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NASA NTRS1977

The effect of the liquid-solid system properties on the interline heat transfer coefficient

A theoretical procedure to determine the heat transfer characteristics of the interline region of an evaporating meniscus using the macroscopic optical and thermophysical properties of the system is outlined. The analysis is based on the premise that the interline transport processes are controlled by the London-van der Waals forces between condensed phases (solid and liquid). The procedure is used to compare the relative size of the interline heat sink of various systems using a constant heat flux model. This solution demonstrates the importance of the interline heat flow number which is evaluated for various systems. The heat transfer characteristics of the decane-steel system are numerically compared with those of the carbon tetrachloride-quartz system.

Wayner, P. C., Jr.↗

NASA NTRS2017

A Comparison of System Architectures for a Mechanically Pumped Two-Phase Thermal Control System

The NASA Jet Propulsion Laboratory is developing a mechanically pumped two-phase fluid loop thermal control system to enable novel mission designs and greater science return. Pumped two-phase fluid loops have the potential to provide robust and effective thermal control that combine the best aspects of passive two-phase systems (heat pipes) and mechanically pumped single-phase fluid loops. The current program requirements include the development of a system with multiple 1 sq.m evaporators, each of which is capable of remaining spatially and temporally isothermal while accommodating heat loads of up to 500 W and local fluxes of up to 5 W/sq.cm. The goal is to attain this using less than 5 W of power. Such a system would be able to accommodate the next generation of payload and bus electronics while using minimal resources. This paper compares two different mechanically pumped two-phase fluid loop architectures in the context of these requirements. A mixed flow and separated flow architecture are compared on a theoretical and experimental basis. Test data from sub-scale, single evaporator/single condenser, mixed flow and separated flow testbeds are presented. In addition, a model is introduced to better understand separated flow systems and some expressions for the theoretical performance limits of such systems are developed. To date, the investigation suggests that a separated flow architecture is better suited to the program requirements. Separated flow systems have the potential to accommodate an isothermalizing two-phase evaporator while using lower levels of power than would be required for a mixed flow system. In addition, it is argued that separated flow systems are more robust and amenable to analysis than mixed flow systems, since they significantly reduce the occurrence of two-phase flow by separating phases in the evaporator. Future work will include developing a full-scale testbed that includes multiple evaporators and condensers in a representative flight configuration.

Furst, Benjamin↗

NASA NTRSDate not supplied

The ZBOT-NC Experiment - Effects of Non-Condensable Gases on Propellant Tank Pressurization and Pressure Control

Introduction Integral to all phases of NASA’s projected planetary expeditions is affordable and reliable cryogenic fluid storage for use in propellant or life support systems. It is greatly advantageous to develop innovative vent-less pressure control designs based on cooling/mixing of the bulk tank fluid to allow storage of the cryogenic fluid with zero or reduced boil-off. The presence of noncondensable gases, can interfere with the condensation at the interface impacting tank pressure control during subcooled jet mixing especially in microgravity. The Zero-Boil-Off Tank (ZBOT) Experiments are a series of small-scale experiments aboard the International Space Station (ISS) that use a transparent volatile simulant fluid in a transparent sealed tank to delineate various fundamental fluid flow, heat and mass transport, and phase change phenomena associated with storage tank pressurization and pressure control in microgravity. The ZBOT-1 experiment was performed on the ISS 2017-2018 timeframe and collected data to validate a state-of-the-art CFD model for tank pressurization and pressure control for a pure system. The ZBOT-NC Experiment is the second experiment in the series to be performed on the International Space Station (ISS) in 2025. Its goal is to investigate the effects of noncondensable gases on interfacial evaporation and condensation during self -pressurization and jet-mixing pressure control in microgravity for a two-component system. Materials & Methods In this work, we will describe the detailed features of the ZBOT-NC experimental hardware and Diagnostics that includes nonintrusive Quantum Dot Thermometry (QDT) for whole field temperature measurement. All microgravity pressurization and pressure control tests will be performed for both the pure and the two-components systems with Xenon and Neon as the two noncondensable gases spanning small and large molecular weights and sizes. The two-phase CFD model that is developed as part of the project will be also presented and discussed. Results Ground-based pressurization and jet mixing experiments and CFD simulation results are compared to each other to validate both the fidelity of the CFD model predictions and the accuracy of the QDT measurement. Model simulations for noncondensable gas effects will also be compared against large Cryogenic LH2-GHe experiments to indicate the noncondensable gas effects on tank pressure control during jet mixing in 1G. Finally, CFD results will be presented to predict the effects of the noncondensable gas during subcooled jet mixing during the ZBOT-NC in advance of the microgravity experiment in 2015.

Evaporation Condensation↗

NASA NTRSDate not supplied

Vapor Growth of ZnSe-based Compound Semiconductors in Low Gravity environment on International Space Station

Six low-gravity experiments of crystal growth of ZnSe-based compound semiconductors by physical vapor transport (PVT) are scheduled to be processed inside Low Gradient Furnace (LGF) on Materials Science Research Rack (MSRR) in Material Science Laboratory (MSL) on International Space Station (ISS) starting from February 27th, 2023. The flight samples consist of three unseeded growths of ZnSe, Cr-doped ZnSe and ZnSeTe as well as growth of ZnSe on top of three single crystal ZnSe seeds with orientation of (100), (110) and (111). The main scientific objective of the flight experiments is to establish the effects of gravity-driven fluid flows on Earth to (i) the non-uniform incorporation of impurities and defects and (ii) the deviation from stoichiometry observed in the grown crystals caused by growth interface fluctuations and evolution as the results of buoyancy-driven convection and irregular fluid-flows. The investigation will also evaluate the effects of gravity on the PVT process by examining (i) the growth kinetics on various seed orientations, (ii) the dopant segregation and distribution in the Cr doped ZnSe, and (iii) the compositional segregation and distribution in the ternary ZnSeTe crystal grown by PVT. Additionally, from X-ray diffraction/topography and by measuring the density and distribution of various crystalline defects it will assess the self-induced strain effects developed during processing at elevated temperatures caused by the weight of the crystals. During the ground-based preparations, the following tasks have been accomplished: • Establish the thermodynamic properties of the ZnSe binary and related ternary systems by measuring the partial pressures of the vapor phase coexisting with the condensed phases and perform phase diagram calculations for comparison. • Evaluate the effects of gravity-driven convection in the growth process by performing experiments under various vapor transport orientations relative to gravity vector, i.e., horizontal, vertically stabilized and destabilized configurations. • Establish a quantitative correlation between growth parameters and the characteristics and properties of the grown crystals by characterizing the crystals using a variety of techniques. • Evaluate the fundamentals of the current theories on vapor transport and crystal growth kinetics by performing in-situ and real-time monitoring techniques during growth. • Develop a one-dimensional diffusion limited theory of mass transport and two- and three-dimensional numerical simulations of both mass transport and heat transfer and thus establish the microgravity requirements for the flight experiments and to predict the characteristics of the grown crystals such as the solid-vapor interface shapes… etc. and establish a fundamental understanding of the crystal growth process from the comparison with experimental results.

ZnSe↗

NASA NTRS2019

Assembly and Integrated Systems Testing for the Flow Boiling and Condensation Experiment (FBCE)

The Flow Boiling and Condensation Experiment (FBCE) is a flight experiment that is designed to operate in the Fluids Integrated Rack (FIR) on the International Space Station (ISS). The objective of the FBCE is to develop an integrated two-phase flow experiment that will serve as a primary platform for obtaining flow boiling and condensation heat transfer data in microgravity. This data will enable the design and analysis of two-phase thermal management systems for future NASA missions that require increased efficiency beyond the current single-phase systems. The FBCE consists of seven modules, each of which must link together mechanically, electrically, and fluidically upon final integration. Five of the modules provide the fluidic and electronic components required to bring the test fluid to the inlet conditions required by the test module, where the primary science is conducted. These inlet conditions encompass fluid quality ranging from a superheated vapor to a subcooled liquid at a variety of flow rates and pressures. The FBCE is currently manufacturing two test modules, each of which has its own separate test campaign with the five support modules. Each of the modules presents a unique challenge in its assembly and checkout, particularly related to ensuring the final hardware configuration can meet the fluid and thermal requirements levied upon them. Following assembly, a series of flight verification tests will be performed, including thermal testing, EMI testing, and final integration in a FIR Ground Integration Unit. This presentation discusses the status of the FBCE as it continues through final verification testing, including current test results and lessons learned throughout the assembly and integration phase of the project. In addition, future options for additional flight test sections will be explored that will benefit the broader NASA thermal and fluids community.

deFiebre, Jesse↗

NASA NTRSDate not supplied

The Zero-Boil-Off Tank Experiment: the Effects of Non-Condensable Gases on Pressurization and Pressure Control of Propellant Tanks in Microgravity

Evaporation Condensation↗

NASA NTRS1991

A Local Condensation Analysis Representing Two-phase Annular Flow in Condenser/radiator Capillary Tubes

NASA's effort for the thermal environmental control of the Space Station Freedom is directed towards the design, analysis, and development of an Active Thermal Control System (ATCS). A two phase, flow through condenser/radiator concept was baselined, as a part of the ATCS, for the radiation of space station thermal load into space. The proposed condenser rejects heat through direct condensation of ATCS working fluid (ammonia) in the small diameter radiator tubes. Analysis of the condensation process and design of condenser tubes are based on the available two phase flow models for the prediction of flow regimes, heat transfer, and pressure drops. The prediction formulas use the existing empirical relationships of friction factor at gas-liquid interface. An attempt is made to study the stability of interfacial waves in two phase annular flow. The formulation is presented of a stability problem in cylindrical coordinates. The contribution of fluid viscosity, surface tension, and transverse radius of curvature to the interfacial surface is included. A solution is obtained for Kelvin-Helmholtz instability problem which can be used to determine the critical and most dangerous wavelengths for interfacial waves.

Karimi, Amir↗

NASA NTRS2015

Laboratory Studies of Cometary Materials - Continuity Between Asteroid and Comet

Laboratory analysis of cometary samples have been enabled by collection of cometary dust in the stratosphere by high altitude aircraft and by the direct sampling of the comet Wild‐2 coma by the NASA Stardust spacecraft. Cometary materials are composed of a complex assemblage of highly primitive, unprocessed interstellar and primordial solar system materials as well as a variety of high temperature phases that must have condensed in the inner regions of the protoplanetary disk. These findings support and contradict conclusions of comet properties based solely on astronomical observations. These sample return missions have instead shown that there is a continuity of properties between comets and asteroids, where both types of materials show evidence for primitive and processed materials. Furthermore, these findings underscore the importance and value of direct sample return. There will be great value in comparing the findings of the Stardust cometary coma sample return mission with those of future asteroid surface sample returns OSIRIS‐REx and Hayabusa II as well as future comet nucleus sample returns.

Messenger, Scott↗

NASA NTRS1978

The effect of the London-van der Waals dispersion force on interline heat transfer

A theoretical procedure to determine the heat transfer characteristics of the interline region (junction of liquid-solid-vapor) from the macroscopic optical and thermophysical properties of the system is outlined. The analysis is based on the premise that the interline transport processes are controlled by the London-van der Waals dispersion force between condensed phases (solid and liquid). Numerical values of the dispersion constant are presented. The procedure is used to compare the relative size of the interline heat sink of various systems using a constant heat flux mode. This solution demonstrates the importance of the interline heat flow number, which is evaluated for various systems.

Wayner, P. C., Jr.↗

NASA NTRS2021

Topical: Boiling, Condensation and Two-Phase Flows in Microgravity

The white paper addresses both fundamental and technological questions in the science of phase-change fluid flows aimed at understanding thermal transport in flow boiling and condensation and the use of these processes in space and terrestrial thermal systems. While flow boiling and condensation are widely employed in Earth-based thermal equipment to reduce the cost, size, and power required to transfer heat, a lack of data and predictive models on the impact of gravity on these phenomena hinders the use of two-phase heat transport in a low-gravity environment. The white paper presents research tasks in long-duration microgravity recommended to expand our knowledge on phase-changing flows. Due to elimination of the masking gravity effects, the proposed research will provide a unique opportunity to bring new insights into the role of capillary and hydrodynamic forces in phase-changing flows. The potential impact of the proposed research ranges from the space power, thermal and cryogenic systems to various terrestrial applications in the petrochemical, pharmaceutical, biochemical, nuclear, and metallurgical industries.

Phase-change fluid flow↗

NASA NTRS1982

Thermal control for the 1990's

Current thermal distribution systems on large spacecraft, such as the Space Shuttle and Spacelab, use pumped fluid loops that circulate the coolant between a series of user stations and a single rejection point, involving complex plumbing and controls with a significant power penalty and limited reliability. In order to provide heat transport at near-isothermal conditions in future large spacecraft, two-phase flow systems will be implemented by taking advantage of the heat of vaporization and condensation of common working fluids at minimal expenditure of power and temperature variation. Such systems are considered for the cases of the thermal requirements of nearly 100 potential astrophysics and astronomy instruments. Data on temperature requirements, power dissipations, environmental fluxes, heat addition or rejection, and general description, are used to form conceptual designs for the thermal utility.

Ollendorf, S.↗

NASA NTRS2004

Thermal performance of a multi-evaporator loop heat pipe with thermal masses and thermal electrical coolers

This paper describes thermal performance of a loop heat pipe (LHP) with two evaporators and two condensers in ambient testing. Each evaporator has an outer diameter of 15mm and a length of 76mm, and has an integral compensation chamber (CC). An aluminum mass of 500 grams is attached to each evaporator to simulate the instrument mass. A thermal electric cooler (TEC) is installed on each CC to provide heating as well as cooling for CC temperature control. A flow regulator is installed in the condenser section to prevent vapor from going back to the evaporators in the event that one of condenser is fully utilized. Ammonia was used ad the working fluid. Tests conducted included start-up, power cycle, heat load sharing, sink temperature cycle, operating temperature control with TECs, and capillary limit tests. Experimental data showed that the loop could start with a heat load of less than 1OW even with added thermal masses. The loop operated stably with even and uneven evaporator heat loads, and even and uneven condenser sink temperatures. The operating temperature could be controlled within +/-0.5K of the set point temperature using either or both TECs, and the required TEC control heater power was less than 2W under most test conditions. Heat load sharing between the two evaporators was also successfully demonstrated. The loop had a heat transport capability of 120W to 140W, and could recover from a dry-out when the heat load was reduced. The 500-gram aluminum mass on each evaporator had a negligible effect on the loop operation. Existing LHPs servicing the orbiting spacecraft have a single evaporator with an outer diameter of about 25mm. Important performance characteristics demonstrated by this LHP included: 1) Operation of an LHP with 15mm diameter evaporators; 2) Robustness and reliability of an LHP with multiple evaporators and multiple condensers under various test conditions; 3) Heat load sharing among LHP evaporators; 4) Effectiveness of TECs in controlling the LHP operating temperature; and 5) Effectiveness of the flow regulator in preventing vapor from going back the evaporators.

loop heat pipes↗

NASA NTRS1992

Condensation phase of the Martian south polar cap

One type of database that can be useful in limiting models of the Mars surface-atmosphere system is the time dependent boundary of CO2 frost for the polar caps. Data acquired by the thermal infrared sensors on spacecraft are not limited by the lighting problems that hamper visual observations. The surface temperature of solid CO2 is limited by Clapeyron's equation as a function of the local partial pressure of CO2 gas. The growth was studied of the Martian south polar cap using the Viking IRTM dataset. These data are available in five bands, four of which should correspond to surface radiation in clear conditions; the 20 micron data was examined in the first phase.

Capuano, J.↗

NASA NTRS2004

Element Mapping in Anhydrous IDPs: Identification of the Host Phases of Major/Minor Elements as a Test of Nebula Condensation Models

Many anhydrous interplanetary dust particles (IDPs) are the most pristine samples of primitive solar system dust currently available for laboratory analysis. Their primitive nature is demonstrated by: 1) the high content of moderately volatile elements, indicating they have not been heated significantly since formation, 2) the absence of hydrated material, indicating they never experienced aqueous processing, 3) the presence of unequilibrated mineral assemblages, 4) the presence of large isotopic anomalies (e.g., D and 15N enrichment), in these IDPs.

Flynn, G. J.↗

NASA NTRS1982

Experimental studies of the vapor phase nucleation of refractory compounds. I - The condensation of SiO

The critical partial pressure of SiO necessary to initiate avalanche nucleation in the SiO-H2 system is measured as a function of the ambient temperature in the range 750-1000 K. Results show that the condensate produced at low temperatures is Si2O3, while a mixture of Si2O3 and amorphous SiO2 is produced at high temperatures. A surface energy of approximately 500 ergs/sq cm for the particles is found by analyzing the critical partial pressure vs temperature using classical nucleation theory. It is concluded that classical nucleation theory is not applicable to this system, because several inconsistencies in the thermodynamic analysis are demonstrated, and it is suggested that a kinetic theory of nucleation may be the preferential way to describe the condensation process.

Nuth, J. A.↗

NASA NTRS1987

A study of two-phase flow in a reduced gravity environment

A test loop was designed and fabricated for observing and measuring pressure drops of two-phase flow in reduced gravity. The portable flow test loop was then tested aboard the NASA-JSC KC135 reduced gravity aircraft. The test loop employed the Sundstrand Two-Phase Thermal Management System (TPTMS) concept which was specially fitted with a clear two-phase return line and condenser cover for flow observation. A two-phase (liquid/vapor) mixture was produced by pumping nearly saturated liquid through an evaporator and adding heat via electric heaters. The quality of the two-phase flow was varied by changing the evaporator heat load. The test loop was operated on the ground before and after the KC135 flight tests to create a one-gravity data base. The ground testing included all the test points run during the reduced gravity testing. Two days of reduced gravity tests aboard the KC135 were performed. During the flight tests, reduced-gravity, one-gravity, and nearly two-gravity accelerations were experienced. Data was taken during the entire flight which provided flow regime and pressure drop data for the three operating conditions. The test results show that two-phase pressure drops and flow regimes can be accurately predicted in zero-gravity.

Hill, D.↗

NASA NTRS1968

Axisymmetric two-phase perfect gas performance program

Computer program calculates the inviscid axisymmetric nozzle expansion of propellant systems having both gaseous and condensed exhaust products. The program uses velocity and thermal lags and will perform calculations for contoured and conical nozzles.

Kliegel, J. R.↗

NASA NTRS1990

Liquid-Vapor Equilibrium of Multicomponent Cryogenic Systems

Liquid-vapor and solid-vapor equilibria at low to moderate pressures and low temperatures are important in many solar system environments, including the surface and clouds of Titan, the clouds of Uranus and Neptune, and the surfaces of Mars and Triton. The familiar cases of ideal behavior are limiting cases of a general thermodynamic representation for the vapor pressure of each component in a homogeneous multicomponent system. The fundamental connections of laboratory measurements to thermodynamic models are through the Gibbs-Duhem relation and the Gibbs-Helmholtz relation. Using laboratory measurements of the total pressure, temperature, and compositions of the liquid and vapor phases at equilibrium, the values of these parameters can be determined. The resulting model for vapor-liquid equilibrium can then conveniently and accurately be used to calculate pressures, compositions, condensation altitudes, and their dependencies on changing climatic conditions. A specific system being investigated is CH4-C2H6-N2, at conditions relevant to Titan's surface and atmosphere. Discussed are: the modeling of existing data on CH4-N2, with applications to the composition of Titan's condensate clouds; some new measurements on the CH4-C2H6 binary, using a high-precision static/volumetric system, and on the C2H6-N2 binary, using the volumetric system and a sensitive cryogenic flow calorimeter; and describe a new cryogenic phase-equilibrium vessel with which we are beginning a detailed, systematic study of the three constituent binaries and the ternary CH4-C2H6-N2 system at temperatures ranging from 80 to 105 K and pressures from 0.1 to 7 bar.

Thompson, W. Reid↗