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Performance of the Rotor Systems Research Aircraft calibrated rotor loads measurement system

The compound Rotor Systems Research Aircraft (RSRA) is designed to make high accuracy, simultaneous measurements of all rotor forces and moments in flight. Physical calibration of the rotor force- and moment-measurement system when installed in the aircraft is required to account for any errors and to ensure that measurement system accuracy is traceable to the National Bureau of Standards. The first static calibration and associated analysis has been completed with good results. Hysteresis was a potential cause of static calibration errors, but was found to be negligible in flight, and analytical methods have been devised to eliminate its effects on calibration data. Flight tests confirmed that the calibrated rotor loads measurement system performs as expected in flight, and that it can dependably make direct measurements of fuselage vertical drag in hover.

Acree, C. W., Jr.↗

The Calibration of the DSCOVR EPIC Multiple Visible Channel Instrument Using MODIS and VIIRS as a Reference

The Deep Space Climate Observatory (DSCOVR), launched on 11 February 2015, is a satellite positioned near the Lagrange-1 (L1) point, carrying several instruments that monitor space weather, and Earth-view sensors designed for climate studies. The Earth Polychromatic Imaging Camera (EPIC) onboard DSCOVR continuously views the sun-illuminated portion of the Earth with spectral coverage in the UV, VIS, and NIR bands. Although the EPIC instrument does not have any onboard calibration abilities, its constant view of the sunlit Earth disk provides a unique opportunity for simultaneous viewing with several other satellite instruments. This arrangement allows the EPIC sensor to be inter-calibrated using other well-characterized satellite instrument reference standards. Two such instruments with onboard calibration are MODIS, flown on Aqua and Terra, and VIIRS, onboard Suomi-NPP. The MODIS and VIIRS reference calibrations will be transferred to the EPIC instrument using both all-sky ocean and deep convective clouds (DCC) ray-matched EPIC and MODIS/VIIRS radiance pairs. An automated navigation correction routine was developed to more accurately align the EPIC and MODIS/VIIRS granules. The automated navigation correction routine dramatically reduced the uncertainty of the resulting calibration gain based on the EPIC and MODIS/VIIRS radiance pairs. The SCIAMACHY-based spectral band adjustment factors (SBAF) applied to the MODIS/ VIIRS radiances were found to successfully adjust the reference radiances to the spectral response of the specific EPIC channel for over-lapping spectral channels. The SBAF was also found to be effective for the non-overlapping EPIC channel 10. Lastly, both ray-matching techniques found no discernable trends for EPIC channel 7 over the year of publically released EPIC data.

Haney, Conor↗

Results of the first complete static calibration of the RSRA rotor-load-measurement system

The compound Rotor System Research Aircraft (RSRA) is designed to make high-accuracy, simultaneous measurements of all rotor forces and moments in flight. Physical calibration of the rotor force- and moment-measurement system when installed in the aircraft is required to account for known errors and to ensure that measurement-system accuracy is traceable to the National Bureau of Standards. The first static calibration and associated analysis have been completed with good results. Hysteresis was a potential cause of static calibration errors, but was found to be negligible in flight compared to full-scale loads, and analytical methods have been devised to eliminate hysteresis effects on calibration data. Flight tests confirmed that the calibrated rotor-load-measurement system performs as expected in flight and that it can dependably make direct measurements of fuselage vertical drag in hover.

Acree, C. W., Jr.↗

Study Methods to Standardize Thermography NDE

The purpose of this work is to develop thermographic inspection methods and standards for use in evaluating structural composites and aerospace hardware. Qualification techniques and calibration methods are investigated to standardize the thermographic method for use in the field. Along with the inspections of test standards structural hardware, support hardware is designed and fabricated to aid in the thermographic process. Also, a standard operating procedure is developed for performing inspections with the Bales Thermal Image Processor (TIP). Inspections are performed on a broad range of structural composites. These materials include various graphite/epoxies, graphite/cyanide-ester, graphite/silicon-carbide, graphite phenolic and Keviar/epoxy. Also metal honeycomb (titanium and aluminum faceplates over an aluminum honeycomb core) structures are investigated. Various structural shapes are investigated and the thickness of the structures vary from as few as 3 plies to as many as 80 plies. Special emphasis is placed on characterizing defects in attachment holes and bondlines, in addition to those resulting from impact damage and the inclusion of foreign matter. Image processing through statistical analysis and digital filtering is investigated to enhance the quality and quantify the NDE thermal images when necessary.

Walker, James L.↗

Study Methods to Standardize Thermography NDE

The purpose of this work is to develop thermographic inspection methods and standards for use in evaluating structural composites and aerospace hardware. Qualification techniques and calibration methods are investigated to standardize the thermographic method for use in the field. Along with the inspections of test standards structural hardware, support hardware is designed and fabricated to aid in the thermographic process. Also, a standard operating procedure is developed for performing inspections with the Bales Thermal Image Processor (TIP). Inspections are performed on a broad range of structural composites. These materials include graphite/epoxies, graphite/cyanide-ester, graphite/silicon-carbide, graphite phenolic and Kevlar/epoxy. Also metal honeycomb (titanium and aluminum faceplates over an aluminum honeycomb core) structures are investigated. Various structural shapes are investigated and the thickness of the structures vary from as few as 3 plies to as many as 80 plies. Special emphasis is placed on characterizing defects in attachment holes and bondlines, in addition to those resulting from impact damage and the inclusion of foreign matter. Image processing through statistical analysis and digital filtering is investigated to enhance the quality and quantify the NDE thermal images when necessary.

Walker, James L.↗

Sci—Fri AM: Mountain — 03: Current status of the NRC primary standard for {sup 192}Ir HDR brachytherapy sources

The Canadian primary standard for {sup 192}Ir HDR brachytherapy sources has been recently revised in a more accurate manner allowing for more realistic uncertainty estimation. Air-kerma strength S{sub k} is derived from measurements of the source's output using a graphite-walled spherical ionization chamber (2S) at several distances. Traceability to NRC primary standards for the {sup 192}Ir calibration coefficient N{sub k} is insured by estimating it as the inverse arithmetic mean of the inverse of the calibration coefficients for a {sup 137}Cs beam and the medium energy x-ray beam quality N250, both of which are traceable to NRC primary standards. The multiple-distance method is combined with a non-linear least squares fit to determine St, while at the same time removing the effects of room scatter and position offset. The previously used shadow-cone method for directly measuring the room scatter is found to be inadequate due to the increased scatter contribution from the lead cone itself, especially at short source-detector distances. Rather than including the reported 1% difference in source strength for {sup 192}Ir HDR sources of different construction into the total uncertainty, users are cautioned that the calibration coefficient provided by NRC is only valid for a microSelectron V2 model. A comprehensive uncertainty budged shows that the total one sigma uncertainty of the standard is actually 0.6% rather than the previously assumed 1.2%. NRC measured S{sub k} agrees within 0.03% of the manufacturer's value.

07 ISOTOPE AND RADIATION SOURCES↗

Low Level Calibration of Liquid Scintillation Counting

Liquid Scintillation Counting (LSC) is an analytical laboratory method that quantifies the concentrations of alpha and beta emitting isotopes. The LSC method can be utilized for the detection of tritium, both environmentally and at nuclear facilities. Most LSC samples are aqueous-based and prepared as a radioactive sample dissolved or suspended in a high efficiency scintillation cocktail that converts radioactive energy into light pulses. When placed in counting vials, the liquid scintillation cocktail allows for optical coupling in which energy is released from the samples radioactive decay, and transferred to the scintillator. That energy is then absorbed to produce excited electrons that fall back to their ground-state and emit a pulse of light that is detected by the liquid scintillation analyzers photomultiplier tubes. Quench is a signal attenuation due to physical, chemical, or color interferences. To compensate for quench, quench standards of a known concentration are implemented at increasing increments of quench per vial to create a quench curve. Quench standards can be purchased pre-made or customized from the manufacturer, however, there are several issues that arise from purchasing the pre-made quench standards. The main issues with ordering pre-made quench standards is that they use higher count values, between 30,000 and 250,000 disintegrations per minute (dpm) of tritium per vial and only come in glass vials. Using higher counting standards in glass vials makes it hard to see lower concentrations in plastic vials. Additionally, when using higher energy standards the accuracy of the calibration readings tend to be lower. On the other hand, making a set of quench standards in-house allows for the customization of the dpm concentration to roughly 1,500-3,000 and preparation in plastic vials. This allows for lower activity readings that results in closer precision of the samples' true concentration. Technical Objectives: Create a quench curve and calibrate the LSA for tritium. Verify the calibration of the quench curve prior to cross sample runs. Check calibration against Quality Control (QC) reference value. Conclusion: a tritium quench curve calibration was performed using a scintillation cocktail with ultima gold (AB and AB/F), acetone (only with AB), and water (only with AB/F). By performing the tritium quench curve calibration, the counting efficiency was correlated to various levels of quench. Calibration checks with quality control standards were also performed to verify that the calibration was correct. The observed results provided acceptable values that matched the quality control standard reference values with an acceptable uncertainty. The next step will be fine tuning and cross comparison checks with legacy instrumentation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Spectral Emittance of Uncoated and Ceramic-Coated Inconel and Type 321 Stainless Steel

The normal spectral emittance of Inconel and type 321 stainless steel with different surface treatments was measured at temperatures of 900, 1,200, 1,500, and 1,800 F over a wavelength range of 1.5 to 15 microns. The measurements involved comparison of the radiant energy emitted by the heated specimen with that emitted by a comparison standard at the same temperature by means of a recording double-beam infrared spectrophotometer. The silicon carbide comparison standard had previously been calibrated against a laboratory black-body furnace. Surface treatments included electropolishing, sandblasting, electro-polishing followed by oxidation in air for 1/2 hour at 1,800 F, sandblasting followed by oxidation in air for 1/2 hour at 1,800 F, application of National Bureau of Standards coating A-418, and application of NBS ceramic coating N-143. The normal spectral emittance of both alloys in the electropolished condition was low and decreased very slightly with increasing wavelength while in the sandblasted condition it was somewhat higher and did not vary appreciably with wavelength. The oxidation treatment greatly increased the normal spectral emittance of both the electropolished and sandblasted type 321 stainless steel specimens and of the electropolished Inconel specimens and introduced some spectral selectivity into the curves. The oxidation increased the normal spectral emittance of the sandblasted Inconel specimens only moderately. Of the specimens to which a coating about 0.002 inch thick was applied, those coated with A-418 had higher emittance at all wavelengths than did those coated with N-143, and the coated specimens of Inconel had higher spectral emittance at all wavelengths than did the corresponding specimens of type 321 stainless steel. Both coatings were found to be partially transparent to the emitted energy at this thickness but essentially opaque at a thickness of 0.005 inch. Coated specimens with 0.005 inch or more of coating did not show the effect of the underlying metal on spectral emittance, and there was no significant difference at wavelengths greater than about five microns in the normal spectral emittance of specimens having the two coatings. At shorter wavelengths the normal spectral emittance of specimens coated with A-418 was greater than that of specimens coated with N-143.

Richmond, Joseph C.↗

TU-E-TOUR-I-00: Exhibit Hall Guided Tours-Dosimters for QC in Diagnostic Imaging (Tuesday)

Tour Leader: Xia Jiang, Ohio State University, Columbus, OH Tour Guides: Xia Jiang, Ohio State University, Columbus, OH Kevin Little, The University of Chicago, Chicago, IL Christina Sammet, Lurie Children’s Hospital of Chicago, Chicago, IL Participating Vendors: IBA PTW - New York Radcal Corporation RTI Electronics, Inc. Exhibit Hall Guided Tours is a new program launching this year at the Annual Meeting. The Guided Tours are designed to enhance the interaction between meeting attendees and exhibitors. This year’s Imaging Guided Tours are organized around the theme of dosimeters for quality control in diagnostic imaging. Tours will begin with an introduction and background given by Dr. Xia Jiang, the Tour Leader. The introduction will cover the types and properties of different radiation dosimeters used for quality assurance in clinical radiology. Attendees will then break into smaller groups, each lead by an AAPM-member Tour Guide. The tour groups will visit the exhibit booths of vendors who provide appropriate dosimeters, and a vendor representative will give a presentation to the group about their particular product(s). The vendor representatives as well as the Tour Guides will be available to answer questions. Outline: Types and properties of radiation detectors and dosimeters Ionization chamber dosimeters Solid state dosimeters Dosimeter calibration: Primary and secondary standards dosimetry laboratories Instruments for measuring tube voltage and exposure time Vendor presentations will likely cover features and innovations of different dosimeter systems, as well as their practical use. Learning Objectives: Understand the types and properties of different instrumentations used for quality control in diagnostic imaging. Understand the process of dosimeter calibration. Gain familiarity with the latest commercial dosimeter systems from different vendors.

61 RADIATION PROTECTION AND DOSIMETRY↗

WE-C-TOUR-I-00: Exhibit Hall Guided Tours-Dosimters for QC in Diagnostic Imaging (Wednesday)

Tour Leader: Xia Jiang, Ohio State University, Columbus, OH Tour Guides: Xia Jiang, Ohio State University, Columbus, OH Kevin Little, The University of Chicago, Chicago, IL Adrien Sanchez, University of Chicago, Chicago, IL Participating Vendors: IBA PTW - New York Radcal Corporation RTI Electronics, Inc. Exhibit Hall Guided Tours is a new program launching this year at the Annual Meeting. The Guided Tours are designed to enhance the interaction between meeting attendees and exhibitors. This year’s Imaging Guided Tours are organized around the theme of dosimeters for quality control in diagnostic imaging. Tours will begin with an introduction and background given by Dr. Xia Jiang, the Tour Leader. The introduction will cover the types and properties of different radiation dosimeters used for quality assurance in clinical radiology. Attendees will then break into smaller groups, each lead by an AAPM-member Tour Guide. The tour groups will visit the exhibit booths of vendors who provide appropriate dosimeters, and a vendor representative will give a presentation to the group about their particular product(s). The vendor representatives as well as the Tour Guides will be available to answer questions. Outline: Types and properties of radiation detectors and dosimeters Ionization chamber dosimeters Solid state dosimeters Dosimeter calibration: Primary and secondary standards dosimetry laboratories Instruments for measuring tube voltage and exposure time Vendor presentations will likely cover features and innovations of different dosimeter systems, as well as their practical use. Learning Objectives: Understand the types and properties of different instrumentations used for quality control in diagnostic imaging. Understand the process of dosimeter calibration. Gain familiarity with the latest commercial dosimeter systems from different vendors.

61 RADIATION PROTECTION AND DOSIMETRY↗

WE-C-TOUR-I-01: Dosimters for QC in Diagnostic Imaging

Tour Leader: Xia Jiang, Ohio State University, Columbus, OH Tour Guides: Xia Jiang, Ohio State University, Columbus, OH Kevin Little, The University of Chicago, Chicago, IL Adrien Sanchez, University of Chicago, Chicago, IL Participating Vendors: IBA PTW - New York Radcal Corporation RTI Electronics, Inc. Exhibit Hall Guided Tours is a new program launching this year at the Annual Meeting. The Guided Tours are designed to enhance the interaction between meeting attendees and exhibitors. This year’s Imaging Guided Tours are organized around the theme of dosimeters for quality control in diagnostic imaging. Tours will begin with an introduction and background given by Dr. Xia Jiang, the Tour Leader. The introduction will cover the types and properties of different radiation dosimeters used for quality assurance in clinical radiology. Attendees will then break into smaller groups, each lead by an AAPM-member Tour Guide. The tour groups will visit the exhibit booths of vendors who provide appropriate dosimeters, and a vendor representative will give a presentation to the group about their particular product(s). The vendor representatives as well as the Tour Guides will be available to answer questions. Outline: Types and properties of radiation detectors and dosimeters Ionization chamber dosimeters Solid state dosimeters Dosimeter calibration: Primary and secondary standards dosimetry laboratories Instruments for measuring tube voltage and exposure time Vendor presentations will likely cover features and innovations of different dosimeter systems, as well as their practical use. Learning Objectives: Understand the types and properties of different instrumentations used for quality control in diagnostic imaging. Understand the process of dosimeter calibration. Gain familiarity with the latest commercial dosimeter systems from different vendors.

61 RADIATION PROTECTION AND DOSIMETRY↗

NREL Pyrheliometer Comparisons: September 23-October 4, 2019 (NPC-2019)

Accurate measurements of direct normal (beam) solar irradiance from pyrheliometers are important for developing and deploying solar energy conversion systems, improving our understanding of the Earth's energy budget for climate change studies, and for other science and technology applications involving solar flux. Providing these measurements places many demands on the quality system used by the operator of commercially available radiometers. Maintaining accurate radiometer calibrations that are traceable to an international standard is the first step in producing research-quality solar irradiance measurements. In 1977, the World Meteorological Organization (WMO) established the World Radiometric Reference (WRR) as the international standard for the measurement of direct normal solar irradiance (Frohlich 1991). The WRR is an internationally recognized, detector-based measurement standard determined by the collective performance of six electrically self-calibrated absolute cavity radiometers comprising the World Standard Group (WSG). Various countries, including the United States, have contributed these specialized radiometers to the Physikalisch-Meteorologisches Observatorium Davos - World Radiation Center (PMOD/WRC) to establish the WSG.

14 SOLAR ENERGY↗

The Twins Embedding of Type Ia Supernovae. II. Improving Cosmological Distance Estimates

We show how spectra of Type Ia supernovae (SNe Ia) at maximum light can be used to improve cosmological distance estimates. In a companion article, we used manifold learning to build a three-dimensional parameterization of the intrinsic diversity of SNe Ia at maximum light that we call the "Twins Embedding."In this article, we discuss how the Twins Embedding can be used to improve the standardization of SNe Ia. With a single spectrophotometrically calibrated spectrum near maximum light, we can standardize our sample of SNe Ia with an rms of 0.101 0.007 mag, which corresponds to 0.084 0.009 mag if peculiar velocity contributions are removed and to 0.073 0.008 mag if a larger reference sample were obtained. Our techniques can standardize the full range of SNe Ia, including those typically labeled as peculiar and often rejected from other analyses. We find that traditional light-curve width + color standardization such as SALT2 is not sufficient. The Twins Embedding identifies a subset of SNe Ia, including, but not limited to, 91T-like SNe Ia whose SALT2 distance estimates are biased by 0.229 0.045 mag. Standardization using the Twins Embedding also significantly decreases host-galaxy correlations. We recover a host mass step of 0.040 0.020 mag compared to 0.092 0.026 mag for SALT2 standardization on the same sample of SNe Ia. These biases in traditional standardization methods could significantly impact future cosmology analyses if not properly taken into account.

79 ASTRONOMY AND ASTROPHYSICS↗

Results of the 1970 balloon flight solar cell standardization program

For the eighth consective year, high-altitude calibration of solar cells was accomplished with the aid of free-flight balloons. Flights were conducted to an altitude of 36,576 m which is above 99.5% of earth's atmosphere where all water vapor levels and significant ozone bands are absent. Solar cells calibrated in this manner are significant used as intensity references in solar simulators and in terrestrial sunlight. Discussed is the method employed for high altitude balloon flight solar cell calibration. Also presented are data collected on 52 standard solar cells on two flights conducted in 1970. Solar cells flown repeatedly on successive flights have shown correlation of better than + or - 1.0%.

Greenwood, R. F.↗

Absolute UV irradiance calibration of the Solar UV Spectral Irradiance Monitor (SUSIM) instruments

The Solar Ultraviolet Spectral Irradiance Monitor (SUSIM) flown on Spacelab 2 (SL2) and a second advanced instrument being prepared for flight on the Upper Atmospheric Research Satellite (UARS) are calibrated using a number of absolute UV irradiance standards in order to meet the stringent calibration goals of the SUSIM program. The SUSIM instruments, the methods of calibration, and the error analyses are described.

Vanhoosier, Michael E.↗

A method for direct, semi-quantitative analysis of gas phase samples using gas chromatography-inductively coupled plasma-mass spectrometry

A new and complete GC–ICP-MS method is described for direct analysis of trace metals in a gas phase process stream. The proposed method is derived from standard analytical procedures developed for ICP-MS, which are regularly exercised in standard ICP-MS laboratories. In order to implement the method, a series of empirical factors were generated to calibrate detector response with respect to a known concentration of an internal standard analyte. Calibrated responses are ultimately used to determine the concentration of metal analytes in a gas stream using a semi-quantitative algorithm. The method was verified using a traditional gas injection from a GC sampling valve and a standard gas mixture containing either a 1 ppm Xe + Kr mix with helium balance or 100 ppm Xe with helium balance. Data collected for Xe and Kr gas analytes revealed that agreement of 6–20% with the actual concentration can be expected for various experimental conditions. To demonstrate the method using a relevant “unknown” gas mixture, experiments were performed for continuous 4 and 7 hour periods using a Hg-containing sample gas that was co-introduced into the GC sample loop with the xenon gas standard. System performance and detector response to the dilute concentration of the internal standard were pre-determined, which allowed semi-quantitative evaluation of the analyte. The calculated analyte concentrations varied during the course of the 4 hour experiment, particularly during the first hour of the analysis where the actual Hg concentration was under predicted by up to 72%. Calculated concentration improved to within 30–60% for data collected after the first hour of the experiment. Similar results were seen during the 7 hour test with the deviation from the actual concentration being 11–81% during the first hour and then decreasing for the remaining period. The method detection limit (MDL) was determined for the mercury by injecting the sample gas into the system following a period of equilibration. The MDL for Hg was calculated as 6.8 μg · m -3 . This work describes the first complete GC–ICP-MS method to directly analyze gas phase samples, and detailed sample calculations and comparisons to conventional ICP-MS methods are provided.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Fixed-head star tracker magnitude calibration on the solar maximum mission

The sensitivity of the fixed-head star trackers (FHSTs) on the Solar Maximum Mission (SMM) is defined as the accuracy of the electronic response to the magnitude of a star in the sensor field-of-view, which is measured as intensity in volts. To identify stars during attitude determination and control processes, a transformation equation is required to convert from star intensity in volts to units of magnitude and vice versa. To maintain high accuracy standards, this transformation is calibrated frequently. A sensitivity index is defined as the observed intensity in volts divided by the predicted intensity in volts; thus, the sensitivity index is a measure of the accuracy of the calibration. Using the sensitivity index, analysis is presented that compares the strengths and weaknesses of two possible transformation equations. The effect on the transformation equations of variables, such as position in the sensor field-of-view, star color, and star magnitude, is investigated. In addition, results are given that evaluate the aging process of each sensor. The results in this work can be used by future missions as an aid to employing data from star cameras as effectively as possible.

Pitone, Daniel S.↗

SU-F-J-182: Investigation of Systems for Improved Accuracy in Clinical Y-90 Percent Delivered Calculations

Purpose: Y-90 Selective Internal Radiation Therapy (SIRT) is used to treat liver tumors, and by nature has variability in the percent of the intended dose that is actually delivered. To determine the quality of the administration, pre and post activity measurements are taken, and used to infer percent delivered. Vendor specifications indicate the use of an ion chamber to take these measurements. In our work, we investigated the accuracy of ion chambers, and compared them to other detector systems. Methods: We have built phantoms, phantom holders, and protocols, which allow us to measure our Y90 doses with varying apparatuses: a dose calibrator, a Geiger-counter, an ion chamber, a crystal based thyroid probe, and a gamma camera. We have set up a system that has enabled us to gather data by measuring clinical Y90 doses as they are used in the clinic using all of the instrumental methods. Five initial doses (25 measurements/acquisitions) have been taken at the time of this abstract submission. Results: Our initial results show that measurements acquired using scintillation based detectors (thyroid probe and gamma camera) correlate better with the gold standard (i.e. the dose calibrator). Pearson correlations between the dose calibrator measurements and the GM counter, Ion chamber, thyroid probe, and gamma camera were found to be 0.88, 0.83, 0.98, 0.99, respectively. More acquisitions and analysis are planned to determine the precision of the systems, as well as optimal energy window settings. Conclusion: It is likely that current standard practice can be improved using scintillation crystal based detectors. Such systems are more sensitive, can integrate signal, and can use energy discrimination. Furthermore, phantoms can be built to integrate with probe and gamma camera systems that are robust and provide reproducibility. Future work will include expanded acquisition and analysis.

60 APPLIED LIFE SCIENCES↗