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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
NASA NTRS1986

Space radiation effects on the dimensional stability of a toughened epoxy graphite composite

The effects of a simulated space radiation environment on the dimensional stability of an elastomer-toughened epoxy-graphite composite were determined. The response of the material was characterized following exposure to radiation doses equivalent to geosynchronous orbit lifetimes ranging from 6 months to 30 years. The results show that radiation interacts with the epoxy matrix to embrittle the composite, beginning at relatively low total doses (10 to the 7th power rads). The embrittlement results in thermal expansion changes and significant laminate microcracking during thermal cycling. These property changes could limit the service life of this material in some spacecraft applications.

Sykes, G. F.↗
NASA NTRS1988

Properties of two composite materials made of toughened epoxy resin and high-strain graphite fiber

Results are presented from an experimental evaluation of IM7/8551-7 and IM6/18081, two new toughened epoxy resin, high strain graphite fiber composite materials. Data include ply-level strengths and moduli, notched tension and compression strengths and compression-after-impact assessments. The measured properties are compared with those of other graphite-epoxy materials.

Dow, Marvin B.↗
NASA NTRS1988

Toughening of a thermoplastic matrix composite - Processing issues

The use of a rubber modified thermoplastic resin has been investigated as a method to improve the impact damage and the Mode I interlaminar fracture toughness of a unidirectional continuous carbon fiber composite. Test results show that the improvement in the fracture toughness is less than expected due to rubber particle agglomeration, poor fiber/matrix adhesion and the induced crystallization of the matrix. These restrictions must be eliminated in order to evaluate the maximum potential of a rubber toughened thermoplastic matrix on a composite's fracture toughness.

Parker, D. S.↗
NASA NTRS1989

Factors influencing the Mode I interlaminar fracture toughness of a rubber toughened thermoplastic matrix composite

The use of a rubber modified thermoplastic resin has been investigated as a method to improve the Mode I interlaminar fracture toughness of a unidirectional continuous carbon fiber composite. Test results show that the improvement in the fracture toughness is less than expected due to rubber particle agglomeration, solvent and molding induced crystallization of the matrix and poor fiber/matrix adhesion. The plastic zone in composites utilizing tough matrices can extend well beyond a single interfibrillar spacing. However, the development of the plastic zone is limited due to the failure of the fiber/matrix interface. In order to fully evaluate the potential of tough composites using toughened matrices, any improvement made in the matrix toughness must be coupled with improvements in the fiber/matrix adhesion.

Parker, D. S.↗
NASA NTRS1989

Analysis of whisker-toughened ceramic components: A design engineer's viewpoint

The use of ceramics components in gas turbines, cutting tools, and heat exchangers has been limited by the relatively low flaw tolerance of monolithic ceramics. The development of whisker toughened ceramic composites offers the potential for considerable improvement in fracture toughness as well as strength. However, the variability of strength is still too high for the application of deterministic design approaches. Several phenomenological reliability theories proposed for this material system are reviewed and the development is reported of a public domain computer algorithm. This algorithm, when coupled with a general purpose finite element program, predicts the fast fracture reliability of a structural component under multiaxial loading conditions.

Duffy, Stephen F.↗
NASA NTRS1990

Microcracking mechanisms and interface toughening of semi-IPN polyimide matrix composites

A new research program was initiated as a preliminary phase. The following three objectives are being pursued for the overall program: to elucidate the mechanisms of microcracking for graphite fiber-reinforced semi-IPN polyimide matrix composites under mechanical and thermal cyclic loading; to devise material engineering solutions for possible improvement of fatigue damage resistance (or the increase of fatigue endurance strength) of semi-IPN matrix composites by tailoring of modulus and toughness of fiber-resin interface region; and to assess processing characteristics of the composites and their roles in controlling the resistance of composites to microcracking and the effectiveness of interface toughening. The main emphasis was placed upon the initial screening of material systems and optimization of processing conditions for semi-IPN matrix composites with tailored interface. As a first set of control material systems to study, the composites were prepared with unsized Celion 6000 graphite fiber reinforcement and the following resin matrices of varied fracture toughness: PMR-15 thermoset polyimide, semi-IPN of PNR-15 thermoset polyimide and NR150B2 thermoplastic polyimide in 75/25 ratio, and semi-IPN of PMR-15 and NR150B2 in 50/50 ratio. For the composites with the resin matrix of semi-IPN in 75/25 ratio, interface tailoring was attempted by using graphite fibers coated with the resins of systematically varied fracture toughness. In the continuing work, a broad range of interlayer toughness will be achieved by coating the fibers with reactants of semi-IPN having lower or higher content of thermoplastic constituent in comparison with the composition of surrounding resin matrix. In pursuing the objectives of the overall research program, the respective roles and interaction of critical parameters were defined.

Lee, Byung L.↗
NASA NTRS1990

Mechanical behavior and failure phenomenon of an in situ-toughened silicon nitride

The Weibull modulus, fracture toughness and crack growth resistance of an in-situ toughened, silicon nitride material used to manufacture a turbine combustor were determined from room temperature to 1371 C. The material exhibited an elongated grain structure that resulted in improved fracture toughness, nonlinear crack growth resistance, and good elevated temperature strength. However, low temperature strength was limited by grains of excessive length (30 to 100 microns). These excessively long grains were surrounded by regions rich in sintering additives.

Salem, Jonathan A.↗
NASA NTRS1991

Toughening of PMR composites by semi-interpenetrating networks

Polymerization of monomer reactants (PMR-15) type polyimide and RP46 prepregs were drum wound using IM-7 fibers. Prepregging and processing conditions were optimized to yield good quality laminates with fiber volume fractions of 60 percent (+/- 2 percent). Samples were fabricated and tested to determine comprehensive engineering properties of both systems. These included 0 deg flexure, short beam shear, transverse flexure and tension, 0 deg tension and compression, intralaminar shear, short block compression, mode 1 and 2 fracture toughness, and compression after impact properties. Semi-2-IPN (interpenetrating polymer networks) toughened PMR-15 and RP46 laminates were also fabricated and tested for the same properties.

Tiwari, S. N.↗
NASA NTRS1992

Estimation of crack closure stresses for in situ toughened silicon nitride with 8 wt pct scandia

An 8-wt pct-scandia silicon nitride with an elongated grain structure was fabricated. The material exhibited high fracture toughness and a rising R-curve as measured by the indentation strength technique. The 'toughening' exponent m was found to be m about 0.1. The high fracture toughness and R-curve behavior was attributed mainly to bridging of the crack faces by the elongated grains. The crack closure (bridging) stress distribution in the wake region of the crack tip was estimated as a function of crack size from the R-curve data, with an arbitrarily assumed distribution function.

Choi, Sung R.↗
NASA NTRS1992

Mechanical behaviour and failure phenomenon of an in situ toughened silicon nitride

The Weibull modulus, fracture toughness and crack growth resistance of an in-situ toughened, silicon nitride material used to manufacture a turbine combustor were determined from room temperature to 1371 C. The material exhibited an elongated grain structure that resulted in improved fracture toughness, nonlinear crack growth resistance, and good elevated temperature strength. However, low temperature strength was limited by grains of excessive length (30 to 100 microns). These excessively long grains were surrounded by regions rich in sintering additives.

Salem, J. A.↗
NASA NTRS1991

Effects of intra- and inter-laminar resin content on the mechanical properties of toughened composite materials

Composite materials having multiphase toughened matrix systems and laminate architectures characterized by resin-rich interlaminar layers (RIL) have been the subject of much recent attention. Such materials are likely to find applications in thick compressively loaded structures such as the keel area of commercial aircraft fuselages. The effects of resin content and its interlaminar and intralaminar distribution on mechanical properties were investigated with test and analysis of two carbon-epoxy systems. The RIL was found to reduce the in situ strengthening effect for matrix cracking in laminates. Mode 2 fracture toughness was found to increase with increasing RIL thickness over the range investigated, and Mode 1 interlaminar toughness was negligibly affected. Compressive failure strains were found to increase with increasing resin content for specimens having no damage, holes, and impact damage. Analytical tools for predicting matrix cracking of off-axis plies and damage tolerance in compression after impact (CAI) were successfully applied to materials with RIL.

Grande, Dodd H.↗
NASA NTRS1992

Evaluation of the mechanical properties and damage tolerance of five new toughened matrix composite materials

Notched and unnotched tension and compression properties of quasi-isotropic laminates are presently evaluated, in conjunction with compression-after-impact (CAI) strengths, for the cases of five different carbon fiber-reinforced/toughened matrix composites. For a given impact energy, CAIs were dependent on impact velocities. When compared with other matrix-toughened materials, the five presently considered were more damage-tolerant than such aircraft primary structure composite systems as T300/5208.

Cano, Roberto J.↗
NASA NTRS1993

Characterization of the thermal conductivity for Advanced Toughened Uni-piece Fibrous Insulations

Advanced Toughened Uni-piece Fibrous Insulations (TUFI) is discussed in terms of their thermal response to an arc-jet air stream. A modification of the existing Ames thermal conductivity program to predict the thermal response of these functionally gradient materials is described in the paper. The modified program was used to evaluate the effect of density, surface porosity, and density gradient through the TUFI materials on the thermal response of these insulations. Predictions using a finite-difference code and calculated thermal conductivity values from the modified program were compared with in-depth temperature measurements taken from TUFI insulations during short exposures to arc-jet hypersonic air streams.

Stewart, David A.↗
NASA NTRS1995

Materials for the General Aviation Industry: Effect of Environment on Mechanical Properties of Glass Fabric/Rubber Toughened Vinyl Ester Laminates

A screening evaluation is being conducted to determine the performance of several glass fabric/vinyl ester composite material systems for use in primary General Aviation aircraft structures. In efforts to revitalize the General Aviation industry, the Integrated Design and Manufacturing Work Package for General Aviation Airframe and Propeller Structures is seeking to develop novel composite materials and low-cost manufacturing methods for lighter, safer and more affordable small aircraft. In support of this Work Package, this study is generating material properties for several glass fabric/rubber toughened vinyl ester composite systems and investigates the effect of environment on property retention. All laminates are made using the Seemann Composites Resin Infusion Molding Process (SCRIMP), a potential manufacturing method for the General Aviation industry.

McBride, Timothy M.↗
NASA NTRS1994

Crack-Growth Resistance of in Situ-Toughened Silicon Nitride

The fracture toughness of a commercial, hot-pressed, in situ-toughened silicon nitride with an elongated grain structure is determined by four different testing methods. The fracture toughness is found to be 5.76 +/- 0.27, 8.48 +/- 0.50, 10.16 +/- 0.66, and 10.68 +/- 0.39 MPa x m(exp 1/2), respectively, by indentation crack size measurement, indentation strength, single-edge-precracked-beam, and chevron-notched-beam methods. The discrepancy in fracture toughness between the testing methods is related to R-curve behavior, as measured using the indentation strength technique. These results indicate that there is no unique fracture toughness value and that a fracture toughness testing method with appropriate qualifiers is needed for rising R-curve materials. Therefore, care should be taken in interpreting and utilizing fracture toughness values evaluated from different testing methods if a material exhibits a rising R-curve. Complete characterization of the R-curve may be a prerequisite.

Salem, Jonathan A.↗
NASA NTRS2005

Toughened Matrix SiC Fiber Reinforced Composites

First matrix cracking stress is a critical parameter for application of Sic fiber reinforced composites in highly stressed, environmentally demanding applications such as turbine blades. High matrix fracture toughness is a key property that contributes to high composite fracture stress. Silicon nitride offers reduced matrix elastic modulus, lower coefficient of thermal expansion, and potentially high fracture toughness compared to Sic matrices. All of these factors can be used to advantage to increase matrix fracture stress. As a first model system we are pursuing toughened silicon nitride matrix composites reinforced with SCS-9 fibers. Fabrication is by tape casting the matrix plies and tape lay-up with fiber plies followed by hot pressing at 1800 C. Progress toward this end will be reported.

Levine, Stanley R.↗