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At least 703 records · Page 39
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Study of interface reaction in a B 4 C/Cr mirror at elevated temperature using soft X-ray reflectivity

Boron carbide is a prominent material for high-brilliance synchrotron optics as it remains stable up to very high temperatures. The present study shows a significant change taking place at 550°C in the buried interface region formed between the Cr adhesive layer and the native oxide layer present on the silicon substrate. An in situ annealing study is carried out at the Indus-1 Reflectivity beamline from room temperature to 550°C (100°C steps). The studied sample is a mirror-like boron carbide thin film of 400 Å thickness deposited with an adhesive layer of 20 Å Cr on a silicon substrate. The corresponding changes in the film structure are recorded using angle-dependent soft X-ray reflectivity measurements carried out in the region of the boron K-edge after each annealing temperature. Analyses performed using the Parratt recursive formalism reveal that the top boron carbide layer remains intact but interface reactions take place in the buried Cr–SiO2 region. After 300°C the Cr layer diffuses towards the substrate. At higher temperatures of 500°C and 550°C the Cr reacts with the native oxide layer and tends to form a low-density compound of chromium oxysilicide (CrSiOx). Depth profiling of Si and Cr distributions obtained from secondary ion mass spectroscopy measurements corroborate the layer model obtained from the soft X-ray reflectivity analyses. Details of the interface reaction taking place near the substrate region of boron carbide/Cr sample are discussed.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2023

Photon-shot-noise-limited transient absorption soft X-ray spectroscopy at the European XFEL

Femtosecond transient soft X-ray absorption spectroscopy (XAS) is a very promising technique that can be employed at X-ray free-electron lasers (FELs) to investigate out-of-equilibrium dynamics for material and energy research. Here, a dedicated setup for soft X-rays available at the Spectroscopy and Coherent Scattering (SCS) instrument at the European X-ray Free-Electron Laser (European XFEL) is presented. It consists of a beam-splitting off-axis zone plate (BOZ) used in transmission to create three copies of the incoming beam, which are used to measure the transmitted intensity through the excited and unexcited sample, as well as to monitor the incoming intensity. Since these three intensity signals are detected shot by shot and simultaneously, this setup allows normalized shot-by-shot analysis of the transmission. For photon detection, an imaging detector capable of recording up to 800 images at 4.5 MHz frame rate during the FEL burst is employed, and allows a photon-shot-noise-limited sensitivity to be approached. The setup and its capabilities are reviewed as well as the online and offline analysis tools provided to users.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2020

Modular Isolated Soft-Switching Medium Voltage String Inverter for Large-Scale PV Farm

This paper presents a single-stage modular isolated soft-switching medium voltage string inverter (MVSI) with tri-port configuration to interconnect PV and storage to medium voltage (MV) grid. The modular MVSI provides advanced functionalities such as energy storage elements integration without additional converters, connection to MV grid resulting in lower distribution losses in the PV farm, high-frequency galvanic isolation, independent control of PV, storage and grid power, high modularity and scalability. The topology of the MVSI, operation principle and model-predictive priority-switching (MPPS) control to achieve fast dynamic balancing across stacked modules are discussed. The independent power control is validated in PLECS simulation and the operation of stacked MVSI with MPPS control is verified through Hardware-in-the-loop (HIL) simulation. Here, the hardware prototype of 25 kVA MVSI building block is developed. 18 kW experimental results of single building block verifying tri-ports operation and 20 kW experimental results of two modules stacked operation are presented. A clean sinusoidal waveform with negligibly low THD in both tests is obtained. A low dv/dt of <; 1kV/us and soft-switching are achieved.

30 DIRECT ENERGY CONVERSION↗
DOE OSTI2023

Origin of Soft-Switching Output Capacitance Loss in Cascode GaN HEMTs at High Frequencies

Output capacitance (C OSS ) loss (E DISS ) is produced when the C OSS of a power device is charged and discharged, which ideally should be a lossless process. This loss was recently revealed to be a crucial concern for GaN high electron mobility transistors (HEMTs) in high-frequency soft-switching applications. Among various GaN devices, the composite-type, cascode GaN HEMT was reported to show the largest E DISS with a voltage dependence distinct from discrete GaN HEMTs. However, the physical origins of the EDISS in cascode GaN HEMTs remain unclear. This work fills this gap by identifying three loss components and, for the first time, experimentally quantifying them in the multi-MHz resonant switching. These loss components include a) the avalanche loss of Si MOSFET, b) the intrinsic E DISS of GaN HEMT, and c) the Si avalanche-induced GaN turn-ON loss. The last component was found to dominate E DISS at high voltage. By eliminating the Si avalanche and the associated loss components (a) and (c), the E DISS of cascode GaN HEMTs can be reduced by up to 75% at the price of an increase in output charge and switching transition time. Furthermore, these results provide new physical insights and practical guidelines to trim the soft-switching loss of cascode GaN HEMTs in high-frequency applications.

42 ENGINEERING↗
DOE OSTI2016

Near-edge x-ray absorption fine structure spectroscopy at atmospheric pressure with a table-top laser-induced soft x-ray source

The authors present a table-top soft x-ray absorption spectrometer, accomplishing investigations of the near-edge x-ray absorption fine structure (NEXAFS) in a laboratory environment. The system is based on a low debris plasma ignited by a picosecond laser in a pulsed krypton gas jet, emitting soft x-ray radiation in the range from 1 to 5 nm. For absorption spectroscopy in and around the “water window” (2.3–4.4 nm), a compact helium purged sample compartment for experiments at atmospheric pressure has been constructed and tested. NEXAFS measurements on CaCl{sub 2} and KMnO{sub 4} samples were conducted at the calcium and manganese L-edges, as well as at the oxygen K-edge in air, atmospheric helium, and under vacuum, respectively. The results indicate the importance of atmospheric conditions for an investigation of sample hydration processes.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2016

SU-F-T-52: Study of Energy Dependent Effect of Dosimetry Systems Used in Therapeutic Soft X-Ray Energy Range

Purpose: To investigate energy dependent effects of different dosimetry systems which can be used as in vivo dosimetry monitoring for intraoperative radiotherapy in therapeutic soft x-ray energy range. Methods: Three dosimetry systems were evaluated in therapeutic soft x-ray energy range: optically stimulated luminescent dosimeter (OSLD) nanoDots, radiochromic EBT2 and EBT3 films. The x-ray photons were produced by a Zeiss Intrabeam 50 kV x-ray radiotherapy system. Solid water and bolus slabs with different thicknesses were used in the process of irradiation. An aluminum filter set was used to measure HVLs of X-rays. Calibration curves were made at different depth of boluses. Results: Half Value Layers at depths of 0, 3, 10, and 20 mm of solid water were measured to represent the energy change versus depth, yielding 0.306, 0.482, 0.865 and 0.901 respectively and indicating nearly unchanged HVL beyond 1 cm depth. The responses of each system at different depths were normalized to the response at 2 cm depth. In film dosimetry, the response is calculated as optical density (OD). The results show that there is nearly the same energy dependence for EBT2 and EBT3. At a HVL of 0.482 mm Al, the relative responses of nanoDots and EBT3 are 0.85 ± 0.04 and 0.89 ± 0.03 compared to those at 0.901 mm Al HVL, respectively, indicating no obvious difference between those two systems within the measurement uncertainty. Conclusion: It was observed that the studied dosimeter response increases about 13% from the x-ray energy of 0.48 mm Al to 0.90 mm Al. Therefore, caution should be exercised in using an appropriate calibration curve, and x-ray beam hardening effect has to be taken into account.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2015

Study of soft X-ray emission during wire array implosion under plasma focus conditions at the PF-3 facility

Results of measurements of soft X-ray emission with photon energies of <1 keV under conditions of a plasma focus (PF) experiment are presented. The experiments were carried out at the world’s largest PF device—the PF-3 Filippov-type facility (I ⩽ 3 MA, T/4 ≈ 15–20 µs, W{sub 0} ⩽ 3 MJ). X-ray emission from both a discharge in pure neon and with a tungsten wire array placed on the axis of the discharge chamber was detected. The wire array imploded under the action of the electric current intercepted from the plasma current sheath of the PF discharge in neon. The measured soft X-ray powers from a conventional PF discharge in gas and a PF discharge in the presence of a wire array were compared for the first time.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2015

Damage threshold of platinum coating used for optics for self-seeding of soft x-ray free electron laser

We investigated the experimental damage threshold of platinum coating on a silicon substrate illuminated by soft x-ray radiation at grazing incidence angle of 2.1 deg. The coating was the same as the blazed grating used for the soft X-ray self-seeding optics of the Linac Coherent Light Source free electron laser. The irradiation condition was chosen such that the absorbed dose was similar to the maximum dose expected for the grating. The expected dose was simulated by solving the Helmholtz equation in non-homogenous media. The experiment was performed at 900 eV photon energy for both single pulse and multi-shot conditions. We have not observed single shot damage. This corresponds to a single shot damage threshold being higher than 3 J/cm 2 . The multiple shot damage threshold measured for 10 shots and about 600 shots was determined to be 0.95 J/cm 2 and 0.75 J/cm 2 respectively. The damage threshold occurred at an instantaneous dose which is higher that the melt dose of platinum.

43 PARTICLE ACCELERATORS↗
DOE OSTI2013

Non-Hardware ("Soft") Cost-Reduction Roadmap for Residential and Small Commercial Solar Photovoltaics, 2013-2020

The objective of this analysis is to roadmap the cost reductions and innovations necessary to achieve the U.S. Department of Energy (DOE) SunShot Initiative's total soft-cost targets by 2020. The roadmap focuses on advances in four soft-cost areas: (1) customer acquisition; (2) permitting, inspection, and interconnection (PII); (3) installation labor; and (4) financing. Financing cost reductions are in terms of the weighted average cost of capital (WACC) for financing PV system installations, with real-percent targets of 3.0% (residential) and 3.4% (commercial).

14 SOLAR ENERGY↗
DOE OSTI2023

VeryFastCCD: a high frame rate soft X-ray detector

Direct X-ray detection in silicon has been transformative for scattering experiments in biology and materials science. While bump-bonded hybrid pixels have been attractive for hard X-ray detection, the challenge for single photon soft X-ray detection is sufficiently low noise. CCD structures on thick, high-resistivity silicon have been successfully used as sensors over the range of soft to hard X-rays at storage rings and FELs. The VeryFastCCD is a high frame rate, column-parallel CCD sensor with 48 μm pixels. Combined with 256-channel custom readout ASICs, frame rates of 5–10 kHz have been achieved with readout noise as low as 20 e and full-well capacity >4 × 10 5 e/pixel. Thin (10 nm and 100 nm) entrance window contact processes have also been developed which provide >85% quantum efficiency for 285 eV X-rays. Systems are currently being developed for several beamlines at the upgraded Advanced Light Source.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2016

SINGLE AND DOUBLE PHOTOIONIZATION AND PHOTODISSOCIATION OF TOLUENE BY SOFT X-RAYS IN A CIRCUMSTELLAR ENVIRONMENT

The formation of polycyclic aromatic hydrocarbons (PAHs) and their methyl derivatives mainly occurs in the dust shells of asymptotic giant branch (AGB) stars. The bands at 3.3 and 3.4 μm, observed in infrared emission spectra of several objects, are attributed C–H vibrational modes in aromatic and aliphatic structures, respectively. In general, the feature at 3.3 μm is more intense than that at 3.4 μm. Photoionization and photodissociation processes of toluene, the precursor of methylated PAHs, were studied using synchrotron radiation at soft X-ray energies around the carbon K edge using time-of-flight mass spectrometry. Partial ion yields of a large number of ionic fragments were extracted from single and 2D-spectra, where electron-ion coincidences have revealed the doubly charged parent molecule and several doubly charged fragments containing seven carbon atoms with considerable abundance. Ab initio calculations based on density functional theory were performed in order to elucidate the chemical structure of these stable dicationic species. The survival of the dications subjected to hard inner shell ionization suggests that they could be observed in the interstellar medium, especially in regions where PAHs are detected. The ionization and destruction of toluene induced by X-rays were examined in the T Dra conditions, a carbon-rich AGB star. In this context, a minimum photodissociation radius and the half-life of toluene subjected to the incidence of the soft X-ray flux emitted from a companion white dwarf star were determined.

74 ATOMIC AND MOLECULAR PHYSICS↗
DOE OSTI2016

SOFT X-RAY EXCESS FROM SHOCKED ACCRETING PLASMA IN ACTIVE GALACTIC NUCLEI

We propose a novel theoretical model to describe the physical identity of the soft X-ray excess that is ubiquitously detected in many Seyfert galaxies, by considering a steady-state, axisymmetric plasma accretion within the innermost stable circular orbit around a black hole (BH) accretion disk. We extend our earlier theoretical investigations on general relativistic magnetohydrodynamic accretion, which implied that the accreting plasma can develop into a standing shock under suitable physical conditions, causing the downstream flow to be sufficiently hot due to shock compression. We perform numerical calculations to examine, for sets of fiducial plasma parameters, the physical nature of fast magnetohydrodynamic shocks under strong gravity for different BH spins. We show that thermal seed photons from the standard accretion disk can be effectively Compton up-scattered by the energized sub-relativistic electrons in the hot downstream plasma to produce the soft excess feature in X-rays. As a case study, we construct a three-parameter Comptonization model of inclination angle θ {sub obs}, disk photon temperature kT {sub in}, and downstream electron energy kT {sub e}to calculate the predicted spectra in comparison with a 60 ks XMM-Newton /EPIC-pn spectrum of a typical radio-quiet Seyfert 1 active galactic nucleus, Ark 120. Our χ {sup 2}-analyses demonstrate that the model is plausible for successfully describing data for both non-spinning and spinning BHs with derived ranges of 61.3 keV ≲ kT {sub e}≲ 144.3 keV, 21.6 eV ≲ kT {sub in} ≲ 34.0 eV, and 17.°5 ≲ θ {sub obs} ≲ 42.°6, indicating a compact Comptonizing region of three to four gravitational radii that resembles the putative X-ray coronae.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2016

SOFT X-RAY IRRADIATION OF SILICATES: IMPLICATIONS FOR DUST EVOLUTION IN PROTOPLANETARY DISKS

The processing of energetic photons on bare silicate grains was simulated experimentally on silicate films submitted to soft X-rays of energies up to 1.25 keV. The silicate material was prepared by means of a microwave assisted sol–gel technique. Its chemical composition reflects the Mg{sub 2}SiO{sub 4} stoichiometry with residual impurities due to the synthesis method. The experiments were performed using the spherical grating monochromator beamline at the National Synchrotron Radiation Research Center in Taiwan. We found that soft X-ray irradiation induces structural changes that can be interpreted as an amorphization of the processed silicate material. The present results may have relevant implications in the evolution of silicate materials in X-ray-irradiated protoplanetary disks.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2016

A DEEP X-RAY VIEW OF THE BARE AGN ARK 120. I. REVEALING THE SOFT X-RAY LINE EMISSION

The Seyfert 1 galaxy Ark 120 is a prototype example of the so-called class of bare nucleus active galactic nuclei (AGNs), whereby there is no known evidence for the presence of ionized gas along the direct line of sight. Here deep (>400 ks exposure), high-resolution X-ray spectroscopy of Ark 120 is presented from XMM-Newton observations that were carried out in 2014 March, together with simultaneous Chandra /High Energy Transmission Grating exposures. The high-resolution spectra confirmed the lack of intrinsic absorbing gas associated with Ark 120, with the only X-ray absorption present originating from the interstellar medium (ISM) of our own Galaxy, with a possible slight enhancement of the oxygen abundance required with respect to the expected ISM values in the solar neighborhood. However, the presence of several soft X-ray emission lines are revealed for the first time in the XMM-Newton RGS spectrum, associated with the AGN and arising from the He- and H-like ions of N, O, Ne, and Mg. The He-like line profiles of N, O, and Ne appear velocity broadened, with typical FWHMs of ∼5000 km s{sup −1}, whereas the H-like profiles are unresolved. From the clean measurement of the He-like triplets, we deduce that the broad lines arise from a gas of density n {sub e} ∼ 10{sup 11} cm{sup −3}, while the photoionization calculations infer that the emitting gas covers at least 10% of 4 π steradian. Thus the broad soft X-ray profiles appear coincident with an X-ray component of the optical–UV broad-line region on sub-parsec scales, whereas the narrow profiles originate on larger parsec scales, perhaps coincident with the AGN narrow-line region. The observations show that Ark 120 is not intrinsically bare and substantial X-ray-emitting gas exists out of our direct line of sight toward this AGN.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS2000

Scaling and technology issues for soft error rates

Th effects of device technology and scaling on soft error rates are discussed, using information obtained from both the device and space communities as a guide to determine the net effect on soft errors.

soft error rate space radiation high-energy proton↗
NASA NTRS2016

Examining the Angular Resolution of the Astro-H's Soft X-Ray Telescopes

The international x-ray observatory ASTRO-H was renamed Hitomi after launch. It covers a wide energy range from a few hundred eV to 600 keV. It is equipped with two soft x-ray telescopes (SXTs: SXT-I and SXT-S) for imaging the soft x-ray sky up to 12 keV, which focus an image onto the respective focal-plane detectors: CCD camera (SXI) and a calorimeter (SXS). The SXTs are fabricated in a quadrant unit. The angular resolution in half-power diameter (HPD) of each quadrant of the SXTs ranges between 1.1 and 1.4 arc min at 4.51 keV. It was also found that one quadrant has an energy dependence on the HPD. We examine the angular resolution with spot scan measurements. In order to understand the cause of imaging capability deterioration and to reflect it to the future telescope development, we carried out spot scan measurements, in which we illuminate all over the aperture of each quadrant with a square beam 8 mm on a side. Based on the scan results, we made maps of image blurring and a focus position. The former and the latter reflect figure error and positioning error, respectively, of the foils that are within the incident 8 mm x 8 mm beam. As a result, we estimated those errors in a quadrant to be approx. 0.9 to 1.0 and approx. 0.6 to 0.9 arc min, respectively. We found that the larger the positioning error in a quadrant is, the larger its HPD is. The HPD map, which manifests the local image blurring, is very similar from quadrant to quadrant, but the map of the focus position is different from location to location in each telescope. It is also found that the difference in local performance causes energy dependence of the HPD.

Astro-H/Hitomi; soft x-ray telescope; SXT; Wolter ↗
NASA NTRSDate not supplied

Design and Analysis of the Rocket Experiment Demonstration of a Soft X-Ray (REDSoX) Polarimeter Mirror Module Assembly

The Rocket Experiment Demonstration of a Soft X-ray (REDSoX) Polarimeter is a NASA sounding rocket experiment that is designed to demonstrate the technology necessary for measuring linear X-ray polarization as a function of energy below 1 keV. In astrophysics, soft X-ray spectropolarimetry will be used to probe the nature of acceleration mechanisms in quasar jets and to test models of neutron star structure. NASA Marshall Space Flight Center (MSFC) has designed a grazing-incidence mirror module assembly (MMA) for the REDSoX payload and used Finite Element Modelling Software (ANSYS) to perform structural analysis of the design. In this paper we will describe the overall design of the REDSoX MMA, details of the analysis techniques used for predicting factor of safety in the mirror adhesive bonds and structural components, the buckling analysis of the outer housing, and the raytrace technique used to estimate the effect of gravity sag on optical performance during ground testing.

Structural Analysis↗
DOE OSTI2011

Real space soft x-ray imaging at 10 nm spatial resolution

Using Fresnel zone plates made with our robust nanofabrication processes, we have successfully achieved 10 nm spatial resolution with soft x-ray microscopy. The result, obtained with both a conventional full-field and scanning soft x-ray microscope, marks a significant step forward in extending the microscopy to truly nanoscale studies.

36 MATERIALS SCIENCE↗