06-14) and clayey (Texas, December 2017) were incubated at different soil moisture levels (air-dried, 25% water holding capacity (WHC), 50% WHC, 100% WHC and 175% WHC) at room temperature for a period of 90 days. Files contain microbial respiration, active and slow SOC pools, and their respective mineralization rates, extractable organic carbon (C), and C-acquiring extracellular enzymes. Findings from these data were used in Singh et al. (2021). This study aimed to examine the interactive effect of soil moisture and texture on SOC mineralization. Soil samples of three distinct textures (sandy, loamy, and clayey) were collected from mixed forests of Georgia, Missouri, and Texas, respectively. Soil cores of 5 cm diameter were collected from numerous random locations at each site from 0-15 cm depth after scraping the litter layer and mixed thoroughly to obtain a composite sample per site. Three additional soil cores were collected to determine the WHC using pressure plate extractors. Soil samples were composited, and triplicate soil samples were incubated in mason jars for a period of 90 days at room temperature under different moisture regimes: air dried, 25% WHC, 50% WHC, at WHC and 100% saturation. Soil respiration was measured weekly, and destructive sampling was conducted at 1, 15, 60, and 90 days to determine extractable organic C, C acquiring enzyme activity, and active and slow SOC pools with their respective mineralization rates. The C acquiring enzyme activity was the total activity of α-glucosidase, β-glucosidase, cellobiohydrolase, and β-xylosidase enzymes. Gas samples for microbial respiration measurements were collected from headspace of incubation jars through the sampling ports on the lids and then analyzed using a Shimadzu Gas Chromatograph (GC-2014). Prior to sampling, the vials were evacuated. Blank correction was also done by collecting gas samples from empty incubation jars. Double pool exponential decay model was used in SigmaPlot to determine the active and slow SOC pools and their mineralization rates (Farrar et al., 2012; Jagadamma et al., 2014). The C-acquiring extracellular enzymes were measured using the microplate method by German et al., (2011). Microbial community structure was determined using the phospholipid fatty acid (PLFA) and neutral lipid fatty acid (NLFA) analyses (Buyer and Sasser, 2012). This dataset has seven data files provided in comma-separate (*.csv) format. Additional metadata are provided: seven data dictionaries and a file-level metadata file in comma separate (*.csv) format and a user guide in PDF (*.pdf) format.

Carbon acquiring enzyme activity↗
DOE OSTI2023

One-Pot Synthesis of Melamine Formaldehyde Resin-Derived N-Doped Porous Carbon for CO 2 Capture Application

The design and synthesis of porous carbons for CO 2 adsorption have attracted tremendous interest owing to the ever-soaring concerns regarding climate change and global warming. Herein, for the first time, nitrogen-rich porous carbon was prepared with chemical activation (KOH) of commercial melamine formaldehyde resin (MF) in a single step. It has been shown that the porosity parameters of the as-prepared carbons were successfully tuned by controlling the activating temperature and adjusting the amount of KOH. Thus, as-prepared N-rich porous carbon shows a large surface area of 1658 m 2 /g and a high N content of 16.07 wt%. Benefiting from the unique physical and textural features, the optimal sample depicted a CO 2 uptake of up to 4.95 and 3.30 mmol/g at 0 and 25 °C under 1 bar of pressure. More importantly, as-prepared adsorbents show great CO 2 selectivity over N 2 and outstanding recyclability, which was prominently important for CO 2 capture from the flue gases in practical application. An in-depth analysis illustrated that the synergetic effect of textural properties and surface nitrogen decoration mainly determined the CO 2 capture performance. However, the textural properties of carbons play a more important role than surface functionalities in deciding CO 2 uptake. In view of cost-effective synthesis, outstanding textural activity, and the high adsorption capacity together with good selectivity, this advanced approach becomes valid and convenient in fabricating a unique highly efficient N-rich carbon adsorbent for CO 2 uptake and separation from flue gases.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1973

Utilization of ERTS data to detect plant diseases and nutrient deficiencies, soil types and moisture levels

The author has identified the following significant results. Findings demonstrate the feasibility of delineating major terrain features, land uses, and crop species through computerized analyses. Channel 6 appears to give the most information for making separations of this type. By enlarging satellite imagery and visually comparing this with high altitude aerial photographs, locating small terrain features and cropland areas on satellite imagery is greatly facilitated. Forest types are discernable on the 2402 imagery with a #25 filter: pine stands have dark tones, hardwood stands have light tones, and pine-hardwood have intermediate tones. No textural differences are evident on this type of imagery. However, on the 2424 imagery with #89B filter, textural differences are evident but tonal differences are absent. Areas of considerable texture are interpreted as stands of high volume while areas of suppressed texture are of low volume. The 2402 imagery with a #57 filter appears to have little information of importance in timber inventory.

Parks, W. L.↗
NASA NTRS1974

Combined spectral and spatial processing of ERTS imagery data

A general procedure is presented for extracting textural properties of blocks of image data. These features are calculated in the spatial domain, taking into account the statistical nature of texture. The procedure is based on the assumption that the texture information in an image is contained in the overall or 'average' spatial relationship which the gray tones in the image have to one another. The spatial gray-tone dependence matrix is discussed together with the spectral features used in the study and the land use classification studies conducted. The results of the study show the usefulness of using both spectral and textural characteristics of ERTS multispectral scanner data for developing classification procedures.

Haralick, R. M.↗
NASA NTRS1976

Documentation of procedures for textural/spatial pattern recognition techniques

A C-130 aircraft was flown over the Sam Houston National Forest on March 21, 1973 at 10,000 feet altitude to collect multispectral scanner (MSS) data. Existing textural and spatial automatic processing techniques were used to classify the MSS imagery into specified timber categories. Several classification experiments were performed on this data using features selected from the spectral bands and a textural transform band. The results indicate that (1) spatial post-processing a classified image can cut the classification error to 1/2 or 1/3 of its initial value, (2) spatial post-processing the classified image using combined spectral and textural features produces a resulting image with less error than post-processing a classified image using only spectral features and (3) classification without spatial post processing using the combined spectral textural features tends to produce about the same error rate as a classification without spatial post processing using only spectral features.

Haralick, R. M.↗
NASA NTRS1982

Evaluation of left ventricular assist device pump bladders cast from ion-sputtered polytetrafluorethylene mandrels

A highly thromboresistant blood contacting interface for use in implanatable blood pump is investigated. Biomaterials mechanics, dynamics, durability, surface morphology, and chemistry are among the critical consideration pertinent to the choice of an appropriate blood pump bladder material. The use of transfer cast biopolymers from ion beam textured surfaces is investigated to detect subtle variations in blood pump surface morphology using Biomer as the biomaterial of choice. The efficacy of ion beam sputtering as an acceptable method of fabricating textured blood interfaces is evaluated. Aortic grafts and left ventricular assist devices were implanted in claves; the blood interfaces were fabricated by transfer casting methods from ion beam textured polytetrafluorethylene mandrels. The mandrels were textured by superimposing a 15 micron screen mesh; ion sputtering conditions were 300 volts beam energy, 40 to 50 mA beam, and a mandrel to source distance of 25 microns.

Source record↗
NASA NTRS1982

Combined use of remote sensing and seismic observations to infer geologically recent crustal deformation, active faulting, and stress fields

Characteristic traits for earthquakes associated with strike-slip motion in Central California and the Salton Sea area, as revealed in ground based studies and LANDSAT imagery, were compared. The mapped lineaments are found to be oriented in several dominant directions. One direction is the same as the trend of the San Andreas fault. The other directions differ from area to area and may reflect the stresses of earlier geologic processes. The pattern of lineament orientations is significantly LANDSAT MSS data, SEASAT synthetic aperture radar data, and magnetic field data from the South Mountain area west of Gettysburg, Pennsylvania were registered to match each other in spatial position and merged. Pattern recognition techniques were applied to the composite data set to determine its utility in recognizing different rock types and structures in vegetated terrain around South Mountain. With the use of a texture algorithm to enhance geologic features, a classification of the entire area was made. A test of the correlation between SAR tone and texture, LANDSAT tone and texture, and magnetic field data revealed no tone or texture measures linking any two of the original data sets.

Alexander, S. S.↗
NASA NTRS1983

Electron microscopic observations of hydrogen implantation in ilmenites

Hydrogen ion beams were found to form submicrometer, bumpy textures on the surface of ilmenite grains. From this effect, it is believed that similar bumpy textures seen on lunar ilmenite, pyroxene, and olivine grains are likely to be caused by solar wind irradiation. As a consequence, the concentration of bumpy textured grains may be a useful index of surface maturity for lunar soils. An attempt was made to search for grains with these bumpy textures in interplanetary dust and lunar and meteoritic regolith breccias in order to obtain information about the duration of their exposure to the solar wind. Solar wind irradiation was simulated on natural, terrestrial ilmenite. Hydrogen ion beams were directed at small grains and polished sections which were then examined by electron microscopy.

Blanford, G. E.↗
NASA NTRS1986

Carbon and carbon-coated electrodes for multistage depressed collectors for electron-beam devices - A technology review

Various aspects of carbon and carbon-coated multistaged depressed collector (MDC) electrode technology are reviewed. The physical properties of untreated graphite electrodes, ion-textured graphite electrodes, and textured, carbon-coated copper electrodes, and surface treatment procedures for these electrodes are described. The secondary electron emissions of the three electrode types are analyzed. MDC fabrication methods are discussed. The performances of MDCs fabricated with untreated graphite electrodes, ion-textured graphite electrodes, and textured, carbon-coated copper electrodes are evaluated. MDC and TWT efficiency levels for tubes fabricated with the three materials are measured.

Curren, Arthur N.↗
NASA NTRS1987

Petrology and precursors of lithic clasts from feldspathic fragmental breccia 67975

Textures and mineral chemistry (by INAA) of five lithic clasts, including both light green and light gray clasts, from feldspathic fragmental breccia 67975 were studied. The presence of five rock types was confirmed: feldspathic microporphyritic melt breccia, metamorphosed mafic-rich melt breccia with zoned and mantled clasts, 'typical' reequilibrated lunar feldspathic granulites with granoblastic texture and homogeneous mineral chemistry, hornfels, and a recrystallized mafic-rich granulite with relict igneous texture and the composition of a ferroan anorthositic norite. The mineralogy and textural data corroborate the grouping of the light green clasts proposed by Lindstrom (1984). However, the light gray clasts do not appear to be coherent in petrologic (or chemical) characteristics; one is a plagioclase-rich, possibly monomict rock with ferroan anorthositic precursor(s), and the other represents a mixture of feldspathic granulite and ferroan anorthositic norite lithologies.

Mcgee, James J.↗
NASA NTRS1987

Development of 8 cm x 8 cm silicon gridded back solar cell for space station

The 8-cm x 8-cm gridded back cell being developed for the space station photovoltaic array is described. Modeling studies show that the beginning of life power output of 1.039 W per cell may be met by several different configurations, the most promising being either a fielded or nonfielded 2 ohm-cm planar 8-mil cell. Experimental data are presented which show that a thermal alpha of 0.63 is achievable on a planar cell but at the expense of some Isc. Planar cells are found to possess short-circuit currents which are 9 percent lower than on textured cells due to the loss of near-IR radiation by transmission through the cell. Preliminary modeling shows that the efficiency of the textured cell exceeds the planar cell by approximately 9 percent at 25 C but the situation is reversed in orbit due to the high thermal alpha of textured cells (0.82). Experimental data show that the IR absorption in textured cells can be reduced by about 3 alpha points without loss of efficiency by controlling the doping concentration in the diffused layers, thus increasing the efficiency in orbit.

Lillington, D. R.↗
NASA NTRS1987

The visual control of simulated altitude

The ability of a subject flying an experimental flight to use the different sources of visual information by looking at the vertical tracking error was investigated using a 3 (altitude) x 3 (texture) x 2 (replication) factorial design. Each subject flew these 18 flights in the same partially counterbalanced order, constructed such that there was one flight at each of the three altitudes, and over each of the three surface textures within each successive set of three flights. The three ground-surface textures used consisted of meridian, latitudinal, and square textures described by Wolpert et al. (1983). The results showed that, in displays where only splay information was available, the subjects tended to confuse lateral motion with vertical.

Johnson, Walter W.↗
NASA NTRS1990

Aeolian removal of dust from radiator surfaces on Mars

Simulated radiator surfaces made of arc-textured Cu and Nb-1 percent-Zr and ion beam textured graphite and C-C composite were fabricated and their integrated spectral emittance characterized from 300 to 3000 K. A thin layer of aluminum oxide, basalt, or iron (III) oxide dust was then deposited on them, and they were subjected to low pressure winds in the Martian Surface Wind Tunnel. It was found that dust deposited on simulated radiator surfaces may or may not seriously lower their integrated spectral emittance, depending upon the characteristics of the dust. With Al2O3 there is no appreciable degradation of emittance on a dusted sample, with basaltic dust there is a 10 to 20 percent degradation, and with Fe2O3 a 20 to 40 percent degradation. It was also found that very high winds on dusted highly textured surfaces can result in their abrasion. Degradation in emittance due to abrasion was found to vary with radiator material. Arc-textured Cu and Nb-1 percent Zr was found to be more susceptible to emittance degradation than graphite or C-C composite. The most abrasion occurred at low angles, peaking at the 22.5 deg test samples.

Gaier, James R.↗
NASA NTRS1990

Formation conditions of pyroxene-olivine and magnesian olivine chondrules

Dynamic crystallization experiments performed on a Type I and an intermediate Type II/III composition demonstrate chondrule texture is controlled by the abundance of heterogeneous nuclei. This factor is controlled by the maximum initial temperature relative to the olivine disappearance temperature for the given heating time. Glassy and excentroradial textures form from superheated melts with no nuclei, and barred textures form with initial temperatures near the olivine disappearance temperature. Porphyritic and granular textures form with initial temperatures below the liquidus with abundant nuclei. Comparison of zoning characteristics of experimental olivines with those in natural porphyritic olivine chondrules indicates cooling rates of 100 to 1000 C/h, whereas olivine morphology indicates barred olivines cooled at rates of 250 to 1000 C/h. Texture/composition relationships suggest chondrules experienced initial temperatures below 1750 C. These observations are consistent with the idea that chondrules formed by transient heating in dust-rich regions (i.e., in the midplane) of the solar nebula.

Radomsky, Patrick M.↗
NASA NTRS1990

Temperature conditions for chondrule formation

An attempt is made to constrain the chondrule-forming process from dynamic crystallization experiments on chondrule analogs and from correlations between texture and bulk composition in natural chondrules. Liquidus temperatures for chondrules from unequilibrated chondrites are calculated using Herzberg's (1979) method. The paper then infers whether each chondrule formed above, at, or below its liquidus based on textures produced in experiments. A range of temperatures to which chondrules may have been initially heated is then derived from the texture-composition-temperature relationships. Finally, the role of dust seeding, or external heterogeneous nucleation, in producing chondrule textures is examined.

Hewins, Roger H.↗
NASA NTRS1990

High emittance surfaces for high temperature space radiator applications

Surface modification techniques are evaluated for emittance enhancement of radiator surfaces. These techniques include acid etching, heat treating, abrasion, sputter texturing, electrochemical texturing, arc texturing, and atomic oxygen beam texturing. Candidate radiator surface materials under consideration include Nb-1 pct Zr, Cu, Ti, Ti-6 pct Al-4 pct V, 304 stainless steel, Al6061-T6, Mo, W, and Ta.

Banks, Bruce A.↗