Detector with Adjustable Aperture for Electron Beam Monitoring
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46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
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Pioneer Venus small probes net flux radiometer experiment
The University of Wisconsin net flux experiment on the Pioneer Venus mission investigated the distribution of radiative energy deposition and loss which drives atmospheric circulation on Venus. The instrument used an external sensor and a novel method of chopping to measure the net flux of solar and planetary radiation during descent through the thick Venus atmosphere. The sensor, consisting of a high temperature flux plate detector and protective diamond windows, was designed to make accurate flux measurements while exposed to the severe Venus environment.
Sromovsky, L. A.↗
A novel diamond-like carbon based photocathode for PICOSEC Micromegas detectors
The PICOSEC Micromegas (MM) detector is a precise timinggaseous detector based on a MM detector operating in a two-stageamplification mode and a Cherenkov radiator. Prototypes equippedwith cesium iodide (CsI) photocathodes have shown promising timeresolutions as precise as 24 picoseconds (ps) for Minimum IonizingParticles. However, due to the high hygroscopicity andsusceptibility to ion bombardment of the CsI photocathodes,alternative photocathode materials are needed to improve therobustness of PICOSEC MM. Diamond-like Carbon (DLC) film have beenintroduced as a novel robust photocathode material, which have shownpromising results. A batch of DLC photocathodes with differentthicknesses were produced and evaluated using ultraviolet light. Thequantum efficiency measurements indicate that the optimizedthickness of the DLC photocathode is approximately3 nm. Furthermore, DLC photocathodes show good resistance to ionbombardment in aging test compared to the CsI photocathode. Finally,a PICOSEC MM prototype equipped with DLC photocathodes was tested inmuon beams. A time resolution of around 42 ps with a detectionefficiency of 97% for 150 GeV/c muons were obtained. These resultsindicate the great potential of DLC as a photocathode for thePICOSEC MM detector.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Uniformity and transmission of proportional counter window materials for use with AXAF
The X-ray detection system used to calibrate the Advanced X-ray Astrophysics Facility (AXAF) mirrors will include gas flow and sealed proportional counters. To meet the ultimate 1 percent goal of the calibration project, the transmission and uniformity of the windows must be well known for the soft X-ray wavelengths involved. Various window materials for use with proportional counters are examined for transmission at X-ray wavelengths in the range of 0.1 to 5.9 keV. These include the usual window materials (polypropylene and beryllium), as well as materials only recently employed for detector applications (polyimide and diamond). The transmission uniformity of beryllium at 1.49 keV is examined with a microchannel plate detector, producing a 'shadowgraph' of the window material illuminated with soft X-rays. This technique allows us to investigate nonuniformities on a spatial scale of about .2 mm.
Flanagan, K.↗
Geant4 and MCNP6.2 modeling of fast-neutron detectors based on single-crystal chemical vapor deposition diamond
Poster for the upcoming SPIE Conference, see https://spie.org/opo/conferencedetails/x-ray-gamma-ray-neutron-detector-physics, due August 17. A manuscript for this poster has also been published
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
A Study of the Radiation Tolerance of CVD Diamond to 70 MeV Protons, Fast Neutrons and 200 MeV Pions
We measured the radiation tolerance of commercially available diamonds grown by the Chemical Vapor Deposition process by measuring the charge created by a 120 GeV hadron beam in a 50 μm pitch strip detector fabricated on each diamond sample before and after irradiation. We irradiated one group of samples with 70 MeV protons, a second group of samples with fast reactor neutrons (defined as energy greater than 0.1 MeV), and a third group of samples with 200 MeV pions, in steps, to (8.8±0.9) × 1015 protons/cm2, (1.43±0.14) × 1016 neutrons/cm2, and (6.5±1.4) × 1014 pions/cm2, respectively. By observing the charge induced due to the separation of electron–hole pairs created by the passage of the hadron beam through each sample, on an event-by-event basis, as a function of irradiation fluence, we conclude all datasets can be described by a first-order damage equation and independently calculate the damage constant for 70 MeV protons, fast reactor neutrons, and 200 MeV pions. We find the damage constant for diamond irradiated with 70 MeV protons to be 1.62±0.07(stat)±0.16(syst)× 10−18 cm2/(p μm), the damage constant for diamond irradiated with fast reactor neutrons to be 2.65±0.13(stat)±0.18(syst)× 10−18 cm2/(n μm), and the damage constant for diamond irradiated with 200 MeV pions to be 2.0±0.2(stat)±0.5(syst)× 10−18 cm2/(π μm). The damage constants from this measurement were analyzed together with our previously published 24 GeV proton irradiation and 800 MeV proton irradiation damage constant data to derive the first comprehensive set of relative damage constants for Chemical Vapor Deposition diamond. We find 70 MeV protons are 2.60 ± 0.29 times more damaging than 24 GeV protons, fast reactor neutrons are 4.3 ± 0.4 times more damaging than 24 GeV protons, and 200 MeV pions are 3.2 ± 0.8 more damaging than 24 GeV protons. We also observe the measured data can be described by a universal damage curve for all proton, neutron, and pion irradiations we performed of Chemical Vapor Deposition diamond. Finally, we confirm the spatial uniformity of the collected charge increases with fluence for polycrystalline Chemical Vapor Deposition diamond, and this effect can also be described by a universal curve.
36 MATERIALS SCIENCE↗
Charge collection efficiency of diamond and silicon sensors irradiated with alpha particles
To evaluate the viability of using semiconductors as sensor materials in a detector for the Associated Particle Imaging technique, the radiation hardness of silicon and diamond diodes to alpha particles has been assessed. Here, the detector lifetimes for both silicon and diamond sensors were measured under the prolonged exposure to alpha particles emitted by an 241 Am source. The silicon detector was exposed to alpha radiation for approximately two months, reaching an accumulated fluence of ~ 1.5 x 10 12 α cm –2 . Additionally, by using a high purity single-crystal diamond with coplanar electrodes operating with full charge collection, the diamond detector response was measured over approximately ten months reaching an accumulated fluence of over 6 x 10 12 α cm –2 cm.
47 OTHER INSTRUMENTATION↗
Geant4 and MCNP6.2 modeling of fast-neutron detectors based on single-crystal chemical vapor deposition diamond
Manuscript for a poster to be presented at SPIE Optics + Photonics 2020 Digital Forum, 24-28 August 2020, https://spie.org/opo/conferencedetails/x-ray-gamma-ray-neutron-detector-physics.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Scanning X-Ray Diffraction Microscopy for Diamond Quantum Sensing
An understanding of nano- and microscale crystal strain in chemical-vapor-deposition diamond is crucial to the advancement of diamond quantum technologies. In particular, the presence of such strain and its characterization presents a challenge to diamond-based quantum sensing and information applications-as well as for future dark-matter detectors, where the directional information about incoming particles is encoded in crystal strain. Here, we exploit nanofocused scanning x-ray diffraction microscopy to quantitatively measure crystal deformation from defects in diamond with high spatial and strain resolution. The combination of information from multiple Bragg angles allows stereoscopic three-dimensional modeling of strain-feature geometry; the diffraction results are validated via comparison to optical measurements of the strain tensor based on spin-state-dependent spectroscopy of ensembles of nitrogen-vacancy centers in the diamond. Finally, our results demonstrate both strain and spatial resolution sufficient for directional detection of dark matter via x-ray measurement of crystal strain and provide a promising tool for diamond growth analysis and improvement of defect-based sensing.
42 ENGINEERING↗
Charged particle diagnostics for inertial confinement fusion and high-energy-density physics experiments
MeV-range ions generated in inertial confinement fusion (ICF) and high-energy-density physics experiments carry a wealth of information, including fusion reaction yield, rate, and spatial emission profile; implosion areal density; electron temperature and mix; and electric and magnetic fields. Here, the principles of how this information is obtained from data and the charged particle diagnostic suite currently available at the major US ICF facilities for making the measurements are reviewed. Time-integrating instruments using image plate, radiochromic film, and/or CR-39 detectors in different configurations for ion counting, spectroscopy, or emission profile measurements are described, along with time-resolving detectors using chemical vapor deposited diamonds coupled to oscilloscopes or scintillators coupled to streak cameras for measuring the timing of ion emission. A brief description of charged-particle radiography setups for probing subject plasma experiments is also given. The goal of the paper is to provide the reader with a broad overview of available capabilities, with reference to resources where more detailed information can be found.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Nature and origin of interstellar diamond from the Allende CV3 meteorite
Data and experimental evidence which support the contention that the C delta diamonds may result from grain-grain collisions in supernova shocks in the interstellar medium are presented. Fragments of the Allende CV3 chondrite were acid-treated. A whitish powder was obtained. For the Analytical Electron Microscopy (AEM) a small drop of ethanol suspension was transferred onto holey carbon support films on 3 mm EM grids. The AEM was performed on transmission-thin fragments of the material which overlay holes in the film, to eliminate interference from the substrate. Electron Spectroscopy for Chemical Analysis (ESCA) was performed on a large aliquot of C. Diamond was identified by selected area electron diffraction. Scanning Transmission Electron Microscope / Energy Dispersive X-ray (STEM-EDS) microanalyses of the C delta diamond, using a light-element detector, show that oxygen and possibly nitrogen are the only impurities consistently present. ESCA spectra from bulk C delta material confirm the presence of N at a level of 0.35 percent or less. Under UV irradiation a yellow-red fluorescence is observed, consistent with that of natural diamonds containing substitutional N. Electron Energy Loss Spectra (EELS) were recorded at 2 eV resolution from the C delta diamond, high pressure synthetic diamond, a diamond film produced in a low pressure plasma by chemical vapor deposition (CVD) on a heated silicon substrate (Roy, 1987), graphite, and amorphous arc sputtered carbon. Comparison of the carbon K edge shape and fine structure shows the Allende C delta phase to be largely diamond, but with a significant pre-edge absorption feature indicative of transitions of C 1s electrons into pi asterisk orbitals which are absent in the purely sp(3)-bonded diamond but present in graphite and amorphous carbon.
Blake, David↗
Directional detection of dark matter using solid-state quantum sensing
Next-generation dark matter (DM) detectors searching for weakly interacting massive particles (WIMPs) will be sensitive to coherent scattering from solar neutrinos, demanding an efficient background-signal discrimination tool. Directional detectors improve sensitivity to WIMP DM despite the irreducible neutrino background. Wide-bandgap semiconductors offer a path to directional detection in a high-density target material. A detector of this type operates in a hybrid mode. Here, the WIMP or neutrino-induced nuclear recoil is detected using real-time charge, phonon, or photon collection. The directional signal, however, is imprinted as a durable sub-micron damage track in the lattice structure. This directional signal can be read out by a variety of atomic physics techniques, from point defect quantum sensing to x-ray microscopy. In this Review, we present the detector principle as well as the status of the experimental techniques required for directional readout of nuclear recoil tracks. Specifically, we focus on diamond as a target material; it is both a leading platform for emerging quantum technologies and a promising component of next-generation semiconductor electronics. Based on the development and demonstration of directional readout in diamond over the next decade, a future WIMP detector will leverage or motivate advances in multiple disciplines toward precision dark matter and neutrino physics.
72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
Flexible positioning of a large area detector using an industrial robot
The DIAD beamline for Dual Imaging and Diffraction at Diamond Light Source has opted to use an industrial robot to position its Dectris Pilatus 2M CdTe diffraction detector. This setup was chosen to enable flexible positioning of the detector in a quarter-sphere around the sample position whilst reliably holding the large weight of 139 kg of detector, detector mount and cabling in a stable position. Metrology measurements showed that the detector can be positioned with a linear repeatability of <19.7 µm and a rotational repeatability of <16.3 µrad. The detector position stays stable for a 12 h period with <10.1 µm of movement for linear displacement and <3.8 µrad for rotational displacement. X-ray diffraction from calibration samples confirmed that the robot is sufficiently stable to resolve lattice d-spacings within the instrumental broadening given by detector position and beam divergence.
36 MATERIALS SCIENCE↗
PACE OCI Short-Wave Infrared Detection Assembly Optical System Design, Alignment, and Environmental Test
The Ocean Color Instrument (OCI), which will be integrated with the Plankton, Aerosol, Cloud, ocean Ecosystem (PACE) satellite, will collect science data that will be used to monitor the health of Earth’s oceans and atmosphere. The Short-Wave Infrared (SWIR) Detection Assembly (SDA), built and characterized by Utah State University Space Dynamics Laboratory (SDL), is a subsystem of OCI consisting of 32 channels covering seven discrete optical bands of interest. A total of 16 SWIR Detection Subassemblies (SDSs) compose the SDA and house the cold optical system. The science data optical input for each SDS is supplied by a 0.22 NA multimode fiber interfacing with a fiber adapter. The diverging light from the fiber is collimated, split by a dichroic beamsplitter to two separate channels, filtered by the science filter, and then reimaged onto the single-element detectors with a final 0.76 NA. Aspheric, diamond-turned powered elements are used throughout the optical design. Fabrication and alignment tolerance analysis/budgets are balanced to ensure the optical system meets throughput requirements. All systems are aligned at ambient temperature using an InSb camera and an in-line illumination microscope system to directly image the active detector area through the science filters. Compensators used during alignment are detector focus and decenter, which are adjusted via photoetched shims in increments of 25 µm. Average focus and centering errors were less than 8 µm among all 32 flight and 10 flight spare detectors. Each SDS spectral response and conversion gain was verified at operational temperature of -65°C in vacuum.
OCI↗
Photocathode characterisation for robust PICOSEC Micromegas precise-timing detectors
The PICOSEC Micromegas detector is a precise-timing gaseous detector based on a Cherenkov radiator coupled with a semi-transparent photocathode and a Micromegas amplifying structure, targeting a time resolution of tens of picoseconds for minimum ionising particles. Initial single-pad prototypes have demonstrated a time resolution below σ = 25 ps, prompting ongoing developments to adapt the concept for High Energy Physics applications, where sub-nanosecond precision is essential for event separation, improved track reconstruction and particle identification. The achieved performance is being transferred to robust multi-channel detector modules suitable for large-area detection systems requiring excellent timing precision. To enhance the robustness and stability of the PICOSEC Micromegas detector, research on robust carbon-based photocathodes, including Diamond-Like Carbon (DLC) and Boron Carbide (B 4 C), is pursued. Results from prototypes equipped with DLC and B 4 C photocathodes exhibited a time resolution of σ ≈ 32 ps and σ ≈ 34.5 ps, respectively. Efforts dedicated to improve detector robustness and stability enhance the feasibility of the PICOSEC Micromegas concept for large experiments, ensuring sustained performance while maintaining excellent timing precision.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Evaluation of radiation hardness of semiconductor materials against alpha particles for an API detector
An Associated Particle Imaging (API) system consists of a high vacuum chamber where deuterium ions are accelerated on a tritium-loaded target, resulting in alpha particles and neutrons emitted back-to-back, the latter escaping the chamber and used, for example, for tomography of a high-Z sample. An accurate determination of the alpha position is crucial to determine the trajectory of the neutron. Existing API systems have several limitations which a semiconductor-based API detector placed inside the vacuum chamber should not present. The semiconductor material can be either silicon or diamond. In particular, large and fast signals are generated by the alpha interactions in these materials. A pixelated API detector will measure the time and hit position of the alphas produced in the reaction. However, during the lifetime of the generator, the semiconductor detector will be exposed to an intense flux of alpha particles that will degrade its performance over time. To assess the radiation hardness of silicon and diamond against the alpha particles, we exposed single diodes made of either of the two materials to a 5 MeV alpha flux generated by an 241Am radioactive source. During irradiation, the diodes were biased and mounted on current-sensitive preamplifier boards. We have therefore been able to measure insitu the evolution of the waveforms as the damage was accumulating in their substrates.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Excellent Timing Cherenkov Light Detection for Dual-readout High-granularity Calorimetry
We are developing a Cherenkov detector aiming for applications in the next-generation calorimetry. It is a calorimetry that combines dual-readout and high-granularity with excellent timing capability. This work is to prove the concept of the Cherenkov detector utilizing a resistive plate chamber (RPC) with Diamond-Like Carbon as resistive electrode. The first prototype was tested with β-rays and cosmic-rays. This paper discusses the behavior of the charge spectrum and the time resolution of the first prototype.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Novel Sensors for Particle Tracking: a Contribution to the Snowmass Community Planning Exercise of 2021
Five contemporary technologies are discussed in the context of their potential roles in particle tracking for future high energy physics applications. These include sensors of the 3D configuration, in both diamond and silicon, submicron-dimension pixels, thin film detectors, and scintillating quantum dots in gallium arsenide. Drivers of the technologies include radiation hardness, excellent position, vertex, and timing resolution, simplified integration, and optimized power, cost, and material.
Detectors↗