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At least 721 records · Page 40

A petrographic thin sectioning technique for evaluating composite materials

Petrographic thin sectioning by a low-speed diamond saw has been used in conjunction with transmission polarized light microscopy for the characterization of the microstructure and deformation mechanisms of a variety of polymer systems. It has proven possible by these means to study three types of thermoplastic matrices for composite applications: PEEK, BPA-based polycarbonate (PC), and a rubber-modified PC. The reinforcing fibers for these matrices were in all cases AS4 carbon fibers, unidirectionally arrayed. Superior analyzability of matrix morphology and subsurface fracture processes is achieved by thin sectioning.

Parker, D. S.↗

NASA/aircraft industry standard specification for graphite fiber toughened thermoset resin composite material

A standard specification for a selected class of graphite fiber/toughened thermoset resin matrix material was developed through joint NASA/Aircraft Industry effort. This specification was compiled to provide uniform requirements and tests for qualifying prepreg systems and for acceptance of prepreg batches. The specification applies specifically to a class of composite prepreg consisting of unidirectional graphite fibers impregnated with a toughened thermoset resin that produce laminates with service temperatures from -65 F to 200 F when cured at temperatures below or equal to 350 F. The specified prepreg has a fiber areal weight of 145 g sq m. The specified tests are limited to those required to set minimum standards for the uncured prepreg and cured laminates, and are not intended to provide design allowable properties.

Source record↗

Tribological evaluation of composite materials made from a partially fluorinated polyimide

Preliminary tribological studies on a new polyimide formulated from the diamine 2,2-bis 4-(4-aminophenoxy) phenyl hexafluoropane (4-BDAF) indicates polyimides made from this diamine have excellent potential for high temperature applications. Two different polyimides were formulated from the diamine, and five different composites were formulated using one of the polyimides. Composites were made using 10 weight percent (w/o) graphite fluoride powder, 20 w/o PTFE powder, 30 w/o silver powder, or 50 w/o carbon fibers, both graphitic and nongraphitic types. The powder additions did not improve the tribological properties as much as the carbon fibers, and the graphitic fibers produced better results than did the nongraphitic fibers. Results also indicated that improved high temperature stability and tribological properties may be obtained with a polyimide made from the dianhydride pyromellitic acid (PMDA) rather than the dianhydride benzophenonetetracarboxylic acid (BTDA).

Fusaro, R. L.↗

Flexural Fatigue Testing and Qualification of Hybrid PAN-pitch Composite Materials with High Through-Thickness Thermal Conductivity

Carbon-fiber-reinforced polymers (CFRPs) considered for motor components within future electric vertical takeoff and landing (eVTOL) vehicles require not only a high strength-to-weight ratio but also a high through-thickness thermal conductivity (TC) to dissipate heat. Previously, CFRPs incorporating pitch CF interleaves demonstrated an increased through-thickness TC relative to the baseline composite, but the effect on flexural fatigue life was not evaluated. For this work, T700S/TC275–1 braided carbon fiber/epoxy prepreg baseline (no interleave), YSH–60A pitch interleave, and YS–80A pitch interleave configurations were tested for fatigue life. A combination of ASTM International Standards D7264 and D3479 were used to develop a reliable testing method. An Instron® (Illinois Tool Works Inc.) 8501 servohydraulic system with a fatigue test fixture was set up with a 16:1 span:thickness ratio, load ratio R set to 0.1, and frequency of 4 Hz. High-cycle fatigue testing was completed, and it was found that YSH–60A interleave performed slightly better than YS–80A below 100,000 cycles but showed no differences above 100,000 cycles. In all cases, the baseline CFRP had superior fatigue life performance both in terms of stress handled and total cycles to failure. These fatigue testing data will inform future use of hybrid CFRP materials by highlighting the tradeoff between increased through-thickness TC and fatigue life. Testing guidelines, equipment, and parameters for static and fatigue tests were successfully outlined for CFRPs.

composites↗

Carbon/graphite composite material study. 3: Agency program activities. National Aeronautics and Space Administration (NASA)

The accidental release of carbon fibers from civil aircraft and the need for protection of civil aircraft systems from such fibers were studied. It was concluded that the electrical hazard from carbon fibers accidentally released in an aircraft crash fire pose no threat to human life. Overall costs associated with carbon fiber release are predicted to be extremely low. The risk of electrical or electronic failures due to carbon fibers is so minimal that future exploitation of carbon composites in aircraft should be continued. Additional protection of aircraft avionics to guard against carbon fibers is unnecessary. A program to develop alternate materials specifically to overcome the potential electrical hazard is not justified.

Source record↗

Brazing of refractory, superalloy, and composite materials for Space Shuttle applications.

Research work concerning the metallic portion of the shuttle-orbiter heat shield (expected to experience temperatures up to 2500 F) is described. The five metals being evaluated are TD-Ni-Cr, Cb-C129Y, Cb752, Hayes 188, and Inconel 625. Brazing techniques whereby pairs of these materials are joined into thin-membered assemblies for heat shield applications are described. Results obtained with the vacuum-furnace brazing process are examined. In addition, the use of brazed aluminum-boron metal-matrix-contoured composite structures for heat shield applications is evaluated.

Beuyukian, C. S.↗

Composite materials: Fatigue and fracture. Vol. 3

The present volume discusses topics in the fields of matrix cracking and delamination, interlaminar fracture toughness, delamination analysis, strength and impact characteristics, and fatigue and fracture behavior. Attention is given to cooling rate effects in carbon-reinforced PEEK, the effect of porosity on flange-web corner strength, mode II delamination in toughened composites, the combined effect of matrix cracking and free edge delamination, and a 3D stress analysis of plain weave composites. Also discussed are the compression behavior of composites, damage-based notched-strength modeling, fatigue failure processes in aligned carbon-epoxy laminates, and the thermomechanical fatigue of a quasi-isotropic metal-matrix composite.

O'Brien, T. K.↗

A new experimental method for the accelerated characterization of composite materials

A method which permits the prediction of long-term properties of graphite/epoxy laminates on the basis of short-term (15 min) laboratory tests is described. Demonstration of delayed viscoelastic fracture in one laminate configuration, and data on the time and temperature response of a matrix-dominated unidirectional laminate contributed to a characterization of the viscoelastic process in the graphite/epoxy composites. Master curves from short-term tests of certain laminate configurations can be employed to generate long-term master curves. In addition, analytical predictions from short-term results can be used to predict long-term (25-hour) laminate properties.

Brinson, H. F.↗

Characterization of interfacial failure in SiC reinforced Si3N4 matrix composite material by both fiber push-out testing and Auger electron spectroscopy

AES depth profiling and a fiber push-out test for interfacial shear-strength determination have been used to ascertain the mechanical/chemical properties of the fiber/matrix interface in SiC-reinforced reaction-bonded Si3N4, with attention to the weak point where interfacial failure occurs. In the cases of both composite fracture and fiber push-outs, the interfacial failure occurred either between the two C-rich coatings that are present on the double-coated SiC fibers, or between the inner C-rich coating and the SiC fiber. Interface failure occurs at points of very abrupt concentration changes.

Eldridge, J. I.↗

Materials - Fiber composites.

Fiber composite materials, their properties, their state of technical advancement, and the plans underway to further the development and application of these materials for efficient flight structures are reviewed. It is considered that the costs of composite materials will drop sharply as the volume and manufacturing expertise is increased. The tailorability of structural elements and unique applications requiring high stiffness seem to be particularly attractive features. A good measure of the state of the technology is the sophistication of the structures being built and flown. Several examples are cited.

Brooks, G. W.↗

Analysis of LDEF micrometeoroid/debris data and damage to composite materials

This report presented published LDEF micrometeoroid/debris impact data in a nomogram format useful for estimating the total number of hits that could be expected on a space structure as a function of time in orbit, angular location relative to ram, and exposed surface area. Correction factors accounting for different altitudes are given. These are normalized to the average LDEF altitude. Examples on how to use the nomograph are also included. In addition, impact data and damage areas observed on composite laminates (experiment AO 180) are discussed.

Tennyson, R. C.↗

Modal Analysis of Embedded Passive Damping Materials in Composite Plates with Different Orientations

This report presents an experimental and numerical investigation of the free vibration of cantilevered composite plates with and without passive damping. A total of seven composite material plates are considered. The lay-up sequences for the two plates without damping are [90/90/0/0], and [90/0/90/0]; the other five plates are the same as the first two with two embedded layers of passive damping material. The passive damping material is embedded at different locations in the plate with orientation [90/0/90/0],. The damping material employed is a 3M material (SJ-2015 ISD 112) with peak damping properties in the ambient temperature range (32 F to 140 F). The composite material used is a carbon fiber (977-2)/epoxy resin (IM7). The effect of the passive damping system employed in this study for the composite plates are discussed. Modal testing is performed on these plates to determine resonant frequencies, amplitude and mode shape information. Numerical results are obtained using COSMOS/M software for the plates without damping. The experimental and numerical results are in very good agreement for different laminated plates without damping layers.

Kehoe, Michael↗

A Convolutional Neural Network for Multiscale Modeling of Composite Materials

An artificial convolutional neural network was created to efficiently mimic a micromechanics model, the High Fidelity Generalized Method of Cells, for use in multi-scale structural finite element analysis. The network was found to quickly and accurately replicate the stiffness predicted by the micromechanics model using a 2D image of an idealized representative volume element of a fiber/matrix microstructure. The long-term goal of this work is to efficiently apply multi-scale methods for predicting the damage progression of a composite structure.

Composites↗

Flexible Wing Base Micro Aerial Vehicles: Composite Materials for Micro Air Vehicles

This paper will discuss the development of the University of Florida's Micro Air Vehicle concept. A series of flexible wing based aircraft that possess highly desirable flight characteristics were developed. Since computational methods to accurately model flight at the low Reynolds numbers associated with this scale are still under development, our effort has relied heavily on trial and error. Hence a time efficient method was developed to rapidly produce prototype designs. The airframe and wings are fabricated using a unique process that incorporates carbon fiber composite construction. Prototypes can be fabricated in around five man-hours, allowing many design revisions to be tested in a short period of time. The resulting aircraft are far more durable, yet lighter, than their conventional counterparts. This process allows for thorough testing of each design in order to determine what changes were required on the next prototype. The use of carbon fiber allows for wing flexibility without sacrificing durability. The construction methods developed for this project were the enabling technology that allowed us to implement our designs. The resulting aircraft were the winning entries in the International Micro Air Vehicle Competition for the past two years. Details of the construction method are provided in this paper along with a background on our flexible wing concept.

Ifju, Peter G.↗

Development of advanced material composites for use as internal insulation for LH2 tanks (gas layer concept)

A program is described that was conducted to develop an internal insulation system for potential application to the liquid hydrogen tanks of a reusable booster, where the tanks would be subjected to repeated high temperatures. The design of the internal insulation is based on a unique gas layer concept, in which capillary or surface tension effects are used to maintain a stable gas layer, within a cellular core structure, between the tank wall and the contained liquid hydrogen. Specific objectives were to select materials for insulation systems that would be compatible with wall temperatures of 350 F and 650 F during reentry into the earth's atmosphere, and to fabricate and test insulation systems under conditions simulating the operating environment. A materials test program was conducted to evaluate the properties of candidate materials at elevated temperatures and at the temperature of liquid hydrogen, and to determine the compatibility of the materials with a hydrogen atmosphere at the appropriate elevated temperature. The materials that were finally selected included Kapton polyimide films, silicone adhesives, fiber glass batting, and in the case of the 350 F system, Teflon film.

Gille, J. P.↗

Transparent metal model study of the use of a cellular growth front to form aligned monotectic composite materials

The purpose of this work was to resolve a scientific controversy in the understanding of how second phase particles become aligned during unidirectional growth of a monotectic alloy. A second aspect was to make the first systematic observations of the solidification behavior of a monotectic alloy during cellular growth in-situ. This research provides the first systematic transparent model study of cellular solidification. An interface stability diagram was developed for the planar to cellular transition of the succinonitrile glycerol (SNG) system. A method was developed utilizing Fourier Transform Infrared Spectroscopy which allows quantitative compositional analysis of directionally solidified SNG along the growth axis. To determine the influence of cellular growth front on alignment for directionally solidified monotectic alloys, the planar and cellular growth morphology was observed in-situ for SNG between 8 and 17 percent glycerol and for a range of over two orders of magnitude G/R.

Kaukler, William F.↗

Stochastic multiscale modeling for quantifying statistical and model errors with application to composite materials

This paper provides a coherent and efficient computational framework for stochastic multiscale analysis of material systems in the presence of parametric uncertainties and modeling errors. Uncertainty in those model parameters that are not deduced as upscaled quantities is attributed to an uncertainty “germ”. While such parameters can appear at any scale, they are predominant at the finest analysis scale. Additional uncertainties stemming from statistical estimation, attributed to lack of data and model error, are associated with each submodel contributing to the multiscale system. Here, a robust and efficient framework based on a generalized extended polynomial chaos expansion (gEPCE) is proposed to simultaneously propagate all these uncertainties in order to provide a probabilistic representation of specific quantities of interest (QoI). We characterize the full probability distribution of the QoI and the uncertainty in the failure probability pertaining to its tails. By combining gEPCE with kernel density estimation (KDE) and directional derivatives, we construct sensitivity measures that connect these statistical metrics of QoI to the various sources of uncertainty to assess their individual and combined impacts. An illustrative problem featuring three-point bending of a composite beam is investigated to demonstrate the presented approach.

36 MATERIALS SCIENCE↗