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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Precise Linker Length and Dynamic Bond Exchange Control Penetrant Diffusion in Dense Vitrimers

Polymer networks with dynamic covalent bonds have been investigated for their self-healing ability, recyclability, and potential as more sustainable materials. Recent results have indicated that in some cases, bond exchange can enhance the transport of penetrants in dense networks, pointing to their potential for separations of membranes. Here, imine dynamic bonds in ethylene oxide (EO) networks with precise linker lengths were synthesized to investigate the transport of N,N′-bis(2,5-di-tert-butylphenyl)-3,4,9,10-perylenedicarboximide (BTBP), a large, anisotropic dye molecule. Networks with mesh sizes smaller than, comparable to, and greater than the size of the penetrant axes were investigated to probe the effects of bond exchange and network confinement on transport. Mesh sizes, which ranged from 0.5 to 1.62 nm, were determined from shear rheology, glass transitions by calorimetry, and probe diffusion coefficients by fluorescence recovery after photobleaching. Permanent networks with identical EO chain lengths were prepared as control samples, and up to a 3 orders of magnitude increase in diffusion coefficient is observed in the dynamic systems for short linkers containing 13 backbone atoms. The longest linkers with 71 backbone atoms show no difference between the permanent and dynamic networks. Linkers shorter than 11 backbone atoms, corresponding to a mesh size smaller than the penetrant small axis, diffusion is no longer observable on the experimental time scale, indicating a sharp cutoff attributed to the precise linkers and narrow mesh size distribution. The dynamic imine exchange time scales were compared to the diffusive hopping times of penetrants and indicate that exchange can occur during a diffusive displacement. Furthermore, these findings provide insights into the factors affecting penetrant transport in dense polymers and inspire the development of next-generation selective polymer membranes.

Diffusion↗
DOE OSTI2020

Penetration of foliar-applied Zn and its impact on apple plant nutrition status: in vivo evaluation by synchrotron-based X-ray fluorescence microscopy

The absorption of foliar fertilizer is a complex process and is poorly understood. The ability to visualize and quantify the pathway that elements take following their application to leaf surfaces is critical for understanding the science and for practical applications of foliar fertilizers. By the use of synchrotron-based X-ray fluorescence to analyze the in vivo localization of elements, our study aimed to investigate the penetration of foliar-applied Zn absorbed by apple leaves with different physiological surface properties, as well as the possible interactions between foliar Zn level and the mineral nutrient status of treated leaves. The results indicate that the absorption of foliar-applied Zn was largely dependent on plant leaf surface characteristics. High-resolution elemental maps revealed that the high binding capacity of the cell wall for Zn contributed to the observed limitation of Zn penetration across epidermal cells. Trichome density and stomatal aperture had opposite effects on Zn fertilizer penetration: a relatively high density of trichomes increased the hydrophobicity of leaves, whereas the presence of stomata facilitated foliar Zn penetration. Low levels of Zn promoted the accumulation of other mineral elements in treated leaves, and the complexation of Zn with phytic acid potentially occurred owing to exposure to high-Zn conditions. The present study provides direct visual evidence for the Zn penetration process across the leaf surface, which is important for the development of strategies for Zn biofortification in crop species.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2021

Energy barriers for Dy and H penetrating graphene on 6 H -SiC(0001) and freestanding bilayer graphene from first-principles calculations

Currently, intercalation of foreign guest atoms into two-dimensional (2D) layered van der Waals materials is an active research area motivated in part by the development of next-generation energy-storage technologies and optoelectronic devices. One such extensively studied 2D material is the graphene-on-SiC system. To realize and control the desired intercalated structures, it is fundamentally important to understand the kinetic process of intercalation. For the intercalation of a guest atom into graphene layers on SiC substrate, a critical kinetic parameter is the energy barrier of a guest atom penetrating the perfect graphene top layer into the gallery under it. However, accurate theoretical calculations for such penetration barriers are unavailable in literature. From our first-principles density functional theory calculations, we obtain the global energy barriers of 3.47 and 1.80 eV for single Dy and H atoms penetrating the graphene top layer on a graphene buffer layer supported by a Si-terminated 6H-SiC(0001) substrate, respectively. Furthermore, for comparison as well as for examining the lateral strain effects, we also obtain the global barriers of 5.05 and 1.50 eV for single Dy and H atoms penetrating freestanding bilayer graphene with a tensile strain of about 8.8% to match our model for supported graphene, as well as the global barriers of 7.21 and 4.18 eV for penetrating unstrained freestanding bilayer graphene, respectively. From corresponding minimum energy paths with multiple energy minima and saddle points, we can also obtain various local energy barriers and the global backward barrier from the graphene gallery back to the top surface.

2D materials↗
DOE OSTI2022

Direct current magnetic Hall probe technique for measurement of field penetration in thin film superconductors for superconducting radio frequency resonators

Superconducting Radio Frequency (SRF) cavities used in particle accelerators are typically formed from or coated with superconducting materials. Currently, high purity niobium is the material of choice for SRF cavities that have been optimized to operate near their theoretical field limits. This brings about the need for significant R & D efforts to develop next generation superconducting materials that could outperform Nb and keep up with the demands of new accelerator facilities. To achieve high quality factors and accelerating gradients, the cavity material should be able to remain in the superconducting Meissner state under a high RF magnetic field without penetration of quantized magnetic vortices through the cavity wall. Therefore, the magnetic field at which vortices penetrate a superconductor is one of the key parameters of merit of SRF cavities. Techniques to measure the onset of magnetic field penetration on thin film samples need to be developed to mitigate the issues with the conventional magnetometry measurements that are strongly influenced by the film orientation and shape and edge effects. In this work, we report the development of an experimental setup to measure the field of full flux penetration through films and multi-layered superconductors. Our system combines a small superconducting solenoid that can generate a magnetic field of up to 500 mT at the sample surface and three Hall probes to detect the full flux penetration through the superconductor. We report this setup can be used to study alternative materials that could potentially outperform niobium, as well as superconductor–insulator–superconductor (SIS) multilayer coatings on niobium.

47 OTHER INSTRUMENTATION↗
DOE OSTI2021

Measurements of Magnetic Field Penetration in Superconducting Materials for SRF Cavities

Superconducting radiofrequency (SRF) cavities used in particle accelerators operate in the Meissner state. To achieve high accelerating gradients, the cavity material should stay in the Meissner state under high RF magnetic field without penetration of vortices through the cavity wall. The field onset of flux penetration into a superconductor is an important parameter of merit of alternative superconducting materials other than Nb which can enhance the performance of SRF cavities. There is a need for a simple and efficient technique to measure the onset of field penetration into a superconductor directly. We have developed a Hall probe experimental setup for the measurement of the flux penetration field through a superconducting sample placed under a small superconducting solenoid magnet which can generate magnetic fields up to 500 mT. The system has been calibrated and used to measure different bulk and thin film superconducting materials. This system can also be used to study SIS multilayer coatings that have been proposed to enhance the vortex penetration field in Nb cavities.

Senevirathne, I. H.↗
DOE OSTI2020

High Penetration Power Electronics Grid: Modeling and Simulation Gap Analysis

Increased penetration of power electronics in the grid is happening through development of high-power drives (like in Type 3 or 4 wind turbines, industrial drives, etc.), high-voltage direct current (HVdc) systems, flexible alternating current transmission systems (FACTS), energy storage systems (ESSs), inverter-based renewables like solar and wind, electric vehicle chargers, and other technologies. Ongoing research and development in new power electronic technologies including, but not limited to, solid-state power substations (SSPS), extreme fast charging (XFC), solid-state transformers, and multi-port power electronics that integrate multiple sources/loads will further increase penetration levels. To ensure stakeholders can integrate high penetration of power electronic technologies safely and reliably requires tools and methods to assess and evaluate their impact on the grid. Objectives: This report surveys, assesses, and analyzes commercially available and open-source tools that can support the assessment and evaluation of power electronics in future grids with high penetration levels. The study includes aspects that range from power flow analysis to dynamics evaluation (including hardware-in-the-loop – HIL testing) for such systems. The challenges and gaps associated with the current generation of toolsets available to assess the technical impact of introducing high penetration of power electronics are reported. The method is summarized in Figure ES-1.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2021

Shattered pellet penetration in low and high energy plasmas on DIII-D

Shattered pellet injection (SPI) has been adopted as the baseline disruption mitigation system for ITER, as the radiative payload penetration into DIII-D plasmas from SPI is superior to those using the massive gas injection (MGI) method. Because of the substantial differences in the energy content of ITER plasma and those in present experiments, reliable 3D MHD modeling, benchmarked against present experiments is needed to project to ITER plasmas. In support of these needs, the depth of SPI fragment penetration in DIII-D plasmas was investigated by injecting SPI into two discharges with vastly different energy content and pedestal height. 400 Torr-L pure Ne fragmented pellets at a velocity of about 200 m s−1 were injected into a 0.2 MJ L-mode discharge and a 2 MJ super H-mode discharge. Results show deep penetration of SPI fragments into low-energy plasmas in DIII-D. SPI fragment penetration is reduced as the plasma energy content increases, with some discharges exhibiting penetration that is confined to the outer regions of the plasma. The injected SPI fragments are also spread out over a distance of about 20 cm, which results in some fragments arriving near the end of or after the thermal quench is over.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1973

Static penetration resistance of soils

Model test results were used to define the failure mechanism associated with the static penetration resistance of cohesionless and low-cohesion soils. Knowledge of this mechanism has permitted the development of a new analytical method for calculating the ultimate penetration resistance which explicitly accounts for penetrometer base apex angle and roughness, soil friction angle, and the ratio of penetration depth to base width. Curves relating the bearing capacity factors to the soil friction angle are presented for failure in general shear. Strength parameters and penetrometer interaction properties of a fine sand were determined and used as the basis for prediction of the penetration resistance encountered by wedge, cone, and flat-ended penetrometers of different surface roughness using the proposed analytical method. Because of the close agreement between predicted values and values measured in laboratory tests, it appears possible to deduce in-situ soil strength parameters and their variation with depth from the results of static penetration tests.

Durgunoglu, H. T.↗
NASA NTRS1975

The Effect of a Planetary Surface Penetrator on the Soil Column Surrounding the Impacting Body

A prototype penetrator instrument was impacted into a dry lake bed. Laboratory studies of the soil surrounding the penetrator revealed that the soil was contaminated by paint and metal from the penetrator's casing. Paint pigment rich in titanium and sulfur was found in the adjacent soil. The highly mobile paint pigment migrated onto viewing ports in the penetrator's exterior. Bulk analysis of the soil adjacent to the impactor showed a significant increase in both elements, as well as the presence of metal chips from the casing and nose cone. It is recommended that great care be taken in the use of coating materials and the metal alloys selected for the penetrator's exterior, or the accuracy of any experiment requiring an uncontaminated in situ sample may be adversely affected.

Blanchard, Maxwell B.↗
NASA NTRS1979

Field measurement of penetrator seismic coupling in sediments and volcanic rocks

Field experiments were conducted to determine experimentally how well a seismometer installed using a penetrator would be coupled to the ground. A dry lake bed and a lava bed were chosen as test sites to represent geological environments of two widely different material properties. At each site, two half-scale penetrators were fired into the ground, a three-component geophone assembly was mounted to the aft end of each penetrator, and dummy penetrators were fired at various distances to generate seismic signals. The recorded signals were digitized, and cross-spectral analyses were performed to compare the observed signals in terms of power spectral density ratio, coherence and phase difference. The analyses indicate that seismometers deployed by penetrators will be as well coupled to the ground as are seismometers installed by conventional methods for the frequency range of interest in earthquake seismology, although some minor differences were observed at frequencies near the upper limit of the frequency band.

Nakamura, Y.↗
NASA NTRS1981

Surface penetrators for planetary exploration: Science rationale and development program

Work on penetrators for planetary exploration is summarized. In particular, potential missions, including those to Mars, Mercury, the Galilean satellites, comets, and asteroids are described. A baseline penetrator design for the Mars mission is included, as well as potential instruments and their status in development. Penetration tests in soft soil and basalt to study material eroded from the penetrator; changes in the structure, composition, and physical properties of the impacted soil; seismic coupling; and penetrator deflection caused by impacting rocks, are described. Results of subsystem studies and tests are given for design of entry decelerators, high-g components, thermal control, data acquisition, and umbilical cable deployment.

Murphy, J. P.↗
NASA NTRS1981

A comparison of observed and analytically derived remote sensing penetration depths for turbid water

The depth to which sunlight will penetrate in turbid waters was investigated. The tests were conducted in water with a single scattering albedo range, and over a range of solar elevation angles. Two different techniques were used to determine the depth of light penetration. It showed little change in the depth of sunlight penetration with changing solar elevation angle. A comparison of the penetration depths indicates that the best agreement between the two methods was achieved when the quasisingle scattering relationship was not corrected for solar angle. It is concluded that sunlight penetration is dependent on inherent water properties only.

Morris, W. D.↗
NASA NTRS1980

Solar-ion penetration in the early solar nebula

A model for the early solar nebula is presented, along with the use of available ion range-energy relationships to determine when the irradiation of meteoritic grains occurred. Ions are assumed to travel on rectilinear paths with an energy change due solely to passage through absorbing materials, and consideration is given to the chances of energetic ions penetrating the nebular cloud to a distance of 3 AU. Cases of no absorbing gas, no absorbing dust, and the presence of both gas and dust are discussed, and model calculations are presented for protons and Fe nuclei ions. Penetration is found to decrease with the increase of the total amount of dust, a step function results when the size of the particles decreases, a fixed dust mass yields a penetration probability tending toward zero as the radius of the particles decreases, the fraction of the total dust mass required for penetration at 3 AU is small, and penetration to 3 AU readily occurs under present conditions.

Housen, K. R.↗
NASA NTRS1985

Comet nucleus gamma-ray spectrometer penetrator - An in situ nucleus composition experiment

An engineering design study of a comet nucleus penetrator system for in situ determinations of comet composition is presented. The system is designed for participation in the Comet Rendezvous/Asteroid Flyby mission to comet Kopff in 1996. The instrumentation payload of the penetrator system will include a passive gamma-ray spectrometer; a high frequency response accelerometer for measurements of the impact deceleration profile of the system as it penetrates to the nucleus of the comet; and several thermocouples mounted along the length of the penetrator to measure temperature and temperature gradients. The mechanical, electrical and thermal interfaces between the penetrator and the Mariner Mark II spacecraft are described. A series of line drawings is provided which illustrates the proposed configuration of the system.

Swenson, B. L.↗
NASA NTRS1988

Penetrator role in Mars sample strategy

The application of the penetrator to a Mars Return Sample Mission (MRSM) has direct advantages to meet science objectives and mission safety. Based on engineering data and work currently conducted at Ball Aerospace Systems Division, the concept of penetrators as scientific instruments is entirely practical. The primary utilization of a penetrator for MRSM would be to optimize the selection of the sample site location and to help in selection of the actual sample to be returned to Earth. It is recognized that the amount of sample to be returned is very limited, therefore the selection of the sample site is critical to the success of the mission. The following mission scenario is proposed. The site selection of a sample to be acquired will be performed by science working groups. A decision will be reached and a set of target priorities established based on data to give geochemical, geophysical and geological information. The first task of a penetrator will be to collect data at up to 4 to 6 possible landing sites. The penetrator can include geophysical, geochemical, geological and engineering instruments to confirm that scientific data requirements at that site will be met. This in situ near real-time data, collected prior to final targeting of the lander, will insure that the sample site is both scientifically valuable and also that it is reachable within limits of the capability of the lander.

Boynton, William↗
NASA NTRS1990

Fluorescent penetrant inspection

The purpose of this experiment is to familiarize the student with fluorescent penetrant inspection and to relate it to classification of various defects. The penetrant method of nondestructive testing is a method for finding discontinuities open to the surface in solids and essentially nonporous bodies. The method employs a penetrating liquid which is applied over the surface and enters the discontinuity or crack. After the excess of penetrant has been cleaned from the surface, the penetrant which exudes or is drawn back out of the crack indicates the presence and location of a discontinuity. The experimental procedure is described.

Sastri, Sankar↗
NASA NTRS1992

Sunlight penetration through the Martian polar caps: Effects on the thermal and frost budgets

An energy balance model of the seasonal polar caps on Mars is modified to include penetration of solar radiation into and through the ice. Penetration of solar radiation has no effect on subsurface temperature or total frost sublimation if seasonal ice overlies a dust surface. An effect is noted for seasonal ice which overlies the residual polar caps. For the case of an exposed water-ice residual polar cap, the temperature at depth is calculated to be up to several degrees warmer and the calculated lifetime of seasonal CO2 frost is slightly lower when penetration of sunlight is properly treated in the model. For the case of a residual polar cap which is perennially covered by CO2 frost, the calculated lifetime of seasonal CO2 frost is very slightly increased as a result of sunlight penetration through the ice. Hence, penetration of sunlight into the ice helps to stabilize the observed dichotomy in the residual polar caps on Mars, although it is a small effect.

Lindner, Bernhard Lee↗
NASA NTRS1992

Sunlight penetration through the Martian polar caps - Effects on the thermal and frost budgets

An energy balance model of the seasonal polar caps on Mars is modified to include penetration of solar radiation into and through the ice. Penetration of solar radiation has no effect on subsurface temperature or total frost sublimation if seasonal ice overlies a dust surface. An effect is noted for seasonal ice which overlies the residual polar caps. For the case of an exposed water-ice residual polar cap, the temperature at depth is calculated to be up to several degrees warmer, and the calculated lifetime of seasonal CO2 frost is slightly lower when penetration of sunlight is properly treated in the model. For the case of a residual polar cap which is perennially covered by CO2 frost, the calculated lifetime of seasonal CO2 frost is very slightly increased as a result of sunlight penetration through the ice. Hence, penetration of sunlight into the ice helps to stabilize the observed dichotomy in the residual polar caps on Mars, although it is a small effect.

Lindner, Bernhard L.↗