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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Temperature-Tuned Faceting and Shape Changes in Liquid Alkane Droplets

Recent extensive studies reveal that surfactant-stabilized spherical alkane emulsion droplets spontaneously adopt polyhedral shapes upon cooling below a temperature T d while remaining liquid. Further cooling induces the growth of tails and spontaneous droplet splitting. Two mechanisms were offered to account for these intriguing effects. One assigns the effects to the formation of an intradroplet frame of tubules consisting of crystalline rotator phases with cylindrically curved lattice planes. The second assigns the sphere-to-polyhedron transition to the buckling of defects in a crystalline interfacial monolayer, known to form in these systems at some T s > T d . The buckling reduces the extensional energy of the crystalline monolayer’s defects, unavoidably formed when wrapping a spherical droplet by a hexagonally packed interfacial monolayer. The tail growth, shape changes, and droplet splitting were assigned to the decrease and vanishing of surface tension, γ. Here we present temperature-dependent γ(T), optical microscopy measurements, and interfacial entropy determinations for several alkane/surfactant combinations. We demonstrate the advantages and accuracy of the in situ γ(T) measurements made simultaneously with the microscopy measurements on the same droplet. The in situ and coinciding ex situ Wilhelmy plate γ(T) measurements confirm the low interfacial tension, ≲0.1 mN/m, observed at T d . Here, our results provide strong quantitative support validating the crystalline monolayer buckling mechanism.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2015

Effect of thermal history on Mossbauer signature and hyperfine interaction parameters of copper ferrite

Two specimens of copper ferrite, CuFe{sub 2}O{sub 4}, have been synthesized by double sintering ceramic technique with different thermal history i.e. slow cooled and quenched. X-ray diffractometry has confirmed single phase fcc spinel structure for slow cooled sample while tetragonal distortion is present in quenched sample. Mossbauer spectral analysis for slow-cooled copper ferrite reveals super position of two Zeeman split sextets along with paramagnetic singlet in the centre position corresponds to delafossite (CuFeO{sub 2}) phase that is completely absent in quenched sample. The hyperfine interaction parameters are highly influenced by heat treatment employed.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Process assessment of small scale low temperature methanol synthesis

Biomass is a renewable energy resource and has the potential to make a significant impact on domestic fuel supplies. Biomass can be converted to fuel like methanol via several step process. The process can be split into following main steps: biomass preparation, gasification, gas cooling and cleaning, gas shift and methanol synthesis. Untill now these configuration still has a problem like high production cost, catalyst deactivation, economy of scale and a huge energy requirements. These problems become the leading inhibition for biomass conversion to methanol, which should be resolved to move towards the economical. To address these issues, we developed various process and new configurations for methanol synthesis via methyl formate. This configuration combining two reactors: the one reactor for the carbonylation of methanol and CO to form methyl formate, and the second for the hydrogenolysis of methyl formate and H{sub 2} to form two molecule of methanol. Four plant process configurations were compared with the biomass basis is 300 ton/day. The first configuration (A) is equipped with a steam reforming process for converting methane to CO and H{sub 2} for increasing H{sub 2}/CO ratio. CO{sub 2} removal is necessary to avoid poisoning the catalyst. COSORB process used for the purpose of increasing the partial pressure of CO in the feed gas. The steam reforming process in B configuration is not used with the aim of reducing the number of process equipment, so expect lower investment costs. For C configuration, the steam reforming process and COSORB are not used with the aim of reducing the number of process equipment, so expect lower investment costs. D configuration is almost similar to the configuration A. This configuration difference is in the synthesis of methanol which was held in a single reactor. Carbonylation and hydrogenolysis reactions carried out in the same reactor one. These processes were analyzed in term of technical process, material and energy balance and economic analysis. The presented study is an attempt to compile most of these efforts in order to guide future work to get cheaper low cost investment. From our study the interesting configuration to the next development is D configuration with methanol yield 112 ton/day and capital cost with 526.4 10{sup 6} IDR. The configuration of D with non-discounted and discounted rate had the break-even point approximately six and eight years.

09 BIOMASS FUELS↗
DOE OSTI2021

A High-Fidelity Modeling Tool to Support the Design of Oxy-Combustors for Direct-Fired Supercritical CO2 Cycles

The challenge in the design of oxy-combustors for direct-fired supercritical CO 2 (sCO 2 ) cycles is in addressing disparate performance metrics and objectives. Key design parameters to consider include, among others, injector design for mixing and flame stability, split of recycled CO 2 diluent between injectors and cooling films, target flame temperatures to control noncondensable products, and strategies to inject the diluent CO 2 for film cooling and thermal control. In order to support novel oxy-combustor designs, a high-fidelity yet numerically efficient modeling framework based on the CRUNCH CFD® flow solver is presented, featuring key physics-based submodels relevant in this regime. For computational efficiency in modeling large kinetic sets, a flamelet/progress variable (FPV) based tabulated-chemistry approach is utilized featuring a three-stream extension to allow for the simulation of the CO 2 film cooling stream in addition to the fuel and oxidizer streams. Finite rate chemistry effects are modeled in terms of multiple progress variables for the primary flame as well as for slower-evolving chemical species such as NO x and SO x contaminants. Real fluid effects are modeled using advanced equations of states. The predictive capabilities of this computationally tractable design support tool are demonstrated on a conceptual injector design for an oxy-combustor operating near 30 MPa. Simulations results provide quantitative feedback on the effectiveness of the film cooling as well as the level of contaminants (CO, NO, and N) in the exhaust due to impurities entering from the injectors. These results indicate that this framework would be a useful tool for refining and optimizing the oxy-combustor designs as well as risk mitigation analyses.

Engineering↗
DOE OSTI2021

The Effect of an Equatorial Continent on the Tropical Rain Belt. Part 1: Annual Mean Changes in the ITCZ

The TRACMIP (Tropical Rain Belts with an Annual Cycle and Continent Model Intercomparison Project) ensemble includes slab-ocean aquaplanet controls and experiments with a highly idealized tropical continent, characterized by modified aquaplanet grid cells with increased evaporative resistance, increased albedo, reduced heat capacity, and no ocean heat transport (zero Q-flux). In the annual mean, an equatorial cold tongue develops west of the continent and induces dry anomalies and a split in the oceanic intertropical convergence zone (ITCZ). Ocean cooling is initiated by advection of cold, dry air from the winter portion of the continent; warm, humid anomalies in the summer portion are restricted to the continent by anomalous surface convergence. The surface energy budget suggests that ocean cooling persists and intensifies because of a positive feedback between a colder surface, drier and colder air, reduced downwelling longwave (LW) flux, and enhanced net surface LW cooling (LW feedback). A feedback between wind, evaporation, and SST (so-called WES feedback) also contributes to the establishment and maintenance of the cold tongue. Simulations with a gray-radiation model and simulations that diverge from protocol (with negligible winter cooling) confirm the importance of moist-radiative feedbacks and of rectification effects on the seasonal cycle. This mechanism coupling the continental and oceanic climate might be relevant to the double ITCZ bias. The key role of the LW feedback suggests that the study of interactions between monsoons and oceanic ITCZs requires full-physics models and a hierarchy of land models that considers evaporative processes alongside heat capacity as a defining characteristic of land.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2025

Cosmic-ray cooling in active galactic nuclei as a new probe of inelastic dark matter

We present a novel way to probe inelastic dark matter using cosmic-ray (CR) cooling in active galactic nuclei (AGNs). Dark matter (DM) in the vicinity of supermassive black holes may scatter off CRs, resulting in the rapid cooling of CRs for sufficiently large cross sections. This in turn can alter the high-energy neutrino and gamma-ray fluxes detected from these sources. We show that AGN cooling bounds obtained through the multimessenger data of NGC 1068 and TXS 0506 + 056 allows us to reach unprecedently large mass splittings for inelastic DM (≳ TeV), orders of magnitude larger than those probed by direct detection experiments and DM capture in neutron stars. Furthermore, we demonstrate that cooling bounds from AGNs can probe thermal light DM with small mass splittings. This provides novel and complementary constraints in parts of a parameter space accessible solely by colliders and beam-dump experiments.

astronomical black holes↗
DOE OSTI2024

Symmetry Breaking and Ascending in the Magnetic Kagome Metal FeGe

Spontaneous symmetry breaking—the phenomenon in which an infinitesimal perturbation can cause the system to break the underlying symmetry—is a cornerstone concept in the understanding of interacting solid-state systems. In a typical series of temperature-driven phase transitions, higher-temperature phases are more symmetric due to the stabilizing effect of entropy that becomes dominant as the temperature is increased. However, the opposite is rare but possible when there are multiple degrees of freedom in the system. Here, we present such an example of a symmetry-ascending phenomenon upon cooling in a magnetic kagome metal FeGe by utilizing neutron Larmor diffraction and Raman spectroscopy. FeGe has a kagome lattice structure with simple A-type antiferromagnetic order below Néel temperature T N ≈ 400 K and a charge density wave (CDW) transition at T CDW ≈ 110 K , followed by a spin-canting transition at around 60 K. In the paramagnetic state at 460 K, we confirm that the crystal structure is indeed a hexagonal kagome lattice. On cooling to around T N , the crystal structure changes from hexagonal to monoclinic with in-plane lattice distortions on the order of 10 − 4 and the associated splitting of the double-degenerate phonon mode of the pristine kagome lattice. Upon further cooling to T CDW , the kagome lattice shows a small negative thermal expansion, and the crystal structure gradually becomes more symmetric upon further cooling. A tendency of increasing the crystalline symmetry upon cooling is unusual; it originates from an extremely weak structural instability that coexists and competes with the CDW and magnetic orders. These observations are against the expectations for a simple model with a single order parameter and hence can only be explained by a Landau free energy expansion that takes into account multiple lattice, charge, and spin degrees of freedom. Thus, the determination of the crystalline lattice symmetry as well as the unusual spin-lattice coupling is a first step towards understanding the rich electronic and magnetic properties of the system, and it sheds new light on intertwined orders where the lattice degree of freedom is no longer dominant. Published by the American Physical Society 2024

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2016

Optical characteristics of p-type GaAs-based semiconductors towards applications in photoemission infrared detectors

Free-carrier effects in a p-type semiconductor including the intra-valence-band and inter-valence-band optical transitions are primarily responsible for its optical characteristics in infrared. Attention has been paid to the inter-valence-band transitions for the development of internal photoemission (IPE) mid-wave infrared (MWIR) photodetectors. The hole transition from the heavy-hole (HH) band to the spin-orbit split-off (SO) band has demonstrated potential applications for 3–5 μm detection without the need of cooling. However, the forbidden SO-HH transition at the Γ point (corresponding to a transition energy Δ{sub 0}, which is the split-off gap between the HH and SO bands) creates a sharp drop around 3.6 μm in the spectral response of p-type GaAs/AlGaAs detectors. Here, we report a study on the optical characteristics of p-type GaAs-based semiconductors, including compressively strained InGaAs and GaAsSb, and a dilute magnetic semiconductor, GaMnAs. A model-independent fitting algorithm was used to derive the dielectric function from experimental reflection and transmission spectra. Results show that distinct absorption dip at Δ{sub 0} is observable in p-type InGaAs and GaAsSb, while GaMnAs displays enhanced absorption without degradation around Δ{sub 0}. This implies the promise of using GaMnAs to develop MWIR IPE detectors. Discussions on the optical characteristics correlating with the valence-band structure and free-hole effects are presented.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2025

Ku-band electron linac for battery-powered hand-portable 2-MeV X-ray generator

X-ray generators, producing radiation in MeV range, are a critical tool for radiography, non-destructive testing and security applications. Field operation of such source requires them to be hand-portable, autonomous and allow parameter adjustability. RF linear accelerators can serve as a flexible, reliable, and robust radiation generator alternative to dangerous radioisotopes and bulky betatrons that are currently used for field radiography if their size, weight, cost, and imaging performance are matched to these sources. Here, in this paper, we present the design and test results of a 2 MeV Ku-band electron linac for a hand-portable X-ray generator system for field radiography being developed by RadiaBeam. The dramatic scale of miniaturization and cost-reduction is achieved thanks to the implementation of innovative technologies such as air-cooled Ku-band air-traffic control magnetrons, a split accelerating structure fabrication technique, and solid-state Marx modulators. This paper presents the design of the first prototype of the accelerator, its operation from Li-Ion batteries, as well as high-power and beam measurements.

43 PARTICLE ACCELERATORS↗
DOE OSTI2023

Mn(Pt 1–x Pd x ) 5 P: Isovalent tuning of Mn-sublattice magnetic order

Here, e report the growth and characterization of MnPd 5 P, a rare-earth-free ferromagnet, with T C ≈ 295 K and planar anisotropy, and conduct a substitutional study with its antiferromagnetic analogue MnPt 5 P. We provide a solution route to grow large single crystals of MnPd 5 P and the series Mn(Pt 1–x Pd x ) 5 P by adding Mn into Pd-P and (Pt 1–x Pd x )-P based melts. All compounds in the family adopt the layered anti-CeCoIn5 type structure with the space group P4/mmm, and EDS and X-ray diffraction results indicate that MnPt 5 P and MnPd 5 P form a complete solid solution. Based on measurements of the temperature- and field-dependent magnetization and resistance, we construct a temperature-composition (T-x) phase diagram for Mn(Pt 1–x Pd x ) 5 P and demonstrate that the initial antiferromagnetic order found in MnPt 5 P is extraordinarily sensitive to Pd substitution. At low Pd fractions (x < 0.010), the single antiferromagnetic transition in pure MnPt 5 P splits into a higher temperature ferromagnetic transition followed first, upon cooling, by a lower temperature ferromagnetic to antiferromagnetic transition and then by a re-entrant antiferromagnetic to ferromagnetic transition at even lower temperatures. The antiferromagnetic region makes up a bubble phase that persists up to x ≈ 0.008-0.009 for T ≈ 150 K, with all samples x < 0.008 recovering their initial ferromagnetic state upon further cooling to base temperature. Over the same low substitution range we find a non-monotonic change in the room temperature value of the unit cell volume, further suggesting that pure MnPt 5 P is very close to an instability. Once x > 0.010, Mn(Pt 1–x Pd x ) 5 P undergoes a only single transition into the ferromagnetic phase. The Curie temperature initially increases rapidly with x, rising from T C ≈ 197 K at x = 0.013 to a maximum of T C ≈ 312 K for x ≈ 0.62, and then falling back to T C ≈ 295 K for pure MnPd 5 P (x = 1.00). Given that Pt and Pd are isoelectronic, this work raises questions as to the origin of the extreme sensitivity of the magnetic ground state in MnPt 5 P upon introducing Pd.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2025

Design of a Structure for Assembly and Cooling the Magnet of the Next-Generation 45 GHz ECR Ion Source MARS-D

Here, the current Electron Cyclotron Resonance Ion Sources (ECRISs), constructed with Nb-Ti wires and the conventional racetrack-and-solenoid structure, have achieved operating frequencies up to 28 GHz and utilized about 90% of the critical current of the Nb-Ti wire. A Mixed Axial and Radial field System Demonstrator (MARS-D) is being developed at Lawrence Berkeley National Laboratory (LBNL). This system, which consists of an innovative hexagonal Closed-Loop Coil (CLC) and a set of solenoids, can generate higher magnetic fields (up to 150% ) while requiring only about 50% of the superconducting wire, enabling Nb-Ti wires to be used in the next-generation 45 GHz ECRIS. However, the assembly and cooling of such an efficient and compact magnet are particularly challenging due to the small radial gap between the CLC and solenoids, as well as the tight operating temperature margin. To address these challenges, a structure was developed that combines a three-section radially split solenoid mandrel with a series of shrink-fit reinforcement rings and cooling channels. This paper presents the detailed structure, manufacturing method, assembly procedure, impregnation method, mechanical Finite Element Analysis (FEA) comparison, and thermal FEA comparison.

ECR ion sources↗
DOE OSTI2014

Dynamically polarized target for the g{sup p}{sub 2} and G{sup p}{sub E }experiments at Jefferson Lab

Recently, two experiments were concluded in Hall A at Jefferson Lab which utilized a newly assembled, solid, polarized hydrogen target. The primary components of the target are a new, high cooling power {sup 4}He evaporation refrigerator, and a re-purposed, superconducting split-coil magnet. It has been used to polarize protons in irradiated NH{sub 3} at a temperature of 1 K and at fields of 2.5 and 5.0 tesla. Maximum polarizations of 55% and 95% were obtained at those fields, respectively. To satisfy the requirements of both experiments, the magnet had to be routinely rotated between angles of 0°, 6°, and 90° with respect to the incident electron beam.

43 PARTICLE ACCELERATORS↗
DOE OSTI2025

Intercalation induced quasi-freestanding layer in TiSe 2

Angle-resolved photoemission spectroscopy is employed to study the electronic structure of bulk TiSe 2 before and after doping with potassium impurities. A splitting in the conduction band into two branches is observed after room-temperature deposition. The splitting energy increases to approximately 130 meV when the sample is cooled to 40 K. One branch exhibits a nondispersive two-dimensional feature, while the other shows the characteristics of three-dimensional bulk band dispersion. Core-level spectroscopy suggests that the K impurities predominantly occupy the intercalated sites within the van der Waals gap. Furthermore, the results indicate the formation of a quasi-freestanding TiSe 2 layer. Additionally, doping completely suppresses the periodic lattice distortion in the surface region. These findings are further supported by density functional theory calculations, which compare the band structure of monolayer and bulk TiSe 2 with experimental data. Thus, the dimensional and intrinsic electronic properties of 1⁢𝑇−TiSe 2 can be controlled through the intercalation procedure used in this work.

36 MATERIALS SCIENCE↗
DOE OSTI2018

50-kW 1kV DC bus air-cooled inverter with 1.7 kV SiC MOSFETs and 3D-printed novel power module packaging structure for grid applications

The traditional heatsink design technologies for forced air-cooling and power semiconductors with low junction temperatures have constrained the converters to be designed with massive heatsinks. The low power losses of WBG device technology and higher junction temperature operation over a wide operating range of power have not been fully utilized with liquid-cooled systems. The other major limitation has also been the traditional power module packaging “stack” approach with baseplate. This paper presents a novel power stage design which involves 1.7 kV silicon carbide (SiC) MOSFETs, a heatsink design with Genetic Algorithm (GA) and built using 3D printing technology, and a novel integrated modular power module for high power density. The air-cooled module assembly has a SiC MOSFET phase leg module with split high-side and low-side switches and a gate driver with cross-talk and short circuit protection functions. The heatsink design was modeled using a co-simulation environment with finite element analysis software and GA in MATLAB and COMSOL. The proposed concepts were verified and validated through experiments at each stage of development. The power stage was evaluated at 800V, 900 V, and 1kV for 20 kHz switching frequency and 50-kW load. The experimental results show that the CEC efficiency is 98.4 %. In addition to the efficiency, a power density of 75 W/in 3 was also achieved.

Chinthavali, Madhu Sudhan↗
DOE OSTI2017

Assessment of the US Department of Energy's Sustainable Energy Resources for Consumers Grant Program

This report presents the results of an assessment of the Sustainable Energy Resources for Consumers (SERC) grant program that was administered by the US Department of Energy Weatherization and Intergovernmental Program Office. Grants totaling $90 million were awarded to 101 local weatherization agencies located in 27 states. More than 15,000 housing units were touched by the SERC program. Close to 29,000 SERC technologies were installed and/or services delivered. The report summarizes the results of site visits to 27 agencies in which the following 14 technologies were observed: solar photovoltaic panels, solar hot water heaters, solar thermal air panels for space heating, tankless water heaters, heat pump water heaters, geothermal heat pumps, super-evaporative cooling systems, combination boilers and indirect water heaters, small-scale residential wind systems, cool roofs, masonry spray foam insulation, attic radiant barriers, mini-split heat pumps, and in-home energy monitors. The evaluation found that the national weatherization network is capable of installing and delivering a wide range of new and innovative technologies, but the usability and adoptability of some technologies may prove impractical for the weatherization network and the demographic for which it serves.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2013

Infrared spectroscopy and tunneling dynamics of the vinyl radical in 4 He nanodroplets

Here, the vinyl radical has been trapped in 4 He nanodroplets and probed with infrared laser spectroscopy in the CH stretch region between 2850 and 3200 cm -1 . The assigned band origins for the CH 2 symmetric (ν 3 ), CH 2 antisymmetric (ν 2 ), and lone α-CH stretch (ν 1 ) vibrations are in good agreement with previously reported full-dimensional vibrational configuration interaction computations. For all three bands, a-type and b-type transitions are observed from the lowest symmetry allowed roconvibrational state of each nuclear spin isomer, which allows for a determination of the tunneling splittings in both the ground and excited vibrational levels. Comparisons to gas phase millimeter-wave rotation-tunneling and high-resolution jet-cooled infrared spectra reveal that the He solvent effect is to reduce the ground and ν 3 excited state tunneling splittings by ≈20%. This solvent-induced modification of the tunneling dynamics can be reasonably accounted for by assuming either a ≈2.5% increase in the effective barrier height along the tunneling coordinate or a ≈5% increase in the effective reduced mass of the tunneling particles.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2011

Energy Performance Comparison of Heating and Air Conditioning Systems for Multi-Family Residential Buildings

The type of heating, ventilation and air conditioning (HVAC) system has a large impact on the heating and cooling energy consumption in multifamily residential buildings. This paper compares the energy performance of three HVAC systems: a direct expansion (DX) split system, a split air source heat pump (ASHP) system, and a closed-loop water source heat pump (WSHP) system with a boiler and an evaporative fluid cooler as the central heating and cooling source. All three systems use gas furnace for heating or heating backup. The comparison is made in a number of scenarios including different climate conditions, system operation schemes and applicable building codes. It is found that with the minimum code-compliant equipment efficiency, ASHP performs the best among all scenarios except in extremely code climates. WSHP tends to perform better than the split DX system in cold climates but worse in hot climates.

15 GEOTHERMAL ENERGY↗
DOE OSTI2018

Superconducting Magnet Performance in LCLS-II Cryomodules

New LCLS-II Linear Superconducting Accelerator Cry-omodules are under construction at Fermilab. Installed in-side each SCRF Cryomodule is a superconducting magnet package to focus and steer an electron beam. The magnet package is an iron dominated configuration with conduc-tively cooled racetrack-type quadrupole and dipole coils. For easier installation the magnet can be split in the vertical plane. Initially the magnet was tested in a liquid helium bath, and high precision magnetic field measurements were performed. The first (prototype) Cryomodule with the magnet inside was built and successfully tested at Fermilab test facility. In this paper the magnet package is discussed, the Cryomodule magnet test results and current leads con-duction cooling performance are presented. So far magnets in nine Cryomodules were successfully tested at Fermilab.

Kashikhin, V.↗