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At least 73 records · Page 4

Full-field quantitative visualization of shock-driven pore collapse and failure modes in PMMA

The dynamic collapse of pores under shock loading is thought to be directly related to hot spot generation and material failure, which is critical to the performance of porous energetic and structural materials. However, the shock compression response of porous materials at the local, individual pore scale is not well understood. This study examines, quantitatively, the collapse phenomenon of a single spherical void in PMMA at shock stresses ranging from 0.4 to 1.0 GPa. Using a newly developed internal digital image correlation technique in conjunction with plate impact experiments, full-field quantitative deformation measurements are conducted in the material surrounding the collapsing pore for the first time. The experimental results reveal two failure mode transitions as shock stress is increased: (i) the first in situ evidence of shear localization via adiabatic shear banding and (ii) dynamic fracture initiation at the pore surface. Numerical simulations using thermo-viscoplastic dynamic finite element analysis provide insights into the formation of adiabatic shear bands (ASBs) and stresses at which failure mode transitions occur. Further numerical and theoretical modeling indicates the dynamic fracture to occur along the weakened material inside an adiabatic shear band. Finally, analysis of the evolution of pore asymmetry and models for ASB spacing elucidate the mechanisms for the shear band initiation sites, and elastostatic theory explains the experimentally observed ASB and fracture paths based on the directions of maximum shear.

42 ENGINEERING↗

Application of the cubic polynomial strength criterion to the failure analysis of composite materials

A comparative failure analysis is presented based on the application of quadratic and cubic forms of the tensor polynomial lamina strength criterion to various composite structural configurations in a plane stress state. Failure loads have been predicted for off-angle laminates under simple loading conditions and for symmetric-balanced laminates subject to varying degrees of biaxial tension, including configurations subject to multimode failures. Some experimental data are also provided to support these calculations. From these results, the necessity of employing a cubic strength criterion to accurately predict the failure of composite laminae is demonstrated.

Tennyson, R. C.↗

Weathering processes implied from analysis of small Martian avalanche chutes

It has been proposed that the smaller features of martian spur and gully slope morphology, located along the upper walls of Valles Marineris, are avalanche chutes. A three-dimensional stability back-analysis technique was developed and applied to these small avalanche chutes, yielding average values of cohesion and angle of internal friction for the mobile layer materials on these slopes at the time of each slope failure. Generally, the analysis showed that at the time of each slope failure material strengths had been reduced to those of moderately cohesive debris down through depths of tens of meters. These results have implications and possible constraints for the nature and rate of martian weathering processes.

Sullivan, R.↗

Acoustic emission measurements of aerospace materials and structures

A development status evaluation is given for aerospace applications of AE location, detection, and source characterization. Attention is given to the neural-like processing of AE signals for graphite/epoxy. It is recommended that development efforts for AE make connections between the material failure process and source dynamics, and study the effects of composite material anisotropy and inhomogeneity on the propagation of AE waves. Broadband, as well as frequency- and wave-mode selective sensors, need to be developed.

Sachse, Wolfgang↗

Determining the ballistic threshold velocity for a composite structure using multiple failure models

A composite structure, such as a laminated composite panel, for example, comprises one or more layers or “plies” embedded in a matrix material or otherwise fixed together in an arrangement, commonly referred to as a “stack up.” Each material in the structure has a corresponding material failure model (MFM) defining the physical characteristics of that material. A ballistic threshold velocity computing device obtains the MFMs for each material in the composite structure, generates a predicted ballistic velocity threshold velocity for each MFM, and then generates a parametric model to compute a composite ballistic velocity threshold velocity for the composite structure.

36 MATERIALS SCIENCE↗

Session 4: ASME Code Rules

General review of code rules What do they cover. What they don’t. Underlying assumptions Probability of failure Material property parameters Stresses and loads Degradation What is NonmetallicsWork Group (NWG) doing? Failure in components Redefining failure Degradation rules Oxidation degradation Irradiation degradation Molten Salt Issues Abrasion/Erosion

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

EFRC-MUSE: Multi-Scale Fluid-Solid Interactions in Architected and Natural Materials

Phase interactions and fluid properties in geological and other environments are critical in applications ranging from hydrogen production and geologic storage and recovery, carbon dioxide storage and sequestration, and the sustainable use of water resources. The four goals of EFRC-MUSE: Multi-Scale Fluid-Solid Interactions in Architected and Natural Materials were based on the priority directions articulated in the Basic Research Needs documents, and the scientific needs in nanoscience. 1. Develop a fundamental understanding of confinement and surface interactions in mesoscale media with nanometer-sized pores on the phase behavior, thermodynamic and multiphase flow properties of multicomponent fluid mixtures. 2. Examine the impact of mineralogy and material heterogeneity on mechanical properties to better understand chemo-mechanical interactions in material failure. 3. Determine in-operando cross-scale structural and nanostructural material properties with fluids in confinement and flow under realistic condi

58 GEOSCIENCES↗

Corrosion of graphite composites in phosphoric acid fuel cells

Polymers, polymer-graphite composites and different carbon materials are being considered for many of the fuel cell stack components. Exposure to concentrated phosphoric acid in the fuel cell environment and to high anodic potential results in corrosion. Relative corrosion rates of these materials, failure modes, plausible mechanisms of corrosion and methods for improvement of these materials are investigated.

Christner, L. G.↗

Reaction propagation test. Evaluation of the behavior of nonmetallic materials in hydrogen

Results of tests conducted to evaluate the behavior of nonmetallic materials in hydrogen are described. The reaction propagation test simulates the conditions resulting from the interaction of an electrical wire in an overload condition in contract with a material in the test medium. The test is designed to evaluate the behavior of a material subjected to an energy input (usually heat) sufficient to cause a reaction which propagates to consume larger quantities of the material. Ten nonmetallic materials were evaluated to establish baseline data on the behavior of nonmetallic materials in hydrogen and to characterize, on an initial basis, one mode of material failure considered to be a factor pertinent to the safe use of a material in hydrogen.

Smith, I. D.↗

Flash and fire test: Evaluation of the behavior of nonmetallic materials in hydrogen

Tests conducted to evaluate the behavior of nonmetallic materials in hydrogen are described. The results of the flash and fire test are presented. The flash and fire test is used to evaluate the tendency of heated materials to ignite in a hydrogen atmosphere when subjected to an ignition source. The test represents a hydrogen parallel to a hazard condition known to exist in oxygen systems. Ten nonmetallic materials were evaluated to establish baseline data on the behavior of the materials and to characterize one mode of material failure considered to be a factor pertinent to the safe use of a material in hydrogen.

Source record↗

The nonlinear bending response of thin-walled laminated composite cylinders

The geometrically nonlinear Donnell shell theory is applied to the problem of stable bending of thin-walled circular cylinders. Responses are computed for cylinders with a radius-to-thickness ratio of 50 and length-to-radius ratios of 1 and 5. Four laminated composite cylinders and an aluminum cylinder are considered. Critical moment estimates are presented for short cylinders for which compression-type buckling behavior is important, and for very long cylinders for which the cross-section flattening, i.e., Brazier effect, is important. A finite element analysis is used to estimate the critical end rotation in addition to establishing the range of validity of the prebuckling analysis. The radial displacement response shows that the character of the boundary layer is significantly influenced by the geometric nonlinearities. Application of a first ply failure analysis using the maximum stress criterion suggests that in nearly all instances material failure occurs before buckling. Failure of the composite cylinders can be attributed to fiber breakage. Striking similarities are seen between the prebuckling displacements of the bending problem and axial compression problem for short cylinders.

Fuchs, Hannes P.↗

Molecular dynamics simulations of ultrafast radiation induced melting at metal–semiconductor interfaces

Metal–semiconductor contacts in silicon carbide (SiC) diodes endure damages at the interface when exposed to harsh radiation environments. Due to the rapid rise in temperature and ultrafast cooling that follows the radiation impact, the structural properties of the materials can be altered through melting, recrystallization, and amorphization. A detailed understanding of the material failure modes at the interface is lacking, specifically at the nanoscale. We use molecular simulations to investigate the ultrafast melting at tungsten (W)–SiC interfaces following radiation damage and apply deep learning techniques to track the transient evolution of the local molecular structures. We show that W near the radiation track undergoes melting and, eventually, most of it recrystallizes with a noticeable degree of undercooling, while SiC is rendered permanently amorphous. The observation of local undercooling in W films is important as it can affect the device performance even before the bulk melting temperature of the material is reached. We also show that at high temperatures, the interface undergoes a fracture-like failure. The results presented here are significant in understating the different failure modes of SiC diode materials.

Ashwin Ravichandran↗

An Advanced Meso-Scale Peridynamic Modeling Technology using High-Performance Computing for Cost-Effective Product Design and Testing of Carbon Fiber Reinforced Polymer Composites in Light-weight Vehicles

We study a peridynamic composite modeling technology based on the discontinuous Galerkin finite element method, implemented in the commercial LS-DYNA software, for modeling and prediction of failure in carbon fiber reinforced polymer composites. The proposed technology is developed for the material failure analysis at the meso-scale, which provides the prevailing fiber-matrix interaction mechanism, without adoption of the representative volume element method and thus avoiding complicated numerical calibration procedures. Three types of experimental tests—in-plane coupon test, out-of-plane coupon test, and a component crash test—are simulated in a high-performance computing environment to assess the performance of the proposed peridynamic composite modeling technology.

36 MATERIALS SCIENCE↗

Modern Material Analysis Instruments Add a New Dimension to Materials Characterization and Failure Analysis

Modern analytical tools can yield invaluable results during materials characterization and failure analysis. Scanning electron microscopes (SEMs) provide significant analytical capabilities, including angstrom-level resolution. These systems can be equipped with a silicon drift detector (SDD) for very fast yet precise analytical mapping of phases, as well as electron back-scattered diffraction (EBSD) units to map grain orientations, chambers that admit large samples, variable pressure for wet samples, and quantitative analysis software to examine phases. Advanced solid-state electronics have also improved surface and bulk analysis instruments: Secondary ion mass spectroscopy (SIMS) can quantitatively determine and map light elements such as hydrogen, lithium, and boron - with their isotopes. Its high sensitivity detects impurities at parts per billion (ppb) levels. X-ray photo-electron spectroscopy (XPS) can determine oxidation states of elements, as well as identifying polymers and measuring film thicknesses on coated composites. This technique is also known as electron spectroscopy for chemical analysis (ESCA). Scanning Auger electron spectroscopy (SAM) combines surface sensitivity, spatial lateral resolution (10 nm), and depth profiling capabilities to describe elemental compositions of near and below surface regions down to the chemical state of an atom.

Panda, Binayak↗

Behavior of Windblown Sand on Mars: Results from Single-Particle Experiments

Experiments are investigating the behavior of individual sand grains in the high-energy martian aeolian regime. Energy partitioning during impact of a saltating grain determines grain longevity, but it also influences the way in which the bed becomes mobilized by reptation. When single grains of sand are fired into loose beds, the bed can absorb up to 90% of the impact energy by momentum transfer to other grains; it has been discovered that the impacting grains cause circular craters even at low impact angles. Hundreds of grains can be splashed by a single high-velocity (100 m/s) impact causing more bed disturbance through reptation than previously thought. The research is supported by NASA's PG&G Program. Because the martian aeolian environment in both high energy and of long duration, the most mobile fractions of windblown sand should have eradicated themselves by attrition, unless sand supply has kept pace with destruction. It is therefore important to understand the rate of grain attrition in order to make sense of the existence of vast dune fields on Mars. Attrition, has been addressed in other studies, but precise data for a single saltating grain striking a loose bed of sand have not been acquired -- the quintessential case to be understood for dunes on Mars. To acquire these data, we are employing a compound crossbow which has the bolt-firing mechanism replaced with a pneumatically-automated sabot system. The sabot can launch individual grains of sand of any size between several millimeters and about 50 microns, at velocities up to 100m/s. This is around the maximum velocity expected for saltating grains on Mars. The sabot sled is equipped with photoelectric sensors for measuring shot velocity. Baffling of the grain's exit orifice has enabled projection of single grains without significant aerodynamic effects from the sabot. Grains are fired into loose beds of sand at about 15 degrees from the horizontal (typical saltation trajectory at impact) while being filmed on high-speed video. High-intensity pulse illumination for the grains is triggered by the solenoid-operated bow trigger. A 45 degree mirror over the impact site provides simultaneous horizontal and vertical images of the impact on each video frame. UV fluorescence is enabling grain and grain-fragment recovery. At 100 m/s, grains of all sizes shatter into many fragments when the sand is replaced with a solid target. Kinetic energy of the grains at this velocity exceeds the critical energy for catastrophic failure of minerals. Although probably exceptional as a grain speed, it suggests that conditions on Mars might elevate materials into an attrition regime not encountered on other planets; individual grains blown across rock pavements on Mars will have short lifespans. When experimental grains impact loose (dune) sand, much, if not most of the kinetic energy is converted into momentum of other grains. Using high-speed filming, the energy involved in splashing grains at the impact site can be derived from the size of the crater, the speed of the splashed grains, and the rebound speed of the impactor. The amount of energy partitioned into material failure (as opposed to momentum) is too small a fraction of the total to be calculated under these circumstances. This does not necessarily mean that little damage occurs to the grains (the full extent of the damage has yet to be determined) because only a small fraction of the impact energy is required for inducing brittle fracture. Damage is orders of magnitude less than during impact against solid surfaces.

Marshall, J. R.↗

Particle Characterization in Rocket Exhaust Plumes

A method to characterize particles in rocket exhaust plumes is developed. The particle velocity, size, and material composition are determined from crater characteristics resulting from impacts into aluminum and copper targets passed through the plume. The targets are mounted on a steel arm approximately 21 inches (53 cm) long which is rotated through the plume at sufficient velocity to prevent material failure resulting from thermal effects. A Scanning Electron Microscope (SEM) with secondary x-ray detectors is used to determine the particle material, and a standard optical measurement microscope is used to determine the crater diameter and depth. The crater diameter and depth are used in turn, as inputs to a ballistics computer code to estimate the velocity and size of the particle. The target has a safe residence time in the plume of approximately 50 ms before reaching an unacceptably high temperature. The = must mach a velocity of 104 ft/s (32 m/s) before entering the plume to produce the design residence time of 20 ms. The arm is actuated by a torsion spring with a 5-inch (13 cm) outer diameter, 0.625-inch (16 mm wire diameter, and 11 coils. A prototype of the entire rocket exhaust particle impact characterization system (PICS) was constructed and statically tested.

Callen, E. Eugene, Jr.↗

Gear Test Assembly - Experimental Testing and Analysis of Gears and Bearings - FY2023

The Gear Test Assembly (GTA) is an experimental test apparatus built and installed in the Mechanisms Engineering Test Loop (METL) at Argonne National Laboratory (ANL). The focus of GTA has been to test larger radial spur gears sets machined from Inconel 718 along with a variety of bearing components that are to be used in the fuel handling machines built for use in pool-type sodium fast reactors. The testing in GTA also informs the design and material choices for the full-scale Gripper Test Assembly (GrTA) being developed by Argonne. To date, the Inconel 718 gears used in all six GTA experimental campaigns have completed over 23.2 million revolutions under various loads equivalent to approximately 37,156 simulated fuel assembly maneuvers (removal from and reinsertion to core) using a conventional height of a core assembly. While the heat treated and untreated tapered roller bearings and cylindrical pin thrust bearings used in the first five experimental campaigns have experienced mechanical or material failure after completing a range of fuel assembly maneuvers ranging from as early as 575 operations in Campaign #5 to 9800 operations in Campaign #1, Campaign #6 was the most successful campaign, achieving 22,563 maneuvers and was concluded before any catastrophic failure occurred. In this report we will present the results from the most recent campaigns, #5 and #6. The longevity of Campaign #6 was likely aided by a variety of adjustments made to the materials and components used and to the experimental testing procedures employed. In terms of materials and components, new gearboxes were fabricated, as opposed to using the old gear boxes which had been impacted by the previous bearing failures, and ball bearings were replaced with tapered roller bearings. The adjustments to the experimental procedure focused on a lowering of the maximum torque applied to the gears and bearings and the increase of the duration of each simulated fuel assembly maneuver conducted. This report will present and discuss the changes made to the materials, components, and procedures and the subsequent results for Campaign #5 and Campaign #6.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

The Peridigm Meshfree Peridynamics Code

Abstract Peridigm is a meshfree peridynamics code written in C++ for use on large-scale parallel computers. It was originally developed at Sandia National Laboratories and is currently managed as an open-source, community driven software project. Its primary features include bond-based, state-based, and non-ordinary state-based constitutive models, bond failure laws, contact, and support for explicit and implicit time integration. To date, Peridigm has been used primarily by methods developers focused on solid mechanics and material failure. Peridigm utilizes foundational software components from Sandia’s Trilinos project and was designed for extensibility. This paper provides an overview of the solution methods implemented in Peridigm , a discussion of its software infrastructure, and demonstrates the use of Peridigm for the solution of several example problems.

97 MATHEMATICS AND COMPUTING↗