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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Difficult Measurements of Materials Systems at Cryogenic Temperatures: Cryo-EELS and Cryo-4D-STEM

Scanning/transmission electron microscopy (S/TEM) in materials science has traditionally been accomplished at room temperature due to their solid state in this temperature range and relative insensitivity to radiolysis damage. Cooling to cryogenic temperatures tended to introduce instabilities such as vibration and drift and can lead to the buildup of carbon contamination or ice reducing contrast. The need to expand TEM experimental techniques into new fields such as quantum and battery materials led to new efforts to reduce these instabilities while achieving temperatures at or well below liquid nitrogen (77 K). Further, developments in detector and spectrometer technology brought new capabilities for high resolution electron energy loss spectroscopy (EELS) and scanning nanodiffraction (4D-STEM). These experimental modalities can require even tighter controls of drift, vibration, and exposure time. Here this presentation will discuss accomplishing difficult experiments at cryogenic temperatures in honor of the late Dr. Lena Kourkoutis who inspired and led many such experiments.

36 MATERIALS SCIENCE↗
NASA NTRS2006

High-sensitivity cryogenic temperature sensors using pressurized fiber Bragg gratings

Cryogenic temperature sensing was studied using a pressurized fiber Bragg grating (PFBG). The PFBG was obtained by simply applying a small diametric load to a regular fiber Bragg grating (FBG), which was coated with polyimide of a thickness of 11 micrometers. The Bragg wavelength of the PFBG was measured at temperatures from 295 to 4.2 K. A pressure-induced transition occurred at 200 K during the cooling cycle. As a result the temperature sensitivity of the PFBG was found to be nonlinear but reach 24 pm/K below 200 K, more than three times the regular FBG. For the temperature change from 80 K to 10 K, the PFBG has a total Bragg wavelength shift of about 470 pm, 10 times more than the regular FBG. From room temperature to liquid helium temperature the PFBG gives a total wavelength shift of 3.78 nm, compared to the FBG of 1.51 nm. The effect of the coating thickness on the temperature sensitivity of the gratings is also discussed.

Wu, Meng-Chou↗
NASA NTRS2006

High-sensitivity Cryogenic Temperature Sensors using Pressurized Fiber Bragg Gratings

Cryogenic temperature sensing was studied using a pressurized fiber Bragg grating (PFBG). The PFBG was obtained by simply applying a small diametric load to a regular fiber Bragg grating (FBG), which was coated with polyimide of a thickness of 11 micrometers. The Bragg wavelength of the PFBG was measured at temperatures from 295 to 4.2 K. A pressure-induced transition occurred at 200 K during the cooling cycle. As a result the temperature sensitivity of the PFBG was found to be nonlinear but reach 24 pm/K below 200 K, more than three times the regular FBG. For the temperature change from 80 K to 10 K, the PFBG has a total Bragg wavelength shift of about 470 pm, 10 times more than the regular FBG. From room temperature to liquid helium temperature the PFBG gives a total wavelength shift of 3.78 nm, compared to the FBG of 1.51 nm. The effect of the coating thickness on the temperature sensitivity of the gratings is also discussed.

Wu, Meng-Chou↗
NASA NTRS2006

Method to increase the toughness of aluminum-lithium alloys at cryogenic temperatures

A method to increase the toughness of the aluminum-lithium alloy C458 and similar alloys at cryogenic temperatures above their room temperature toughness is provided. Increasing the cryogenic toughness of the aluminum-lithium alloy C458 allows the use of alloy C458 for cryogenic tanks, for example for launch vehicles in the aerospace industry. A two-step aging treatment for alloy C458 is provided. A specific set of times and temperatures to age the aluminum-lithium alloy C458 to T8 temper is disclosed that results in a higher toughness at cryogenic temperatures compared to room temperature. The disclosed two-step aging treatment for alloy 458 can be easily practiced in the manufacturing process, does not involve impractical heating rates or durations, and does not degrade other material properties.

Sankaran, Krishnan K.↗
NASA NTRS1983

A technique for dynamically calibrating pressure transducers at cryogenic temperatures

A technique was developed for the calibration of dynamic pressure transducers at cryogenic temperatures. The calibration system utilizes an 8.9 Newton peak thrust shaker which oscillates a helium-filled bellows to generate a sinusoidal dynamic pressure to calibrate transducers immersed in a cryogenic environment. The system has a dynamic pressure measurement uncertainty of approximately 11% and is capable of producing peak-to-peak dynamic pressure amplitudes of 1.4 kPa over a frequency range of 40 to 100 hertz and a temperature range of 100 to 300 K. It provides an unprecedented capability of both static and dynamic calibration of pressure transducers from ambient to cryogenic temperature.

Gibbens, B. V.↗
NASA NTRS1976

Experimental investigation to validate use of cryogenic temperatures to achieve high Reynolds numbers in boattail pressure testing

An investigation has been conducted in the Langley 1/3 meter transonic cryogenic tunnel to validate the use of cryogenic temperatures to achieve high Reynolds numbers in nozzle boattail pressure testing. Tests were conducted at 0 degree angle of attack and at Mach numbers of 0.60, 0.85, and 0.90 on two wing-body configurations with differing boattail geometries. Test data were obtained by using two different techniques, the cryogenic method and the conventional method, to obtain the same Reynolds number. Later, the test data obtained from the two techniques on boattail pressure coefficient distributions and pressure drag coefficients were compared; results from the comparisons show excellent repeatability for all test conditions and indicate no measurable errors when using cryogenic temperatures to achieve high Reynolds numbers for nozzle boattail pressure testing.

Reubush, D. E.↗
NASA NTRSDate not supplied

Assessment of Using Ideal Gas for Predicting Boattail Flow at Cryogenic Temperatures

The applicability of using ideal gas assumptions to simulate high Reynolds number experimental data that was obtained at cryogenic temperatures is examined. Flow over an axisymmetric nozzle boattail model was calculated using reference temperatures of 117 K and 300 K and at Reynolds numbers from 50 to 200 million per meter. From the testing perspective, pressure, compression factor, and isentropic coefficients calculated using one-dimensional real gas equations are used to examine the departure of cryogenic flow from ideal gas flow across the range of temperatures and potential impacts on measured aerodynamic data. Solutions developed using ideal gas assumptions in a three-dimensional Navier-Stokes code are compared with experimental data obtained at cryogenic temperatures at two unit Reynolds numbers at freestream Mach numbers of 0.6 and 0.9. Results for several one- and two-equation turbulence models are shown. Predicted pressure coefficient distributions along the nozzle boattail differed from experimental data between 8% to less than 0.5% depending on the turbulence model and Mach number. The greatest discrepancy occurred in the level of static pressure recovery in the recompression region where the flow was separated. Solutions using warm and cryogenic freestream temperatures predicted similar boattail pressure distributions at the same unit Reynolds number.

Nozzle↗
NASA NTRSDate not supplied

Assessment of Using Ideal Gas for Predicting Boattail Flow at Cryogenic Temperatures

The applicability of using ideal gas assumptions to simulate high Reynolds number experimental data that was obtained at cryogenic temperatures is examined. Flow over an axisymmetric nozzle boattail model was calculated using reference temperatures of 117 K and 300 K and at Reynolds numbers from 50 to 200 million per meter. From the testing perspective, pressure, compression factor, and isentropic coefficients calculated using one-dimensional real gas equations are used to examine the departure of cryogenic flow from ideal gas flow across the range of temperatures and potential impacts on measured aerodynamic data. Solutions developed using ideal gas assumptions in a three-dimensional Navier-Stokes code are compared with experimental data obtained at cryogenic temperatures at two unit Reynolds numbers at freestream Mach numbers of 0.6 and 0.9. Results for several one- and two-equation turbulence models are shown. Predicted pressure coefficient distributions along the nozzle boattail differed from experimental data between 8% to less than 0.5% depending on the turbulence model and Mach number. The greatest discrepancy occurred in the level of static pressure recovery in the recompression region where the flow was separated. Solutions using warm and cryogenic freestream temperatures predicted similar boattail pressure distributions at the same unit Reynolds number.

Nozzle↗