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At least 73 records · Page 4

The effect of impact damage and circular holes on the compressive strength of a graphite-epoxy laminate

Specimens were impacted by 1.27-cm-diameter aluminum spheres with speeds ranging from 52 to 101 m/s. Some specimens were impacted without any applied compressive load and then loaded to failure to determine their residual strength. Other specimens were loaded to a prescribed axial compressive strain and impacted while at that applied load. Loaded specimens that did not fail catastrophically on impact were subsequently loaded to failure to determine their residual strength. Low-velocity impact damage was found to degrade seriously the laminate static compressive strength. Low-strain compression-compression cyclic loading was found to degrade further the compressive strength of impact-damaged specimens. Specimens with circular holes having diameters up to a third of the specimen width were loaded to failure in compression. It was found that circular holes can also degrade the static compressive strength of the laminate. The effects of circular holes and impact damage on the compressive strength of the laminate are compared.

Starnes, J. H., Jr.↗

Fractography of unidirectional graphite-epoxy as a function of moisture, temperature and specimen quality

Optical microscopy and SEM have been used to examine the tensile failure surfaces of (0-deg)8 T300/5208 graphite-epoxy specimens, and fractography is employed to determine how moisture content and temperature, together with specimen preparation, affect failure modes. A low energy failure morphology is noted in defective specimens; specimens made from nondefective prepregs appeared to exhibit a decrease in flaw sensitivity and increasing strength with either temperature or moisture, although moisture also seemed to increase interfacial debonding between filament and matrix. The combination of temperature and moisture degraded performance by increasing interfacial debonding, and rendering the epoxy more prone to fracture.

Clements, L. L.↗

The correlation of ultrasonic attenuation and shear strength in graphite-polyimide composites

The buffer rod technique for measuring attenuation in thin specimens is modified here to apply to specimens having intermediate thicknesses and high attenuation. The described procedure, which requires only one accessible surface of the material, was used to determine the initial attenuation values of ultrasonic waves in short beam shear specimens of graphite-polyimide composite material. It is shown that there is good correlation between the initial attenuation values and the shear strengths of the specimens determined by the standard short beam shear test method. The modified ultrasonic buffer block technique offers much potential for service as a quantitative, nondestructive, quality assurance test for composite materials.

Hayford, D. T.↗

Titanium Nitride: An Oxidizable Coating for the High-Temperature Protection of Graphite

A titanium nitride coating for graphite, prepared by deposition process, protected test specimens for 60 seconds the vapors in a supersonic ceramic-heated air jet with a stagnation temperature of approximately 2,250 K. For the same test conditions, coated specimens showed no damage to the graphite body for the 60-second test, whereas uncoated specimens were very severely damaged after 20 seconds and were destroyed toward the end of the test. A discussion of the coating of these graphite specimens and of some of the conditions necessary for the utilization of oxidizable substances as oxidation-protective coatings for bodies facing high convective heat transfer in the atmosphere is presented.

Wakelyn, N. T.↗

Monitoring Fiber Stress During Curing of Single Fiber Glass- and Graphite-Epoxy Composites

The difference in thermal expansion characteristics of epoxy matrices and graphite fibers can produce significant residual stresses in the fibers during curing of composite materials. Tests on single fiber glass-epoxy and graphite-epoxy composite specimens were conducted in which the glass and graphite fibers were preloaded in tension, and the epoxy matrix was cast around the fibers. The fiber tension was monitored while the matrix was placed around the fiber and subjected to the temperature-time curing cycle. Two mechanisms responsible for producing stress in embedded fibers were identified as matrix thermal expansion and contraction and matrix cure shrinkage. A simple analysis based on the change in fiber tension during the curing cycle was conducted to estimate the produced stresses. Experimental results on single fiber glass- and graphite-epoxy composites show that the fiber was subjected to significant tensile stresses when the temperature was raised from the first to the second dwell period. When initial fiber pretension is about 60 percent of the fiber failure load, these curing-induced stresses can cause tensile fracture of the embedded fiber.

Madhukar, Madhu S.↗

Graphite Oxidation Rate Study on ET-10 and ETU-10 Grades - Task 4: QA Support and Testing for Structural Graphite Oxidation

INL performed targeted oxidation tests to measure oxidation rates for samples of ET-10 and ETU-10 graphite under CRADA No. 21CRA22 Mod. 3, Annex A, “Tritium Testing to Support Kairos Power Advanced Reactor Demonstration” (04/02/2024). All testing was conducted within INL’s Carbon Characterization Laboratory (CCL) using test standard ASTM D7542-21 "Standard Test Method for Air Oxidation of Carbon and Graphite in the Kinetic Regime" [ASTM International, 2021]. Kairos Power provided all test specimens through its graphite vendor Ibiden, Inc. to INL and ASTM specimen specified dimensions. Information within this report only provides the Arrhenius oxidation rate plots as a function of temperature for each graphite grade tested. The raw mass loss per time data will be provided on the Nuclear Data Management and Analysis System (NDMAS) portal located on the INL information system.

36 MATERIALS SCIENCE↗

Stiffness change of a graphite epoxy laminate under reverse fatigue loading

The stiffness of a flat specimen, made of graphite epoxy (T300/934), was measured during reverse fatigue loading. Laminates of basic layup, unidirectional cross-ply and angle-ply, as well as multidirectional (isotropic) layup, were tested. It was found that all the laminates exhibit rapid stiffness degradation on the last (third) fatigue stage. Except for the 0-deg unidirectional laminate, the last stage starts at about 70 to 80 percent of the fatigue life, regardless of the load level and the final mode of failure (tension or compression). It is shown that, for this material, stiffness degradation is a result of crack accumulation, mainly along the fibers, even for the fiber dominated laminates. This general phenomenon can serve to predict usable safe life of laminates under fatigue loading.

Rotem, Assa↗

Stiffness Study of Wound-Filament Pressure Vessels

Report presents theoretical and experimental study of stiffness of lightweight, jointed pressure vessels made of wound graphite fibers and epoxy. Specimens fabricated from layers of graphite fibers, wet with epoxy, on aluminum mandrel. Segment ends thickened with interspersed layers of axially oriented fibers to reduce pinhole bearing stresses and local deformations. Segments cured at 390 degrees F (199 degrees C). Report presents results of vibrational tests of one-quarter-scale models of wound-filament pressure vessels.

Verderaime, V.↗

Investigation of Oxidation-Resistant Coatings on Graphite and Molybdenum in Two Arc-Powered Facilities

A number of leading-edge specimens of ATJ graphite and 0.5-percent titanium-molybdenum alloy were tested in a 6-inch subsonic low-pressure arc-powered tunnel and a 1,500-kw subsonic arc jet to determine the effectiveness of several refractory coatings in preventing the oxidation of these materials. The results indicate that the siliconized coating for the ATJ graphite and the W-2 and Durak MG coatings for the titanium-molybdenum alloy provide adequate protection at temperatures up to 3,000 F for the durations of the tests in these facilities, approximately 70 seconds in the arc tunnel and approximately 10 minutes in the arc jet. Weight losses (less than one-half of 1 percent) experienced by a few of the coated specimens indicate that tests of longer duration in these environments may prove deleterious and that the stability of these coatings may be depreciated under the low-pressure environmental conditions encountered during reentry.

Peters, Roger W.↗

Sub-ply level scaling approach investigated for graphite-epoxy composite beam columns

Scale model graphite-epoxy composite specimens were fabricated using the 'sub-ply level' approach and tested as beam-columns under an eccentric axial load to determine the effect of specimen size on flexural response and failure. In the current research project, although the fiber diameters are not scaled, the thickness of the pre-preg material itself has been scaled by adjusting the number of fibers through the thickness of a single ply. Three different grades of graphite-epoxy composite material (AS4/3502) were obtained from Hercules, Inc., in which the number of fibers through the thickness of a single ply was reduced (Grade 190 with 12 to 16 fibers, Grade 95 with 6 to 8 fibers, and Grade 48 with 3 to 4 fibers). Thus, using the sub-ply level approach, a baseline eight ply quasi-isotropic laminate could be fabricated using either the Grade 48 or Grade 95 material and the corresponding full-scale laminate would be constructed from Grade 95 or standard Grade 190 material, respectively. Note that in the sub-ply level approach, the number of ply interfaces is constant for the baseline and full-scale laminates. This is not true for the ply level and sublaminate level scaled specimens. The three grades of graphite-epoxy composite material were used to fabricate scale model beam-column specimens with in-plane dimensions of 0.5*n x 5.75*n, where n=1,2,4 corresponsing to 1/4, 1/2, and full-scale factors. Angle ply, cross ply, and quasi-isotropic laminate stacking sequences were chosen for the investigation and the test matrices for each laminate type are given. Specimens in each laminate family with the same in-plane dimensions but different thicknesses were tested to isolate the influence of the thickness dimension on the flexural response and failure. Also, specific lay-ups were chosen with blocked plies and dispersed plies for each laminate type. Specimens were subjected to an eccentric axial load until failure. The load offset was introduced through a set of hinges which were attached to the platens of a standard load test machine. Three sets of geometrically scaled hinges were used to ensure that scaled loading conditions were applied. This loading condition was chosen because it promotes large flexural deformations and specimens fail at the center of the beam, away from the grip supports. Five channels of data including applied vertical load, end shortening displacement, strain from gages applied back-to-back at the midspan of the beam, and rotation of the hinge from a bubble inclinometer were recorded for each specimen. The beam-column test configuration was used previously to study size effects in ply level scaled composite specimens of the same material system, sizes, and stacking sequences. Thus, a direct comparison between the two scaling approaches is possible. Ply level scaled beam-columns with angle ply, cross ply, and quasi-isotropic lay-ups exhibited no size dependencies in the flexural response, but significant size effects in strength. The reduction in strength with increasing specimen size was not predicted successfully by analysis techniques. It is anticipated that results from this investigation will lead to a better understanding of the strength scale effect in composite structures.

Jackson, Karen E.↗

Baseline tensile tests of composite materials for LDEF (Long Duration Exposure Facility) exposure

Tensile specimens of five graphite fiber reinforced composite materials were tested at room temperature to provide baseline data for similar specimens exposed to the space environment in low-Earth orbit on the NASA Long Duration Exposure Facility. All specimens were 4-ply (+ or - 45 deg)s layups; at least five replicate specimens were tested for each parameter evaluated. Three epoxy-matrix materials and two polysulfone-matrix materials, several fiber volume fractions, and two sizes of specimen were evaluated. Stress-strain and Poisson's ratio-stress curves, ultimate stress, strain at failure, secant modulus at 0.004 strain, inplane shear stress-strain curves, and unidirectional shear modulus at .004 shear strain are presented.

Witte, William G.↗

Application of fracture mechanics to graphite under complex stress conditions

The purpose of this study was to examine the applicability of linear-elastic fracture mechanics to graphite under multiaxial stress conditions. The specimens were thick-walled graphite cylinders with flat heads which were internally pressurized. Two series of specimens were used. The first series had complete circumferential notches machined diagonally into the head-cylinder juncture region, while the second series was unnotched. The methods of linear-elastic fracture mechanics and a finite-element analysis were used to predict pressures to cause fracture for both notched and unnotched specimens.

Yahr, G. T.↗

Scale effects in the response and failure of fiber reinforced composite laminates loaded in tension and in flexure

The feasibility of using scale model testing for predicting the full-scale behavior of flat composite coupons loaded in tension and beam-columns loaded in flexure is examined. Classical laws of similitude are applied to fabricate and test replica model specimens to identify scaling effects in the load response, strength, and mode of failure. Experiments were performed on graphite-epoxy composite specimens having different laminate stacking sequences and a range of scaled sizes. From the experiments it was deduced that the elastic response of scaled composite specimens was independent of size. However, a significant scale effect in strength was observed. In addition, a transition in failure mode was observed among scaled specimens of certain laminate stacking sequences. A Weibull statistical model and a fracture mechanics based model were applied to predict the strength scale effect since standard failure criteria cannot account for the influence of absolute specimen size on strength.

Jackson, Karen E.↗

Nonlinear response and failure characteristics of internally pressurized composite cylindrical panels

Results of an experimental and analytical study of the nonlinear response and failure characteristics of internally pressurized 4- to 16-ply-thick graphite-epoxy cylindrical panels are presented. Specimens with clamped boundaries simulating the skin between two frames and two stringers of a typical transport fuselage were tested to failure. Failure results of aluminum specimens are compared with the graphite-epoxy test results. The specimens failed at their edges where the local bending gradients and interlaminar stresses are maximum. STAGS nonlinear two-dimensional shell analysis computer code results are used to identify regions of the panels where the response is independent of the axial coordinate. A geometrically nonlinear one-dimensional cylindrical panel analysis was derived and used to determine panel response and interlaminar stresses. Inclusion of the geometric nonlinearity was essential for accurate prediction of panel response. The maximum stress failure criterion applied to the predicted tensile stress in the fiber direction agreed best with the experimentally determined first damage pressures.

Boitnott, R. L.↗

Graphite-epoxy panel compression strength reduction due to local impact

The effects of low velocity impact on the compressive strength of graphite/epoxy structures are reviewed. Extensive tests were conducted on sandwich beams, laminated plates and stiffened panels. Conditions for failures were investigated by impact tests on statically loaded test specimens. Lightly loaded graphite structures (such as aircraft secondary structure) were insensitive to impact damage. In more heavily loaded structures, (such as wing panels), appreciable reductions in compressive strength occurred. The implications of the tests for structural design are discussed by comparing panel masses for designs where ultimate strains were reduced due to impact considerations with the masses of designs with higher ultimate strains. Preliminary test data are presented to show the possibility of improvements in damage to tolerance achievable by using an alternate matrix material.

Card, M. F.↗

Exploratory investigation of two resin-matrix composites subjected to arc-tunnel heating

Flexture and short beam shear specimens of a graphite epoxy and a graphite polymimide composite material were tested in an arc tunnel environment. The materials were subjected to seven heating rates from 12.5 to 308 kW/sw m for test times from 5 to 1000 seconds. The temperature response of the specimens was measured and the strength degradation caused by the various heating environments was determined.

Pittman, C. M.↗

Space fabrication demonstration system

The development effort on the composite beam cap fabricator was completed within cost and close to abbreviated goals. The design and analysis of flight weight primary and secondary beam builder structures proceeded satisfactorily but remains curtailed until further funding is made available to complete the work. The induction fastening effort remains within cost and schedule constraints. Tests of the LARC prototype induction welder is continuing in an instrumented test stand comprised of a Dumore drill press (air over oil feed for variable applied loads) and a dynamometer to measure actual welding loads. Continued testing shows that the interface screening must be well impregnated with resin to ensure proper flow when bonding graphite-acrylic lap shear samples. Specimens prepared from 0.030 inch thick graphite-polyethersulfone are also available for future induction fastening evaluation.

Source record↗

The 737 graphite composite flight spoiler flight service evaluation

The flight service experience of 108 graphite-epoxy spoilers on 737 transport aircraft, and related ground-based environmental exposure of graphite-epoxy material specimens were evaluated. Four spoilers were installed on each of 27 aircraft for a 5-year study. As of February 28, 1975, a total of 294,280 spoiler flight-hours and 460,686 spoiler landings were accumulated. Based on visual, ultrasonic, and destructive testing, no moisture migration into the honeycomb core and no core corrosion has occurred. Tests of removed spoilers and of ground-based exposure specimens after the first year of service indicate no significant changes in composite strength.

Stoecklin, R. L.↗