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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
NASA NTRS1985

Containerless Processing of Glass Forming Melts in Space

The major objectives of this work are: (1) obtain quantitative evidence for the suppression of heterogeneous nucleation/crystallization in containerless melts in micro-g; (2) study melt homogenization in the absence of gravity driven convection; (3) develop the procedures for preparing precursor samples suitable for flight experiments; (4) perform comparative property analysis of glasses melted on Earth and in micro-g; (5) determine the feasibility of preparing glass shells in micro-g for use as laser fusion targets; and (6) assess the operational performance of the single axis acoustic levitator/furnace apparatus for processing multicomponent, glass forming melts in micro-g. Ways of obtaining these goals are discussed.

Day, D. D.↗
NASA NTRS1974

Acoustic field positioning for containerless processing

The non-contact positioning of materials in a space processing chamber is accomplished using a new type of acoustic levitator. Liquid and solid materials are positioned using a single source of sound. Fine control of position may be obtained by motion of an acoustical reflector. Electrical power required is usually less than 100 watts. The system operates satisfactorily at high and low temperatures and is adaptable as an add-on feature to existing space experiments. Containerless melting and solidification can be performed and a freely suspended liquid can be shaped to the contour of the sound field. Experiments are described in which aluminum, glass and plastic materials are melted and solidified in the containerless state. The system has applications to containerless crystal growth, melting and related processes.

Whymark, R. R.↗
NASA NTRS1975

Acoustic field positioning for containerless processing

The noncontact positioning of materials in a space processing chamber is accomplished using a new type of acoustic levitator. Liquid and solid materials are positioned using a single source of sound. Fine control of position may be obtained by motion of an acoustical reflector. The electrical power required is usually less than 100 watts. The system operates satisfactorily at high and low temperatures and is adaptable as an 'add-on' feature to existing space experiments. Containerless melting and solidification can be performed and a freely suspended liquid can be shaped to the contour of the sound field. Experiments are described in which aluminum, glass and plastic materials are melted and solidified in the containerless state. The system has applications to containerless crystal growth, melting and related processes.

Whymark, R. R.↗
NASA NTRS1985

Electric Field Containerless Processing Technology

The objective of this task is to develop the science and technology base required to design and construct a high temperature electric field positioning module that could be used by materials scientists to conduct containerless science experiments in a low gravity environment. Containerless science modules that employ electric fields to position and manipulate samples offer several advantages over acoustic or electromagnetic systems. The electric field system will operate not only at atmospheric pressures but also in a vacuum, in contrast to the acoustic modules which can only operate in atmosphere where the acoustic forces are sufficient. The electric field technique puts minimum energy into the sample, whereas the electromagnetic system can deposit energy into the sample through eddy current heat as well as physical mixing in the sample. Two types of electric field modules have been constructed and tested to date. One employs a charged sample and uses electrostatic forces to position and control the sample. The second type of module induces electrical polarization of the sample and electric field gradients to position and control the sample.

Elleman, D. D.↗
NASA NTRS1988

Containerless processing of glass forming melts in space

The near weightlessness of a material in the reduced gravity environment of space offers the opportunity of melting and cooling glass forming compositions without a container. This reduces the heterogeneous nucleation/crystallization which usually occurs at the walls of the container, thereby, extending the range of glass forming compositions. Based primarily on this idea, containerless glass forming experiments, which used a single axis acoustic levitator/furnace (SAAL), were conducted on SPAR rocket flights, 6 and 8, and on Space Shuttle mission, STS-7 and STS-61A. The experiments on the Space Shuttle were designed to include other studies related to melt homogenization and mixing, development of techniques for preparing uncontaminated preflight samples, and simple shaping experiments.

Day, D. E.↗
NASA NTRS1990

Containerless processing of fluoride glass

Ground-based experiments on glass formation, crystallization, surface tension, vaporization, and chemical durability of a zirconium-barium-lanthanum (ZBL) fluoride glass are summarized. In a container large, columnar grains grew out from the container-glass interface during cooling. The main crystalline phase was alpha BaZrF6. A ZBL glass sphere was levitated acoustically during Shuttle flight STS-11. The glass was melted and then cooled while being levitated (containerless). Crystallization in the recovered sample was very fine and mainly beta BaZr2F10, showing the influence of the container on the nucleation and microstructure of crystallization in the glass. Glass formation should be easier for a containerless glass than in a container.

Doremus, Robert H.↗
DOE OSTI2023

Electromagnetic levitation containerless processing of metallic materials in microgravity: rapid solidification

Space levitation processing allows researchers to conduct benchmark tests in an effort to understand the physical phenomena involved in rapid solidification processing, including alloy thermodynamics, nucleation and growth, heat and mass transfer, solid/liquid interface dynamics, macro- and microstructural evolution, and defect formation. Supported by ground-based investigations, a major thrust is to develop and refine robust computational tools based on theoretical and applied approaches. This work is accomplished in conjunction with experiments designed for precise model validation with application to a broad range of industrial processes.

42 ENGINEERING↗
NASA NTRS1977

Containerless processing of tungsten

Simultaneous electromagnetic levitation and electron-beam heating allow contaminationless melting of tungsten. Possible application for this technique is production of X-ray targets.

Beser, N.↗
NASA NTRS1977

Containerless processing of beryllium

Melting and solidification of a beryllium alloy containing 1.5% BeO by weight in the weightless environment of space has produced cast beryllium with a relatively uniform dispersion of BeO throughout. Examination of the cast material shows that it is coarse grained, although the BeO is not heavily agglomerated in the flight specimen. Ground based comparison experiments show extreme agglomeration and segregation of BeO, resulting in large zones which are practically free of the oxide. Several postulated hypotheses for the failure to grain refine the beryllium are formulated. These are: (1) spherodization of the BeO particles during specimen preparation and during the molten phase of the experiment; (2) loss of nucleation potency through aging in the molten phase; and (3) inability of BeO to act as a grain refiner for beryllium. Further investigation with non spherodized particles and shorter dwell times molten may delineate which of these hypotheses are valid. The results of this flight experiment indicate that the weightless environment of space is an important asset in conducting research to find grain refiners for beryllium and other metals for which cast dispersions of grain refining agents cannot be prepared terrestrially due to gravitationally driven settling and agglomeration.

Wouch, G.↗
NASA NTRS1982

Levitator for Containerless Processing

Objects are levitated by aerodynamic forces in an apparatus originally developed for space research but just as effective on Earth. New levitator is orientation-independent. Also works equally as well whether or not gravity is present. Apparatus supports a sphere by aerodynamic forces from gas flowing through convergent/divergent section. Concentric inner tube is moved along axis of cylindrical housing.

Berg, L. H.↗
NASA NTRS1982

The motion of bubbles inside drops in containerless processing

A theoretical model of thermocapillary bubble motion inside a drop, located in a space laboratory, due to an arbitrary axisymmetric temperature distribution on the drop surface was constructed. Typical results for the stream function and temperature fields as well as the migration velocity of the bubble were obtained in the quasistatic limit. The motion of bubbles in a rotating body of liquid was studied experimentally, and an approximate theoretical model was developed. Comparison of the experimental observations of the bubble trajectories and centering times with theoretical predictions lends qualified support to the theory.

Shankar, N.↗
NASA NTRS1984

Quenching Alloys in Containerless Processing

Magnetic levitation and gas quenching combined in proposed method to melt and rapidly solidify alloys without contacting container walls. Method used to develop new carbides for drill bits, high-ductility structured steel and new high-strength superplastic alloys.

Oran, W. A.↗
NASA NTRS1983

Electromagnetic levitation coil fabrication technique for MSFC containerless processing facilities

A technique is described for more reproducible fabrication of electromagnetic levitation coils. A split mandrel was developed upon which the coil is wound. After fabrication the mandrel can be disassembled to remove it from the coil. Previously, a full day was required to fabricate a levitation coil and the success rate for a functional coil was only 50 percent. About eight coils may be completed in one day using the technique developed and 95 percent of them are good levitation coils.

Ethridge, E. C.↗
NASA NTRS1986

Containerless processing of glass forming melts: D-1, MEA/A-2 experiment 81F01 conducted on STS-61A flight, October 1985

Results of experiment 81F01, which was conducted in the Material Experiment Assembly MEA/A-2 on the D-1 Spacelab Mission (STS-61A), are presented. The general plan of the experiment was to heat, melt, and quench six spherical samples of different glass forming compositions while they were levitated in a single axis acoustic levitator furnace (SAAL). In addition, two non-melting sintered alumina samples were used to check the operational characteristics of the SAAL under reduced gravity conditions. Three of the eight samples were levitated between 1250 and 1500 C before the lack of coolant created an over-temperature condition that caused the SAAL to shut down prematurely. Two of the three samples processed were calcia-gallia-silica and soda-lime-silica glass forming compositions. Evidence of a two to three times increase in the tendency for glass formation was obtained for the calcia-gallia-silica. The final glass appeared reasonably homogeneous even though it was made from hot pressed powders containing deliberate heterogeneities. A photographic record was obtained of the microgravity sample processing sequences.

Day, D. E.↗
NASA NTRS1987

Apparatus ad method for quiescent containerless processing of high temperature metals and alloys in low gravity

The electron bombardment furnace consists of two confinement grid sections which may be moved and separated from each other. Inside the bombardment furnace, a tungsten element is enclosed. The material specimen is located within the tungsten element and grounded by means of grounded support wires connected to the respective sections of the furnace. The material specimen is supported on the ground wires and heated by electron bombardment until melt occurs. The furnace sections are separated in opposite directions causing the ground wires to pull from the surfaces of the specimen, leaving the specimen freely suspended in the process chamber without the action of external forces. The specimen remains in its melt condition in the processing chamber where it can be undercooled without external forces acting on the specimen, which would cause dynamic nucleation.

Robinson, Michael B.↗
NASA NTRS1990

Containerless processing projects

The primary research objective was the examination of fundamental acoustics of the Drop Physics Module. An advanced chamber system was developed for acoustics and sample characterization. Sample interaction with an acoustic field was studied. The shaping of liquid drops by acoustic forces was also examined. The acoustic torque as a function of sample position and shape was studied along with levitated sample stability and the effects of feedback systems.

Source record↗
NASA NTRS1991

Containerless processing and rapid solidification of Nb-Si alloys of hypereutectic composition

A combination of bulk undercooling in an electromagnetic levitation apparatus and splat quenching between two copper plates is used to process Nb-Si alloys in order to maximize rapid solidification conditions and minimize the effects of recalescence, with emphasis on the solidification of characteristics of alloys in the 21 to 27 at. pct Si range of composition. SEM and TEM as well as X-ray diffraction are used to characterize the microstructures of the processed samples. In the range of compositions studied, the splat-quenched drops always formed the tetragonal Nb3Si phase directly from the liquid. Drops solidified in the coil were characterized by the presence of the primary intermetallic Nb5Si3 and the absence of both peritectic Nb3Si and the equilibrium eutectic. In these cases, a metastable alpha-Nb + beta-Nb5Si3 eutectic formed. The results are discussed in terms of possible metastable configurations of the Nb-Si phase diagram as well as concepts of nucleation and growth kinetics applied to the Nb3Si and Nb5Si3 intermetallics.

Hofmeister, W. H.↗