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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Absolute measurement of vacuum ultraviolet photon flux in an inductively coupled plasma using a Au thin film

A new method for absolute measurement of the vacuum ultraviolet (VUV) photon flux at the edge of a plasma is described. The light produced by the plasma was allowed to strike a negatively biased, gold-coated copper substrate remote from the plasma. The resulting photoelectron emission current was measured, and the absolute photon flux was then found from the known photoelectron yield of Au. The method was used to quantify the amount of VUV light produced by an Ar/He inductively coupled plasma (ICP). Strong emissions at 104.82 and 106.67 nm, corresponding to the 1s 2 and 1s 4 resonant states of Ar, were observed. The maximum, integrated VUV photon flux measured at the remote location was 3.2 × 10 13 photons/cm 2 s. This was estimated to correspond to a flux of 5 × 10 15 photons/cm 2 s at the edge of the ICP, in the range of reported values under similar conditions.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2020

High-temperature all-fiber non-destructive multi-parameter sensing system with consistent performance

A high-temperature all-fiber non-destructive multi-parameter sensing system is developed. The system can operate consistently in a wide range of temperature changes by specially designed active signal generation and detection units. It is capable of monitoring temperature up to 600°C and cracks on metal pipes with an acoustic wave generation unit and an acoustic detection unit. A gold-coated multi-mode fiber is used to deliver a laser pulse for acoustic excitation while minimizing parasitic acoustic signals at high temperature. An in-fiber Fabry–Perot fiber Bragg grating (FP-FBG) is fabricated in another single-mode fiber and bonded to the test object for acoustic detection. The FP-FBG avoids strain redistribution inside the bonder at high temperature to ensure consistent operation. The feasibility of the system for temperature monitoring and crack detection in real-world applications is also demonstrated on an industry-standard P91 pipe.

He, Jiaji (ORCID:0000000165661887)↗
DOE OSTI2020

The Effect of Adsorbed Volatile Organic Compounds on an Ultrathin Water Film Measurement

Using surface plasmon resonance imaging (SPRi), we have recently shown for the first time the existence of a monolayer water film between droplets during dropwise condensation. This study examines the effect of adsorbed volatile organic compounds (VOCs) on the ultrathin film measurement using SPRi. Further, the work presents the proper surface-treatment process that enables measurements of the ultrathin water layer during high-speed imaging of dropwise condensation at 3000 frame per second. In this study, two methods were applied for cleaning the surface (gold-coated glass)—(1) standard cleaning procedure (SCP) using acetone, isopropyl alcohol, and deionized water and (2) SCP followed by air plasma cleaning. This work discusses the effect of the cleaning procedures on surface roughness, contact angle, and surface chemistry using atomic force microscopy, optical microscopy, and an X-ray photoelectron spectroscope meter. The results showed that SCP before the SPRi is a proper surface-treatment method. The effect of adsorbed VOCs during dropwise condensation on a surface treated with SCP was measured to be 0.0025 (reflectivity unit), which was 70% smaller than the reflectance associated with a monolayer water film. The results of this work confirm a monolayer water film observation during the dropwise condensation, which has been reported before.

36 MATERIALS SCIENCE↗
NASA NTRS1965

Plated nickel wire mesh makes superior catalyst bed

Porous nickel mesh screen catalyst bed produces gas evolution in hydrogen peroxide thrust chambers used for attitude control of space vehicles. The nickel wire mesh disks in the catalyst bed are plated in rugose form with a silver-gold coating.

Sill, M.↗
NASA NTRS1968

Thermal protective visor for entering high temperature areas

Chamber observer suit visor protects the eyes and ears of the wearer while he is performing rescue operations during a fire. The visor is a simple curved sandwich of selected glass plates, gold coated polyester plastic film, and a dead air space, all mounted in an aluminum frame.

Burgett, F. A.↗
NASA NTRS1973

High resolution rocket EUV solar spectrograph.

The design and performance of an Aerobee 150 rocket-borne solar spectrograph covering a wavelength range of 10 to 385 A are discussed. The spectrograph uses a gold-coated replica concave grating of 3-m radius with 1200 grooves/mm at an angle of incidence of 88 deg. The spectra are recorded on glass photographic plates making possible wavelength determination to 0.003 A if known standard wavelengths occur frequently enough. Special attention to scattered light made possible the photographing of the solar spectrum from 60 to 385 A without using filters to absorb the strong visible and UV sunlight, although the solar spectrum was also recorded through metal foil filters. In the laboratory the spectrograph has been used to record spectra of highly ionized metals with a resolution of 0.03 A or better.

Behring, W. E.↗
NASA NTRS1974

GaAs laser diode pumped Nd:YAG laser

A 1.5-mm by 3-cm neodymium-ion doped YAG laser rod has been side pumped using a GaAs laser diode array tuned to the 8680-A absorption line, achieving a multimode average output power of 120 mW for a total input power of 20 W to the final-stage laser diode drivers. The pumped arrangement was designed to take advantage of the high brightness of a conventional GaAs array as a linear source by introducing the pump light through a slit into a close-wrapped gold coated pump cavity. This cavity forms an integrating chamber for the pump light.

Conant, L. C.↗
NASA NTRS1975

A study of molecular contamination

Contamination kinetics of typical space materials were studied using several techniques, including ellipsometry. Data were obtained on contaminant deposition rates, sticking coefficients, and reevaporation of the contamination. Materials studied included silicone sealants, a thermal control paint, and a graphite laminate as contaminant sources, and gold coated surfaces, a thermal control paint and a second surface mirror material as the contaminees. Both deposition and reevaporation rates were found to be nonlinear with time, and followed an exponential decay. A hypothesis is presented that the nonlinear behavior was a result of disproportionation of the molecular weight fractions of the polymers. The measured sticking coefficients were found to vary substantially with temperature over narrow ranges. Simulated space radiation was found to reduce the evaporation rates of contaminants by several orders of magnitude.

Allen, T. H.↗
NASA NTRS1976

Photoelectrolytic Production of Hydrogen Using Semiconductor Electrodes

Experimental data for the photoelectrolytic production of hydrogen using GaAs photoanodes was presented. Four types of GaAs anodes were investigated: polished GaAs, GaAs coated with gold, GaAs coated with silver, and GaAs coated with tin. The maximum measured efficiency using a tungsten light source was 8.9 percent for polished GaAs electrodes and 6.3 percent for tin coated GaAs electrodes.

Byvik, C. E.↗
NASA NTRS1977

Fabrication and performance of intrinsic germanium photodiodes

The paper presents fabrication details for an intrinsic germanium photodiode developed for study of atmospheric constituents, the airglow and auroras in the 1-2 micron spectral range. Attention is given to cutting of the single crystal, spreading of the lithium dispersion, sputtering of a gold coating, and surface passivation. A wavelength response curve is presented.

Beiting, E. J., III↗
NASA NTRS1979

Determination of total surface reflectivity

Method of measuring total reflectance employs relatively inexpensive reflectometer with gold-coated hemispherical reflector. Light sources may be tungsten lamp for visable region, or Globar lamp for infrared.

Desmet, D. J.↗
NASA NTRS1982

Very high X-ray efficiency from a blazed grating

The efficiency of X-ray diffraction from reflection gratings has been investigated experimentally using a gold-coated plane grating of 25 x 120 mm with a nominal blaze angle of 21 deg in a conical diffraction mount. Results show that conical diffraction is capable of producing very high dispersion efficiencies. The peak of first order at 13.3 A is 40%; at 44 A, the peak is 34%. The most immediate application of this result is to X-ray astronomy where sources are weak.

Cash, W.↗
NASA NTRS1985

The experimental computer control of a two-dimensional hyperbolic system

The experimental computer control of a two-dimensional hyperbolic system is described. The system consists of a 5-foot gold-coated rubber membrane mounted on a circular cylindrical drum. Seven electrodes reside on a command surface located behind the membrane inside the drum. These electrodes served as capacitive sensors and electrostatic force actuators of transverse membrane deflection. The membrane was modelled as flat, isotropic and uniformly tensioned. Transverse membrane deflections were expanded in normal modes. Controllers regulating membrane deflection are designed using aggregation and design procedures based upon sensor and actuator influence functions. The resulting control laws are implemented on a minicomputer in two sets of experiments. The experimental study confirms the theoretically predicted behavior of the system, usefulness of the aggregation and design procedures, and the expectation that spillover can be made a beneficial source of damping in residual systems.

Yam, Y.↗
NASA NTRS1983

New techniques for fusion bonding and replication for large glass reflectors

Lightweight, space-deployable glass honeycomb telescope primary mirror structures are produced by a novel method which involves the heating to softening temperature of many borosilicate or silica glass tube sections that are packed to form a honeycomb matrix and filled with a high expansion coefficient refractory sand. The close packed tubes yield a hexagonal-cell honeycomb. Attention is given to the results of an experiment in which a highly refractory master was used to shape a honeycomb of less refractory glass, employing a 1-micron thick, vacuum-deposited gold coating as a parting layer between the two.

Angel, J. R. P.↗
NASA NTRS1985

The LAMAR telescope module for high throughput imaging and spectroscopy

Kirkpatrick-Baez mirror assemblies for the LAMAR experiment of the Space Shuttle are described. The aperture is 20 cm x 30 cm and the distance from the front of the mirror to the focal plane is 3.4 m. The reflectors are made from 1.8 mm gold coated float glass. A prototype brassboard mirror was constructed with only one-third of the plates. Its angular resolution is 35 arcsec (HPW) in visible light. X-ray tests over small areas indicate very little scattering. The fabrication technique is applicable to larger mirror systems such as those of XMM. The use of flatter material for the reflectors results in better angular resolution.

Gorenstein, P.↗
NASA NTRS1986

X-ray telescope module for the LAMAR Space Shuttle experiment

The first of eight X-ray telescopes is under construction for the LAMAR experiment. Each consists of two orthogonal sets of nested confocal one-dimensional parabolic plates of gold-coated float glass, selected for flatness from commercial stock. Each is initially bent to a cylinder by bonding a thin, highly curved titanium sheet to its inactive surface. The final parabolic figure is produced by an automated system which includes seven diode arrays that detect a visible-light line image. Eight precise motorized linear translators operating under the control of a computer, tune the plate to the optimum figure. The plate is then fixed in position by epoxy bonds. The precision of the system is several arcsec, but the intrinsic flatness of the glass is expected to limit the half-power diameter (HPD) of the telescope to about 25 arcsec.

Gorenstein, P.↗
NASA NTRS1987

Noncontact true temperature measurement

A laser pyrometer has been developed for acquiring the true temperature of a levitated sample. The laser beam is first expanded to cover the entire cross-sectional surface of the target. For calibration of such a system, the reflectivity signal of an ideal 0.95 cm diameter gold-coated sphere (reflectivity = 0.99) is used as the reference for any other real targets. The emissivity of the real target can then be calculated. The overall system constant is obtained by passively measuring the radiance of a blackbody furnace (emissivity = 1.0) at a known, arbitrary temperature. Since the photo sensor used is highly linear over the entire operating temperature range, the true temperature of the target can then be computed. Preliminary results indicate that true temperatures thus obtained are in excellent correlation with thermocouple measured temperatures.

Lee, Mark C.↗
NASA NTRS1989

Degradation and crosslinking of perfluoroalkyl polyethers under X-ray irradiation in ultrahigh vacuum

Degradation of three types of commercially available perfluoroalkyl polyethers (PFPE)-Demnum S200, Fomblin Z25, and Krytox 16256-by X-ray irradiation was studied by using X-ray photoemission spectroscopy (XPS) and a mass spectrometer under ultra-high-vacuum conditions. The carbons in the polymers were characterized by chemical shifts of Cls binding energies. Gaseous products containing COF2 and low-molecular-weight fluorocarbons were formed. From Fomblin Z25, which has acetal linkages (-OCF2O-), a large quantity of COF2 gas was evolved. Liquid products became tacky after a long irradiation time, and some did not dissolve in Freon. High-pressure liquid chromatography (HPLC) showed that molecular weight distribution became broader and that higher molecular weight polymers were formed from Demnum and Krytox. We concluded from these results that degradation and cross-linking took place simultaneously. Demnum crosslinked more easily than the other fluids. The time dependence of both XPS spectra of Cls and mass spectra showed that C-O-bonded carbons in PFPE'S were removed faster than other carbons. There was no substrate effect on the degradation reaction because the first-order rate constants calculated from the change of gaseous products were similar when stainless steel (440C) and gold-coated surfaces were used. Metal fluorides were formed on stainless steel during the reaction. A mechanism for the degradation of PFPE'S is discussed on the basis of their molecular structures.

Mori, Shigeyuki↗