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Analysis of Darkened Fragments Resulting from Laboratory Hypervelocity Experiments

NASA’s Orbital Debris Program Office (ODPO) relies on measurements from optical, radar, and in situ measurements to facilitate the development of data-driven orbital debris environmental engineering models such as the NASA Orbital Debris Engineering Model (ORDEM). For optical measurements, the ODPO relies on ground-based optical telescopes to statistically assess objects in geosynchronous orbit and, in the future, low Earth orbit (LEO). The data collected include the detected object’s orbital parameters, time of observation, and optical magnitude. The latter parameter can be converted to a size using NASA’s optical Size Estimation Model (oSEM). It is well known that the observed magnitude of orbital debris can vary based on an object's material constituents, observational geometry, and the effects of space weathering. To assess these magnitude variations, the ODPO uses the Optical Measurement Center (OMC) at NASA Johnson Space Center to characterize a variety of materials and fragments from laboratory impact tests representative of fragments that constitute the orbital debris population. One experiment was DebriSat: a 56 kg spacecraft was built to incorporate structural elements of a modern LEO spacecraft and was subjected to a hypervelocity impact test at the U.S. Air Force’s Arnold Engineering Development Complex using test parameters that may be encountered in LEO. The DebriSat project has provided an abundance of information for assessing fragmentation debris in terms of material, color, shape, size, density, mass, and other derived parameters. Prior to the impact test, the ODPO collected spectral measurements on a subset of the materials used to construct DebriSat for a “ground-truth” of their optical properties. After the successful hypervelocity impact test, the DebriSat team observed a fine, dark dust coating all the fragments. Prior research has suggested that this came from ablated material deposited on the fragments during the impact test, causing a change in the reflective properties [1]. Given that this lower reflectivity on the DebriSat fragments will influence the laboratory-acquired magnitudes used to calculate size and inform potential updates to the oSEM, it is critical to assess if this darkening effect on the DebriSat fragments is a laboratory bias or something that could occur in on-orbit breakup events. This presentation will provide a brief overview of the OMC and DebriSat experiment, focused on the optical characterization of a subset of materials using broadband photometric measurements and spectroscopic measurements. In addition, elemental analysis of various DebriSat fragments and the soft-catch foam used in the hypervelocity experiment compared with pristine foam will be examined to further evaluate the source of the dark material coating all fragments. Finally, the authors will present a twofold plan 1) for assessing potential biases in laboratory impact experiments that could affect laboratory optical characterization and 2) for mitigating biases when compared with ground-based optical telescopic measurements of the orbital debris environment.

Heather Cowardin↗

NASA NTRS1999

Edge-Flames in Von Karman Swirling Flows

Classical understanding of diffusion flames dictates that they, unlike the premixed flames, do not possess a characteristic propagation velocity and are constrained by stoichiometric requirements at the flame surface. However, it has been commonly observed that when local extinction occurs within a diffusion flame sheet, the edges that are formed propagate with distinct speeds. In general, the propagation speed of these edges depend on their geometrical shape (concave, convex, or straight) among other factors. Recently, Buckmaster investigated the dynamics of straight diffusion flame edges separating burning and quenched regions using simplified one-dimensional models. He showed that these flame edges can have positive, negative, or zero velocity depending on the Damkoehler number of the equilibrium diffusion flame that support them. It was also shown that this unsteady flame-edge behavior is intrinsically linked to S-curve behavior of the diffusion flame with varying Damkoehler number. When the system Damkoehler number lies between the extinction and ignition limits, flame edges can propagate as an "ignition wave" or as a "failure wave," and for a critical Damkoehler number remain as a stationary flame-edge. We have extend Buckmaster's 1-d model to more general edge-flame configurations where the edges appear as "flame holes" or as "flame disks". These two configurations along with the straight-edge case cover the entire range of possible edge-flame geometry observable in planar diffusion-flame sheets. A generalized map of edge-flame propagation velocities as a function of the system Damkoehler number and the edge-flame radius is presented. Experimentally we show that edge flames can be created using diffusion flames embedded in von Karman boundary layers. In a von Karman boundary layer, the flow is generated by spinning a solid (fuel) disk in a quiescent ambient gas. Under normal gravity we were able to produce "flame disks" over a range of fuel-disk rotational velocities varying from 0 to 20 revolutions per second, by orienting the burning surface of the fuel disk facing downward.

Nayagam, Vedha↗

NASA NTRS2021

A Method for Landsat and Sentinel 2 (HLS) BRDF Normalization

The Harmonized Landsat/Sentinel-2 (HLS) project aims to generate a seamless surface reflectance product by combining observations from USGS/NASA Landsat-8 and ESA Sentinel-2 remote sensing satellites. These satellites’ sampling characteristics provide nearly constant observation geometry and low illumination variation through the scene. However, the illumination variation throughout the year impacts the surface reflectance by producing higher values for low solar zenith angles and lower reflectance for large zenith angles. In this work, we present a model to derive the bidirectional reflectance distribution function (BRDF) normalization and apply it to the HLS product at 30m spatial resolution. It is based on the BRDF parameters estimated from the MODerate Resolution Imaging Spectroradiometer (MODIS) surface reflectance product (M{O,Y}D09) at 1 km spatial resolution using the VJB method (Vermote et al., 2009). Unsupervised classification (segmentation) of HLS images is used to disaggregate the BRDF parameters to the HLS spatial resolution and to build a BRDF parameters database at HLS scale. We first test the proposed BRDF normalization for different solar zenith angles over two homogeneous sites, in particular one desert and one Peruvian Amazon forest. The proposed method reduces both the correlation with the solar zenith angle and the coefficient of variation (CV) of the reflectance time series in the red and near infrared bands to 4% in forest and keeps a low CV of 3% to 4% for the deserts. Additionally, we assess the impact of the view zenith angle (VZA) in an area of the Brazilian Amazon forest close to the equator, where impact of the angular variation is stronger because it occurs in the principal plane. The directional reflectance shows a strong dependency with the VZA. The current HLS BRDF correction reduces this dependency but still shows an under-correction, especially in the near infrared, while the proposed method shows no dependency with the view angles. We also evaluate the BRDF parameters using field surface albedo measurements as a reference over seven different sites of the US surface radiation budget observing network (SURFRAD) and five sites of the Australian OzFlux network.

Belen Franch↗

DOE OSTI2023

Chiral Spectroscopy of Nanostructures

Chirality is ubiquitous in the universe and in living creatures over detectable length scales from the subatomic to the galactic, as exemplified in the two extremes by subatomic particles (neutrinos) and spiral galaxies. Between them are living creatures that display multiple levels of chirality emerging from hierarchically assembled asymmetric building blocks. Not too far from the bottom of this pyramid are the foundational building blocks with chiral atomic centers on sp 3 carbon atoms exemplified by L-amino acids and D-sugars that are self-assembled into higher-order structures with increasing dimensions forming highly complex, amazingly functional, and energy-efficient living systems. The organization and materials employed in their construction inspired scientists to replicate complex living systems via the self-assembly of chiral components. Multiple studies pointed to unexpected and unique electromagnetic properties of chiral structures with nanoscale and microscale dimensions, including giant circular dichroism and collective circularly polarized scattering that their constituent units did not possess. To address the wide variety of chiral geometries observed in continuous materials, singular particles, and their complex systems, multiple analytic techniques are needed. Simultaneously, their spectroscopic properties create a pathway to multiple applications. For example, mirror-asymmetric vibrations at chiral centers formed by sp 3 carbon atoms lead to optical activity for the infrared (IR) wavelength regions. At the same time, understanding the optical activity in, for example, the IR region enables biomedical applications because multiple modalities of biomedical imaging and vibrational optical activity (VOA) of biomolecules are known for IR range. In turn, VOA can be realized in both absorption and emission modalities due to large magnetic transition moments, as vibrational circular dichroism (VCD) or Raman optical activity (ROA) spectroscopy. In addition to the VOA, in the range of longer wavelengths, lattice vibrational mode or phononic behavior occurs in chiral crystals and nanoassemblies, which can be readily detected by terahertz circular dichroism (TCD) spectroscopy. Meanwhile, chiral self-assembly can induce circularly polarized light emission (CPLE) regardless of the existence of chirality in coassembled fluorophores. The CPLE from self-assembled chiral materials is particularly interesting because the CPLE can originate from both circularly polarized luminescence and circularly polarized scattering (CPS). Furthermore, because self-assembled nanostructures often exhibit stronger optical activity than their building blocks owing to dimension and resonance effects, the optical activity of single assembled nanostructures can be investigated by using microscopic technology combined with chiral optics. Here, we describe the state of the art for spectroscopic methods for the comprehensive analysis of chiral nanomaterials at various photon wavelengths, addressed with special attention given to new tools emerging both for materials with self-organized hierarchical chirality and single-particle spectroscopy.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Spectral Fidelity of Earth's Terrestrial and Aquatic Ecosystems

The Surface Biology and Geology (SBG) investigation will create global maps of spectral surface reflectance and emissivity at a cadence of 16 days or better, with coverage to address global questions about Earth's geology, cryosphere and ecosystems. The revolutionary potential poses a commensurate challenge: creating contiguous maps free from regional biases induced by atmosphere, observation geometry, or inversion error. This will require an accurate calibration with precise knowledge of each channel's spectral response. In this work, we quantify the impact of spectral calibration on SBG's aquatic and terrestrial ecosystem objectives. We find that contemporary algorithms for ecosystem trait retrieval demand more accurate spectral calibration than historical missions. Errors due to drift or spatial nonuniformity in the wavelength calibration that have previously been considered acceptable can cause systematic errors larger than the instrument noise and of the same order as the variability SBG aims to measure. Moreover, their impact on atmospheric correction can induce climate-dependent systematic errors that thwart comparisons between ecosystems. These results underscore the importance of spectral response accuracy in SBG mission design.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

Tris(carbene)borates; alternatives to cyclopentadienyls in organolanthanide chemistry

The chemistry of the tris-carbene anion phenyltris(3-alkyl-imidazoline-2-yliden-1-yl)borate, [C3 Me ] - ligand, is initiated for f-block metal cations. Neutral, molecular complexes of the form Ln(C3) 2 I are formed for cerium(III), while a separated ion pair [Ln(C3) 2 ]I forms for ytterbium(III). DFT/QTAIM computational analyses of the complexes and related tridentate tris(pyrazolyl)borate (Tp) – supported analogs demonstrates the anticipated strength of the σ donation and confirms greater covalency in the metal–carbon bonds of the [C3 Me ] - complexes in comparison with those in the Tp Me,Me complexes. The DFT calculations demonstrate the crucial role of THF solvent in accurately reproducing the contrasting molecular and ion-pair geometries observed experimentally for the Ce and Yb complexes.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

TriWaSp: a multi-faceted visible spectroscopy diagnostic on the ST40 tokamak

Here, we present a new state-of-the-art Triple Wavelength Spectrometer (TriWaSp), recently deployed on ST40, a high field low aspect ratio spherical tokamak. The TriWaSp has a range of possible applications due to its flexible design; the current configuration focuses on charge exchange recombination spectroscopy from carbon and neon impurities in the ST40 plasma. This paper discusses the detailed setup of the system and presents initial charge exchange ion temperature measurements using a single line of sight, which show good agreement with other ion temperature diagnostics. Building on these commissioning results and forward modelling of the system, a new observation geometry has been implemented for the next experimental campaign which will considerably improve the localisation of ion temperature and velocity profile measurements.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2022

Deep-learning-guided high-resolution subsurface reflectivity imaging with application to ground-penetrating radar data

Subsurface reflectivity imaging is one of the most important geophysical characterization methods for revealing subsurface structures. In many cases, accurate subsurface reflectivity imaging is challenging because of, for example, random or coherent noise in the data and sparse source-receiver observation geometry. Here, we develop a deep-learning-guided iterative imaging method to improve subsurface structure imaging. Specifically, we train a supervised neural network to infer a noise-free, high-resolution image from a noisy, low-resolution image and use this estimated image as guidance to regularize least-squares imaging. We develop a systematic method to generate high-quality synthetic training data (data-label pairs) to train the guidance neural network. The trained neural network can provide high-fidelity predictions even for field-data images that are not in the training data. We validate our new imaging method using one synthetic and two field ground-penetrating radar data examples, and find that our method can produce clean, high-resolution subsurface reflectivity images where existing single-pass and least-squares imaging methods fail due to noise and insufficient data coverage.

58 GEOSCIENCES↗

DOE OSTI2026

Fyn–Saracatinib Complex Structure Reveals an Active State-like Conformation

Fyn is a Src-family tyrosine kinase implicated in synaptic dysfunction and neuroinflammation across multiple neurodegenerative disorders, including Alzheimer’s disease (AD) and Parkinson’s disease (PD). Saracatinib (AZD0530) is a potent Src-family inhibitor that has been explored as a repurposed therapeutic; however, its clinical utility is limited by poor kinase selectivity caused by high sequence conservation within Src-family ATP-binding sites. Here, we combine surface plasmon resonance (SPR) and X-ray crystallography to define saracatinib recognition by the Fyn kinase domain (KD). SPR single-cycle kinetics shows that saracatinib binds the isolated Fyn KD and full-length Fyn with low-nanomolar affinity, whereas dasatinib binds with subnanomolar affinity and markedly slower dissociation. We determined the crystal structure of the Fyn KD-saracatinib complex at 2.22 Å resolution. The kinase adopts an active-like conformation with the DFG motif and αC-helix in the ‘in’ state and a conserved β3 αC Lys-Glu salt bridge. Saracatinib occupies the adenine and ribose pockets, and engages the hinge through direct and water-mediated hydrogen bonding while complementing a hydrophobic back pocket by van der Waals contacts. Comparison with reported saracatinib-bound structures of other kinases suggests that the active-state geometry observed for Fyn creates a pocket not observed in inactive-like complexes, providing a structural handle for designing Fyn-selective inhibitors. Comparison with all saracatinib-bound kinase co-structures currently available in the PDB (ALK2 and PKMYT1) indicates a conserved monodentate hinge binding mode but kinase-dependent αC-helix conformations, providing a structural rationale for designing Fyn-selective analogues.

AZD0530↗

NASA NTRS1974

Error analysis for station position from tracking of the Lageos satellite

The earth physics satellite systems error analysis program was applied to the problem of predicting the relative accuracy of station position determinations under varying orbital and observing geometries. The reference case consists of nine ground stations extending over 1500 km which lasers ranged to a LAGEOS satellite, with simultaneous Doppler tracking from a geosynchronous satellite for 16 days. Eleven variations from the reference case were tested. The results showed little sensitivity to whether the LAGEOS altitude is 3700 or 5690 km. More significant were the high inclination, and that LAGEOS was tracked by a geosynchronous satellite.

Parmenter, M. E.↗

NASA NTRS1974

Infrared measurements of stratospheric composition

The observational techniques and results of IR measurements of the minor and trace molecular composition of the lower stratosphere are reviewed. Emphasis is given to those theoretical aspects of the formation of emission and absorption spectra which affect the quantitative interpretation of observational data in terms of the vertical distribution of observed molecular species. The principal experimental techniques currently being used are briefly reviewed, followed by a detailed summary of current knowledge of the abundances and spatial variability of the known minor constituents. The question of the determination of the minimum detectable concentration of a constituent molecule and its relationship to the instrumental parameters, the molecular transition intensities, and observation geometry is discussed; upper limit concentrations are given for some additional species of importance in current stratospheric studies.

Farmer, C. B.↗

NASA NTRS1979

Analysis of Viking infrared thermal mapping data of Mars. The effects of non-ideal surfaces on the derived thermal properties of Mars

The thermal interia of the surface of Mars varies spatially by a factor of eight. This is attributable to changes in the average particle size of the fine material, the surface elevation, the atmospheric opacity due to dust, and the fraction of the surface covered by rocks and fine material. The effects of these non-ideal properties on the surface temperatures and derived thermal inertias are modeled, along with the the effects of slopes, CO2 condensed onto the surface, and layering of fine material upon solid rock. The non-ideal models are capable of producing thermal behavior similar to that observed by the Viking Infrared Thermal Mapper, including a morning delay in the post-dawn temperature rise and an enhanced cooling in the afternoon relative to any ideal, homogeneous model. The enhanced afternoon cooling observed at the Viking-1 landing site is reproduced by the non-ideal models while that atop Arsia Mons volcano is not, but may be attributed to the observing geometry.

Muhleman, D. O.↗

NASA NTRS1980

The plane of symmetry of interplanetary dust in the inner solar system

Observations of the zodiacal light from the space probes Helios 1 and 2 between 1.0 and 0.3 AU show - superimposed on the general radial dependence - a systematic variation of brightness and brightness distribution with position in the orbit which is caused by the inclination of the symmetry plane of interplanetary dust with respect to the ecliptic. By suitable choice of the observing geometry, the inclination and the ascending node of the symmetry plane can be determined directly from the data without recourse to model calculations. The resulting values of i equals 3.0 plus or minus 0.3 deg, Omega equals 87 plus or minus 4 deg are not compatible with a concentration of interplanetary dust to the invariable plane of the solar system. The data support the simple view that the distribution of interplanetary dust in the inner solar system is characterized throughout by one plane of symmetry and suggest that this plane extends to at least 1 AU.

Leinert, C.↗

NASA NTRS1980

Fracture trace expression and analysis in radar imagery of rain forest terrain (Peru)

Mapping of minor lineaments from radar imagery of the rain forest in southeast Peru is biased due to the selective suppression of some topography which results from the observation geometry of the imaging radar system and the varied perception of lineaments on the imagery by different interpreters. Team analysis of the imagery compensates for several of the sources of bias, and results in the clear recognition of differing regimes within the regional fracture field in the study area.

Martin-Kaye, P. H. A.↗

NASA NTRS1981

Observations of polar aurora on Jupiter

North-south spatial maps of Jupiter were obtained with the SWP camera in IUE observations of 10 December 1978, 19 May 1979, and 7 June 1979. Bright auroral emissions were detected from the north and south polar regions at H Ly alpha (1216 A) and in the H2 Lyman bands (1250-1608 A) on 19 May 1979; yet no enhanced polar emission was detected on the other days. The relationship between the IUE observing geometry and the geometry of the Jovian magnetosphere is discussed.

Lane, A. L.↗

NASA NTRS1982

Comparative analysis of co-registered SIR-A, Seasat and Landsat images

A number of areas were covered by Seasat SAR and SIR-A, thus providing information at two different incidence angles (20 deg and 50 deg respectively). These angles correspond to scattering from two different surface roughness scales. The results of the analysis from two areas will be presented. The first is the San Rafael area in Utah where Seasat/SIR-A/Landsat data were coregistered and discriminant analysis is being applied to classify surface units. The second area is the Chotts area in Algeria where appreciable changes have been observed between Seasat and SIR-A images. However, it is not clear if the changes are due to the different observation geometry or changes in the surface between 1978 and 1981.

Elachi, C.↗

NASA NTRS1986

Tracking Landsat-5 by a differential GPS technique

As part of an international campaign to develop precise geodetic applications of the Global Positioning System (GPS), the Jet Propulsion Laboratory is conducting a demonstration of differential GPS tracking using Landsat-5. Two strategies have been investigated: one in which only the Landsat-5 orbit is estimated, and one in which both the Landsat-5 and GPS orbits are estimated together. Error studies show that under the limited conditions of the experiment, three-dimensional Landsat-5 position accuracies of about 5 m with the first strategy and 2 m with the second strategy can be achieved over a 20-min period of good observing geometry. Orbit determination results using a version of the first strategy appear to achieve the 5 m goal. This is supported by various formal error measures and independent comparisons. The more powerful strategy has yet to be carried out.

Yunck, T. P.↗

NASA NTRS1988

UV resonance line dayglow emissions on earth and Jupiter

The similarities and differnces between atomic resonance line emissions on earth and Jupiter are studied. For earth, the scattering of the conservative atomic oxygen triplet transition at 1304 A and the nonconservative atomic oxygen sextuplet at 989 A is considered. For Jupiter, the scattering of the conservative atomic hydrogen doublet at 1216 A and the nonconservative atomic hydrogen doublet at 1026 A are addressed. Models are presented for the intensities of the emission features as seen from a distance of several planetary radii, using the same observational geometry for both earth and Jupiter. Variations of the line-integrated emissions across the disk and near the limb of each planet are examined in detail. Line profiles for the emission near the limb and at disk-center are also studied. The models reveal the importance of including inhomogeneities and temperature variations of the atmosphere in scattering models, and indicate that outer planet emissions previously interpreted as 'electroglow' may be solely due to resonant scattering of solar emissions.

Gladstone, G. Randall↗