Performance Improvement of the CHeX Flight Cryostat
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Advances in cryogenic electron microscopy have opened new avenues for probing quantum phenomena in correlated materials. This study reports the installation and performance of a new side-entry condenZero cryogenic cooling system for JEOL (Scanning) Transmission Electron Microscopes (S/TEM), utilizing compressed liquid helium (LHe) and designed for imaging and spectroscopy at ultra-low temperatures. The system includes an external dewar mounted on a vibration-damping stage and a pressurized, low-noise helium transfer line with a remotely controllable needle valve, ensuring stable and efficient LHe flow with minimal thermal and mechanical noise. Performance evaluation demonstrates a stable base temperature of 4.37 K measured using a Cernox bare chip sensor on the holder with temperature fluctuations within ±0.004 K. Complementary in-situ electron energy-loss spectroscopy (EELS) via aluminum bulk plasmon analysis was used to measure the local specimen temperature and validate cryogenic operation during experiments. The integration of cryogenic cooling with other microscopy techniques, including electron diffraction and Lorentz TEM, was demonstrated by resolving charge density wave (CDW) transitions in NbSe2 using electron diffraction, and imaging nanometric magnetic skyrmions in MnSi via Lorentz TEM. In conclusion, this platform provides reliable cryogenic operation below 7 K, establishing a low-drift route for direct visualization of electronic and magnetic phase transformations in quantum materials.
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Modified stainless steel Dewar aids rotating beam fatigue test in a cryogenic environment. The Dewar is modified to receive extended specimen supporting members through specially designed rotary seals. The test set can be fully enclosed and pressurized with an inert gas to make the system explosion proof.
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Transparent vinyl tent is designed for easy assembly with minimum use of handtools. Tent prevents toxic or explosive vapors from entering building. Frame posts are mounted on casters to allow easy mobility.
In continuation of single-conductor studies, quench onset data of quasi-steady operation are reported for a Formvar-coated composite (Nb48Ti/Cu) in bundle geometry (conductor thickness about 0.2 cm, approximately square cross section). Overall thermal conductances of the heater simulation technique applied are of the order 0.1 W/(sq cm-K), comparable to single-specimen results, around 4 K and below the lambda transition in agreement with model predictions. Considerable deterioration, however, occurs below 3 K and down to the lambda temperature during operation in near-saturated He I. Consequences for magnets of intermediate energy density are discussed with emphasis on the modifications necessitated by coatings.
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This paper describes the experiment to measure the singularity of the specific heat of helium around the lambda transition at 2.177 Kelvin, with nano Kelvin resolution.
A multi-purpose, cylindrical thermal insulation test apparatus is used for testing insulation materials and systems of materials using a liquid boil-off calorimeter system for absolute measurement of the effective thermal conductivity (k-value) and heat flux of a specimen material at a fixed environmental condition (cold-side temperature, warm-side temperature, vacuum pressure level, and residual gas composition). The apparatus includes an inner vessel for receiving a liquid with a normal boiling point below ambient temperature, such as liquid nitrogen, enclosed within a vacuum chamber. A cold mass assembly, including the upper and lower guard chambers and a middle test vessel, is suspended from a lid of the vacuum canister. Each of the three chambers is filled and vented through a single feedthrough. All fluid and instrumentation feedthroughs are mounted and suspended from a top domed lid to allow easy removal of the cold mass. A lift mechanism allows manipulation of the cold mass assembly and insulation test article.
A multi-purpose, cylindrical thermal insulation test apparatus is used for testing insulation materials and systems of materials using a liquid boil-off calorimeter system for absolute measurement of the effective thermal conductivity (k-value) and heat flux of a specimen material at a fixed environmental condition (cold-side temperature, warm-side temperature, vacuum pressure level, and residual gas composition). An inner vessel receives liquid with a normal boiling point below ambient temperature, such as liquid nitrogen, enclosed within a vacuum chamber. A cold mass assembly, including upper and lower guard chambers and middle test vessel, is suspended from a lid of the vacuum canister. Each of the three chambers is filled and vented through a single feedthrough. All fluid and instrumentation feedthroughs are mounted and suspended from a top domed lid allowing easy removal of the cold mass. A lift mechanism allows manipulation of the cold mass assembly and insulation test article.
The South Pole Telescope Shirokoff Line Intensity Mapper (SPT-SLIM) is a millimeter-wavelength line-intensity mapping experiment, which was deployed on the South Pole Telescope (SPT) during the 2024-2025 Austral summer season. This pathfinder experiment serves to demonstrate the on-sky operation of multi-pixel on-chip spectrometer technology. We report on the cryogenic performance of the SPT-SLIM receiver for the first year of commissioning observations. The SPT-SLIM receiver utilizes an Adiabatic Demagnetization Refrigerator (ADR) for cooling the focal plane of superconducting filterbank spectrometers to a temperature of 150 mK. We demonstrate stable thermal performance of the focal plane module during observations consistent with thermal modeling, enabling a cryogenic operating efficiency above 80%. We also report on the receiver control system design utilizing the Observatory Control System (OCS) platform for automated cryogenic operation on the SPT.
The Long-Baseline Neutrino Facility (LBNF) situated at the Sanford Underground Research Facility (SURF) in Lead, South Dakota, serves as the host for the Deep Underground Neutrino Experiment (DUNE), employing cryostats with nearly 70,000 metric tons of high purity liquid argon (LAr). The integrity of LAr quality is pivotal in determining the electron lifetime within DUNE, directly impacting its signal-to-noise ratio. Specifically, Far Detector 1 (FD-1) in cryostat 1 requires an electron lifetime over 3 ms within its 3.5 m drift, corresponding to less than 100 parts-per-trillion (ppt) Oxygen equivalent contamination. Far Detector 2 (FD-2) in cryostat 2 demands over 6 ms electron lifetime within its 6.0 m drift, corresponding to less than 50 ppt Oxygen equivalent contamination. Nitrogen (N2) absorption of LAr scintillation light, known as quenching, necessitates N2 contamination in LAr to remain below 1 ppm to minimize photon loss and enhance energy reconstruction. Studies indicate that at 1 ppm N2, approximately 20% of scintillation light is lost, highlighting the importance of minimizing N2 contamination. Brazil State University of Campinas's (UNICAMP) contribution to LBNF focuses on developing argon purification and regeneration for DUNE FD-1 and FD-2. To that effect, they constructed a test facility to perform studies on LAr purification at a smaller scale, the Purification Liquid Argon Cryostat (PuLArC) with approximately 90 liters of LAr. One of the filtration materials was considered and tested Li-FAU molecular sieve. Value engineering on argon purification media was conducted, leading to the identification of Li-FAU zeolite's ability to effectively capture N2 impurities during LAr circulation. Testing at UNICAMP's PuLArC facility demonstrated that 1 kg of Li-FAU is capable of reducing N2 contamination from 20-50 ppm to 0.1-1.0 ppm within 1-2 hours of circulation. In October 2023, testing at the Iceberg cryostat in Fermilab's Noble Liquid Test Facility (NLTF), with approximately 2,625 liters of LAr, confirmed the efficacy of 3 kg of Li-FAU in reducing N2 contamination from ~ 5 ppm of injected N2 down to less than 1 ppm over 96-hour cycles, showcasing its potential for larger-scale LAr cryostats. Further tests are planned to validate Li-FAU's use as a possible alternative to Molecular Sieve 4A in LBNF-DUNE and related liquid argon experiments. This contribution will describe how the research was performed and present the test setups and results in detail. This advancement not only has the potential to enhance DUNE's precision but also to elevate liquid argon experiments globally, showcasing the power of international scientific collaboration.
Results from commissioning and first year of operations of the cryogenic system of the Short-Baseline Neutrino Detector (SBND) and its membrane cryostat installed at the Fermi National Accelerator Laboratory are described. The SBND detector is installed in a 200 m$^3$ membrane cryostat filled with liquid argon, which serves both as target and as active media. For the correct operation of the detector, the liquid argon must be kept in very stable thermal conditions while the contamination of electronegative impurities must be consistently kept at the level of small fractions of parts per billion. The detector is operated in Booster Neutrino Beams (BNB) at Fermilab for the search of sterile neutrinos and measurements of neutrino-argon cross sections. The cryostat and the cryogenic systems also serve as prototypes for the much larger equipment to be used for the LBNF/DUNE experiment. Since its installation in 2018-2023 and cooldown in spring of 2024, the cryostat and the cryogenic system have been commissioned to support the detector operations. The lessons learned through installation, testing, commissioning, cooldown, and initial operations are described.
Results from commissioning and first year of operations of the cryogenic system of the Short-Baseline Neutrino Detector (SBND) and its membrane cryostat installed at the Fermi National Accelerator Laboratory are described. The SBND detector is installed in a 200 m3 membrane cryostat filled with liquid argon, which serves both as target and as active media. For the correct operation of the detector, the liquid argon must be kept in very stable thermal conditions while the contamination of electronegative impurities must be consistently kept at the level of small fractions of parts per billion. The detector is operated in Booster Neutrino Beams (BNB) at Fermilab for the search of sterile neutrinos and measurements of neutrino-argon cross sections. The cryostat and the cryogenic systems also serve as prototypes for the much larger equipment to be used for the LBNF/DUNE experiment. Since its installation in 2018-2023 and cooldown in spring of 2024, the cryostat and the cryogenic system have been commissioned to support the detector operations. The lessons learned through installation, testing, commissioning, cooldown, and initial operations are described.