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NASA NTRS1988

A sintering model for SiC(sub)w/Si3N4 composites

Presented is a model which suggests that it should be possible to pressureless sinter a SiC(sub w)/ Si3N4 composite to theoretical density. Prior failure to achieve complete densification by sintering is attributed to the use of compositions which result in a glass deficit. There is one basic premise for this model. The ratio of glass amount to surface area of nonglass constituents must be the same for both composite and sinterable monolithic Si3N4. This model suggests that whisker and grain sizes and whisker loading influence the glass amount necessary for successful sintering of composites. According to the model, a large glass amount will be necessary for successful sintering of these composites. However, grain boundary thicknesses in the composite will be less than those in the analogous monolithic materials. This suggests that good high temperature strength may still be attained. A recent report supports the predictions of the model.

Freedman, Marc R.↗

NASA NTRS2008

Nb(x)Ti(1-x)N Superconducting-Nanowire Single-Photon Detectors

Superconducting-nanowire singlephoton detectors (SNSPDs) in which Nb(x)Ti(1-x)N (where x<1) films serve as the superconducting materials have shown promise as superior alternatives to previously developed SNSPDs in which NbN films serve as the superconducting materials. SNSPDs have potential utility in optical communications and quantum cryptography. Nb(x)Ti(1-x)N is a solid solution of NbN and TiN, and has many properties similar to those of NbN. It has been found to be generally easier to stabilize NbxTi1 xN in the high-superconducting-transitiontemperature phase than it is to so stabilize NbN. In addition, the resistivity and penetration depth of polycrystalline films of Nb(x)Ti(1-x)N have been found to be much smaller than those of films of NbN. These differences have been hypothesized to be attributable to better coupling at grain boundaries within Nb(x)Ti(1-x)N films.

Stem, Jeffrey A.↗

NASA NTRS1989

Fatigue crack growth in a unidirectional SCS-6/Ti-15-3 composite

An investigation was conducted to characterize and model the fatigue crack growth (FCG) behavior of a SCS-6/Ti-15-3 metal matrix composite. Part of the study was conducted using a fatigue loading stage mounted inside a scanning electron microscope (SEM). This unique facility allowed high magnification viewing of the composite fatigue processes and measurement of the near crack tip displacements. The unidirectional composite was tested in the (0)8 (i.e., longitudinal) and (90)8 (i.e., transverse) orientations. For comparison purposes unreinforced matrix material produced by the identical process as the reinforced material was also tested. The results of the study reveal that the fatigue crack growth behavior of the composite is a function of specimen geometry, fiber orientation and the interaction of local stress fields with the highly anisotropic composite. In the case of (0)8 oriented single edge notch (SEN) specimens and (90)8 oriented compact tension (CT) specimens, the crack growth was normal to the loading direction. However, for the (0)8 CT specimens the crack grew mostly parallel to the loading and the fiber direction. The unusual fatigue behavior of the (0)8 CT specimens was attributed to the specimen geometry and the associated high tensile bending stresses perpendicular to the fiber direction. These stresses resulted in preferential cracking in the weak interface region perpendicular to the fiber direction. The interface region, and in particular the carbon coating surrounding the fiber proved to be the composites weakest link. In the (0)8 SEN the crack growth was confined to the matrix leaving behind unbroken fibers which bridged the cracked surfaces. As the crack grew longer, more fibers bridged the crack resulting in a progressive decrease in the crack growth rates and eventual crack arrest. The actual near crack tip displacement measurements were used in a proposed formulation for a bridging-corrected effective crack driving force, delta K(sub eff). This parameter was able to account for most of the experienced bridging and correlated the (0)8 SEN fatigue crack growth data reasonably well.

Kantzos, Peter↗

NASA NTRS2022

Compositional Measurements of Saturn's Upper Atmosphere and Rings From Cassini INMS: An Extended Analysis of Measurements From Cassini's Grand Finale Orbits

The Cassini spacecraft's final orbits sampled Saturn's atmosphere and returned surprisingly complex mass spectra from the Ion and Neutral Mass Spectrometer (INMS). Signal returned from the instrument included native Saturn species, as expected, as well as a significant amount of signal attributed to vaporized ices and higher mass organics believed to be owing into Saturn's atmosphere from the rings. In this paper, we present an in-depth compositional analysis of the mass spectra returned from Cassini's last few orbits. We use a mass spectral deconvolution algorithm designed specifically to handle the complexities involved with unit resolution spaceflight mass spectrometry data to determine the relative abundance of species detected in the observations. We calculate the downward external flux and mass deposition rates of ring volatile species into Saturn's atmosphere and conclude that during these observations ring material was being deposited into Saturn's equatorial region at a rate on the order of 10(exp 4) kg/s.

Saturn↗

NASA NTRS2022

Compositional Measurements of Saturn's Upper Atmosphere and Rings From Cassini INMS: An Extended Analysis of Measurements From Cassini's Grand Finale Orbits

The Cassini spacecraft's final orbits sampled Saturn's atmosphere and returned surprisingly complex mass spectra from the Ion and Neutral Mass Spectrometer (INMS). Signal returned from the instrument included native Saturn species, as expected, as well as a significant amount of signal attributed to vaporized ices and higher mass organics believed to be flowing into Saturn's atmosphere from the rings. In this paper, we present an in-depth compositional analysis of the mass spectra returned from Cassini's last few orbits. We use a mass spectral deconvolution algorithm designed specifically to handle the complexities involved with unit resolution spaceflight mass spectrometry data to determine the relative abundance of species detected in the observations. We calculate the downward external flux and mass deposition rates of ring volatile species into Saturn's atmosphere and conclude that during these observations ring material was being deposited into Saturn's equatorial region at a rate on the order of 10(exp 4) kg/s.

Saturn↗

NASA NTRS2020

Solution of the Nonlinear High-Fidelity Generalized Method of Cells Micromechanics Relations via Order-Reduction Techniques

The High-Fidelity Generalized Method of Cells (HFGMC) is one technique, distinct from traditional finite element approaches, for accurately simulating nonlinear composite material behavior. In this work, the HFGMC global system of equations for doubly-periodic repeating unit cells with nonlinear constituents has been reduced in size through the novel application of a Petrov-Galerkin Proper Orthogonal Decomposition order-reduction scheme in order to improve its computational efficiency. Order-reduced models of an E-glass/Nylon 12 composite led to a 4.8 to 6.3x speedup in the equation assembly/solution runtime while maintaining model accuracy. This corresponded to a 21 to 38 percent reduction in total runtime. The significant difference in assembly/solution and total runtimes was attributed to the evaluation of integration point inelastic field quantities; this step was identical between the unreduced and order-reduced models. Nonetheless, order-reduced techniques offer the potential to significantly improve the computational efficiency of multiscale calculations.

Ricks, Trenton M.↗

NASA NTRS2007

Potential Space Applications for Body-Centric Wireless and E-Textile Antennas

Space environment benefits of body-centric wireless communications are numerous, particularly in the context of long duration Lunar and Martian outposts that are in planning stages at several space agencies around the world. Since crew time for such missions is a scarce commodity, seamless integration of body-centric wireless from various sources is paramount. Sources include traditional data, such as audio, video, tracking, and biotelemetry. Newer data sources include positioning, orientation, and status of handheld tools and devices, as well as management and status of on-body inventories. In addition to offering lighter weight and flexibility, performance benefits of e-textile antennas are anticipated due to advantageous use of the body s surface area. In creating e-textile antennas and RF devices, researchers are faced with the challenge of transferring conventional and novel designs to textiles. Lack of impedance control, limited conductivity, and the inability to automatically create intricate designs are examples of limitations frequently attributed to e-textiles. Reliable interfaces between e-textiles and conventional hardware also represent significant challenges. Addressing these limitations is critical to the continued development and acceptance of fabric-based circuits for body-centric wireless applications. Here we present several examples of e-textile antennas and RF devices, created using a NASA-developed process, that overcome several of these limitations. The design and performance of an equiangular spiral, miniaturized spiral-loaded slot antenna, and a hybrid coupler are considered, with the e-textile devices showing comparable performance to like designs using conventional materials.

Kennedy, Timothy F.↗

NASA NTRS1977

Investigation of the double exponential in the current-voltage characteristics of silicon solar cells

Difficulties in relating observed current-voltage characteristics of individual silicon solar cells to their physical and material parameters were underscored by the unexpected large changes in the current-voltage characteristics telemetered back from solar cells on the ATS-1 spacecraft during their first year in synchronous orbit. Depletion region recombination was studied in cells exhibiting a clear double-exponential dark characteristic by subjecting the cells to proton irradiation. A significant change in the saturation current, an effect included in the Sah, Noyce, Shockley formulation of diode current resulting from recombination in the depletion region, was caused by the introduction of shallow levels in the depletion region by the proton irradiation. This saturation current is not attributable only to diffusion current from outside the depletion region and only its temperature dependence can clarify its origin. The current associated with the introduction of deep-lying levels did not change significantly in these experiments.

Wolf, M.↗

NASA NTRS2008

Sub-Surface Windscreen for the Measurement of Outdoor Infrasound

A windscreen has been developed that features two advantages favorable for the measurement of outdoor infrasound. First, the sub-surface location, with the top of the windscreen flush with the ground surface, minimizes the mean velocity of the impinging wind. Secondly, the windscreen material (closed cell polyurethane foam) has a sufficiently low acoustic impedance (222 times that of air) and wall thickness (0.0127 m) to provide a transmission coefficient of nearly unity over the infrasonic frequency range (0-20 Hz). The windscreen, a tightly-sealed box having internal dimensions of 0.3048 x 0.3048 x 0.3556 m, contains a microphone, preamplifier, and a cable feed thru to an external power supply. Provisions are made for rain drainage and seismic isolation. A three-element array, configured as an equilateral triangle with 30.48 m spacing and operating continuously in the field, periodically receives highly coherent signals attributed to emissions from atmospheric turbulence. The time delays between infrasonic signals received at the microphones permit determination of the bearing and elevation of the sources, which correlate well with locations of pilot reports (PIREPS) within a 320 km radius about the array. The test results are interpreted to yield spectral information on infrasonic emissions from clear air turbulence.

Shams, Qamar A.↗

NASA NTRS2008

Nb(x)Ti(1-x)N Superconducting-Nanowire Single-Photon Detectors

Superconducting-nanowire single-photon detectors (SNSPDs) in which Nb(x)Ti(1-x)N (where x<1) films serve as the superconducting materials have shown promise as superior alternatives to previously developed SNSPDs in which NbN films serve as the superconducting materials. SNSPDs have potential utility in optical communications and quantum cryptography. Nb(x)Ti(1-x)N is a solid solution of NbN and TiN, and has many properties similar to those of NbN. It has been found to be generally easier to stabilize Nb(x)Ti(1-x)N in the high-superconducting-transition temperature phase than it is to so stabilize NbN. In addition, the resistivity and penetration depth of polycrystalline films of Nb(x)Ti(1-x)N have been found to be much smaller than those of films of NbN. These differences have been hypothesized to be attributable to better coupling at grain boundaries within Nb(x)Ti(1-x)N films.

Stern, Jeffrey A.↗

NASA NTRS1992

NASA-ACEE/Boeing 737 graphite-epoxy horizontal stabilizer service

The 737 graphite-epoxy horizontal stabilizer was developed by Boeing as part of the NASA-ACEE (Aircraft Energy Efficiency) Advanced Composite Structures Program. NASA-ACEE programs challenged large-transport manufacturers to use graphite material in redesigning existing aircraft components. The goal of the program was to develop the necessary data and technology to achieve production commitments to advanced composites. Boeing designed, fabricated, and certified five shipsets of horizontal stabilizers for the 737-200 airframe. The program was initiated in July 1977 and certification was achieved in August 1982. Schedule highlights are shown. The work performed on this program is reported in NASA technical summaries and final reports. Boeing introduced the stabilizer into commercial operation in 1984, and has maintained surveillance for seven years of in-service evaluation. Outstanding performance was demonstrated with no service incidents attributed to the graphite-epoxy structure. Boeing will continue to monitor and support these aircraft, adding to the database of commercial composite experience.

Quinlivan, J. T.↗

NASA NTRS2012

The Violent Early Solar System, as Told by Lunar Sample Geochronology

One of the legacies of the samples collected by the Apollo and Luna missions is the link forged between radiometric ages of rocks and relative ages according to stratigraphic relationships and impact crater size-frequency distributions. Our current understanding of the history of the inner solar system is based on the relative chronology of individual planets, tied to the absolute geochronology of the Moon via these important samples. Sample ages have enabled us to infer that impact-melt breccias from Apollo 14 and 15 record the formation of the Imbrium Basin, those from the highland massifs at Apollo 17 record the age of Serenitatis, those from the KREEP-poor Apollo 16 site record the age of Nectaris, and materials from Luna 24 record the age of Crisium. Ejecta from smaller and younger craters Copernicus and Tycho were sampled at Apollo 12 and 17, respectively, and local craters such as Cone at Apollo 14, and North Ray and South Ray at Apollo 16 were also sampled and ages determined for those events. Much of what we understand about the lunar impact flux is based on these ages. Samples from these nearside locations reveal a preponderance of impact-disturbed or recrystallized ages between 3.75 and 3.95 billion years. Argon and lead loss (and correlated disturbances in the Rb-Sr system) have been attributed to metamorphism of the lunar crust by an enormous number of impacts in a brief pulse of time, called the Lunar Cataclysm or Late Heavy Bombardment. Subsequent high-precision geochronometric analyses of Apollo samples and lunar highlands meteorites show a wider range of ages, but very few older than 4 Ga. The paucity of ancient impact melt rocks has been interpreted to mean that either that most impact basins formed at this time, or that ejecta from the large, near-side, young basins dominates the Apollo samples.

Cohen, Barbara A.↗

NASA NTRS2013

The Violent Early Solar System, as Told by Sample Geochronology

Cohen, Barbara↗

NASA NTRS1995

Incineration as a Method for Resource Recovery from Inedible Biomass in a Controlled Ecological Life Support System

Resource recovery from waste streams in a space habitat is essential to minimize the resupply burden and achieve self-sufficiency. In a Controlled Ecological Life Support System (CELSS) human wastes and inedible biomass will represent significant sources of secondary raw materials necessary for support of crop plant production (carbon, water, and inorganic plant nutrients). Incineration, pyrolysis, and water extraction have been investigated as candidate processes for recovery of these important resources from inedible biomass in a CELSS. During incineration CO2 is produced by oxidation of the organic components and this product can be directly utilized by plants. Water is concomitantly produced, requiring only a phase change for recovery. Recovery of inorganics is more difficult, requiring solubilization of the incinerator ash. The process of incineration followed by water solubilization of ash resulted in loss of 35% of the inorganics originally present in the biomass. Losses were attributed to volatilization (8%) and non-water-soluble ash (27%). All of the ash remaining following incineration could be solubilized with acid, with losses resulting from volatilization only. The recovery for individual elements varied. Elemental retention in the ash ranged from 100% of that present in the biomass for Ca, P, Mg, Na, and Si to 10% for Zn. The greatest water solubility was observed for potassium with recovery of approximately 77% of that present in the straw. Potassium represented 80% of the inorganic constituents in the wheat straw, and because of slightly greater solubility made up 86% of the water-soluble ash. Following incineration of inedible biomass from wheat, 65% of the inorganics originally present in the straw were recovered by water solubilization and 92% recovered by acid solubilization. Recovery of resources is more complex for pyrolysis and water extraction. Recovery of carbon, a resource of greater mass than the inorganic component of biomass, is more difficult following pyrolysis and water extraction of biomass. In both cases, additional processors would be required to provide products equivalent to those resulting from incineration alone. The carbon, water, and organic resources of inedible biomass are effectively separated and output in usable forms through incineration.

Bubenheim, David L.↗

NASA NTRS1982

Relict drainages, conical hills, and the eolian veneer in southwest Egypt - Applications to Mars

The fluvial and mass wasting origin of the particles in the eolian deposits, the segregation of these materials on the basis of grain size, and the migration of those particles capable of saltation to areas of accumulation in lowland basins of the Sahara are suggested as analogs for the formation and accumulation of 'sand' sheets and dunes on the northern plains and in the polar erg on Mars. Outliers of the Martian plateau in the fretted terrain are seen as having been dissected, at least initially, by channels whose upstream portions are incised in the uplands. The Martian 'wadis' possess many geomorphic peculiarities similar to those of the Gilf (Gilf Kebir Plateau, southwest Egypt) wadis, and like the Egyptian features they have been attributed to mass wasting. Even though basal sapping and removal of debris by wind have almost certainly modified the Martian features, their deep incision in the plateau and their inferred northward extensions in the northern plains are thought to require not only initial downcutting by fairly energetic streams but also prolonged and long-distance flow of water.

Breed, C. S.↗

NASA NTRS1995

Processing Mechanisms for Interstellar Ices: Connections to the Solar System

The organic component of the interstellar medium, which has revealed itself through the ubiquitous 3.4 micrometers hydrocarbon absorption feature, is widespread throughout the disk of our galaxy and has been attributed to dust grains residing in the diffuse interstellar medium. The absorption band positions near 3.4 micrometers are characteristic of C-H stretching vibrations in the -CH3 and -CH2- groups of saturated aliphatic hydrocarbons associated with perturbing chemical groups. The production of complex molecules is thought to occur within dense molecular clouds when ice-mantled grains are processed by various energetic mechanisms. Studies of the processing of interstellar ices and the subsequent production of organic residues have relevance to studies of ices in the solar system, because primitive, icy solar system bodies such as those in the Kuiper belt are likely reservoirs of organic material, either preserved from the interstellar medium or produced in situ. Connections between the interstellar medium and the early solar nebula have long been a source of interest. A comparison of the interstellar organics and the Murchison meteorite illustrates the importance of probing the interstellar connection to the solar system, because although the carbonaceous meteorites are undoubtedly highly processed, they do retain specific interstellar signatures (such as diamonds, SiC grains, graphite and enriched D/H). The organic component, while not proven interstellar, has a remarkable similarity to the interstellar organics observed in over a dozen sightlines through our galaxy. This paper compares spectra from laboratory organics produced through the processing of interstellar ice analog materials with the high resolution infrared observations of the interstellar medium in order to investigate the mechanisms (such as ion bombardment, plasma processing, and UV photolysis) that may be producing the organics in the ISM.

Pendleton, Y. J.↗

NASA NTRS2003

The Dependence of Target Properties Upon Fresh Crater Morphologies on Mars

Viking and Mars Orbiter Camera (MOC) images for approx. 900 "fresh" complex craters were chosen for inspection from a database of 1599 complex craters for which physical attributes have been obtained using the Mars Orbiter Laser Altimeter (MOLA). Preliminary analysis revealed that many of the complex craters have been significantly modified by various processes of denudation, as well as partial or complete infilling with sediments +/- impact melt +/- lava, considerably shallowing many of the craters. This study confirms that the majority of the 894 sampled complex craters are affected by such processes. In 474 cases (52%), no central peaks were observed owing to erosion or burial. Of the remaining craters with visible central peaks, 159 of the freshest craters were selected for further study. These were chosen based on: the absence of significant infilling materials; the presence of a sharp rim and, typically; the preservation of the finer scale morphologic features of the associated ejecta blanket. These craters were used in order to assess the association between the target type and various central peak morphologies, ejecta types and crater depth/diameter relations.

Whitehead, J.↗

NASA NTRS1993

Automated fiber placement composite manufacturing: The mission at MSFC's Productivity Enhancement Complex

Automated fiber placement is a manufacturing process used for producing complex composite structures. It is a notable leap to the state-of-the-art in technology for automated composite manufacturing. The fiber placement capability was established at the Marshall Space Flight Center's (MSFC) Productivity Enhancement Complex in 1992 in collaboration with Thiokol Corporation to provide materials and processes research and development, and to fabricate components for many of the Center's Programs. The Fiber Placement System (FPX) was developed as a distinct solution to problems inherent to other automated composite manufacturing systems. This equipment provides unique capabilities to build composite parts in complex 3-D shapes with concave and other asymmetrical configurations. Components with complex geometries and localized reinforcements usually require labor intensive efforts resulting in expensive, less reproducible components; the fiber placement system has the features necessary to overcome these conditions. The mechanical systems of the equipment have the motion characteristics of a filament winder and the fiber lay-up attributes of a tape laying machine, with the additional capabilities of differential tow payout speeds, compaction and cut-restart to selectively place the correct number of fibers where the design dictates. This capability will produce a repeatable process resulting in lower cost and improved quality and reliability.

Vickers, John H.↗