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All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Data-driven picosecond X-ray imaging for quantitative plasma-induced shock characterization

Imaging dynamic events, especially shockwave behavior, is key to advancing high-energy-density (HED) research. Recent advances in fourth- and fifth-generation X-ray light sources allow for high-resolution imaging of fast phenomena, but limited beam time necessitates maximizing data acquisition. We present a benchtop-scale pulsed plasma device submerged in liquid heptane, capable of generating dynamic events at rates exceeding 10 Hz, supporting the field’s data-driven goals by producing large, high-quality imaging datasets. Using X-ray phase contrast imaging (XPCI) at the Advanced Photon Source, we imaged weak shockwaves (Mach ~ 1.2) in heptane interacting with plasma-induced cavitation bubbles, causing deviation from Rankine-Hugoniot behavior; to our knowledge, this represents the first direct imaging of such interaction. Our quantitative analysis offers insight into weak shock phenomena and energy-focusing applications in pulsed plasmas. These results highlight the potential for large datasets to advance dynamic HED research at current light source facilities, and have implications for fields such as inertial confinement fusion, plasma-enhanced chemical processing, and biomedical applications.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Absolute mass calibration of fission product distributions measured with the E-$v$ method

The mass calibration of fission product distributions measured with the energy–velocity (E-v) method constitutes a technical challenge. The energy loss of the fission fragments in the various dead layers of the spectrometer and other sources of pulse-height defects of the energy detectors are a significant source of systematic uncertainty in the mass calculations used to determine the measured fission product yields. Here, in this study, the absolute calibration of the fission mass distributions is accomplished by measuring prompt γ-rays in coincidence with the fission fragments. This allows for the direct calibration of the mass spectra and eliminates any dependence on potentially complicated energy corrections. The first test measurement was performed at the Los Alamos Neutron Science Center employing the SPectrometer for Ion DEtermination in fission Research (SPIDER). SPIDER is a 2E-2v spectrometer designed for measuring independent fission product yields from neutron-induced fission. In this test, the single-arm SPIDER (E-v) system and an array of 252 Cf sources were used. The single-arm system consisted of two time pick-off detectors for measuring the time-of-flight of the fission fragments and a double-sided silicon strip detector (DSSD) for measuring the kinetic energy. Characteristic γ-rays from fission fragments were detected using three high-purity germanium (HPGe) detectors. For the mass calibration, γ–mass coincidence events from twelve product isotopes were used. The measured FPYs from 252 Cf spontaneous fission were found to be in excellent agreement with the evaluated data after applying the absolute mass calibration. From the γ–mass coincidence events, the mass resolution of the system was also extracted. An average mass resolution of ~1.4 AMU (FWHM) for the light fragments and ~2.4 AMU (FWHM) for the heavy fragments were found. This was the first in-situ calibration and characterization of the SPIDER spectrometer, which paves the way for high-quality FPY measurements with this instrument.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2022

Photoinduced chemomimetic biocatalysis for enantioselective intermolecular radical conjugate addition

Exploiting nature’s catalysts for non-natural transformations that are inaccessible to chemocatalysis is highly desirable but challenging. On the one hand, the widespread nicotinamide-dependent oxidoreductases have not been utilized for single-electron-transfer-induced bimolecular cross-couplings; on the other, the addition of catalytic asymmetric radical con- jugate to terminal alkenes remains a challenge owing to strong racemic background reaction and unselective termination of prochiral radical species. Here we report a chemomimetic biocatalysitic approach for construction of alpha-carbonyl stereocentres via an unnatural intermolecular conjugate addition of N-(acyloxy)phthalimides-derived radicals with acceptor-substituted terminal alkenes, by combination of visible-light excitation and nicotinamide-dependent ketoreductases (KREDs). Based on protein crystal structure, we engineered KREDs via a semi-rational mutagenesis strategy to improve reaction outcomes with a small and high-quality variants library. Here, mechanistic investigations combining wet experiments, crystallographic studies and computational simulations demonstrate that the repurposed biocatalyst can suppress racemic background reaction and unselected side reactions, yielding enantioselectivity that is challenging to achieve by chemocatalysis.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

fpikachu96/KRED-data

Exploiting nature’s catalysts for non-natural transformations that are inaccessible to chemocatalysis is highly desirable but challenging. On the one hand, the widespread nicotinamide-dependent oxidoreductases have not been utilized for single-electron-transfer-induced bimolecular cross-couplings; on the other, the addition of catalytic asymmetric radical conjugate to terminal alkenes remains a challenge owing to strong racemic background reaction and unselective termination of prochiral radical species. Here we report a chemomimetic biocatalysitic approach for construction of alpha-carbonyl stereocentres via an unnatural intermolecular conjugate addition of N-(acyloxy)phthalimides-derived radicals with acceptor-substituted terminal alkenes, by combination of visible-light excitation and nicotinamide-dependent ketoreductases (KREDs). Based on protein crystal structure, we engineered KREDs via a semi-rational mutagenesis strategy to improve reaction outcomes with a small and high-quality variants library. Mechanistic investigations combining wet experiments, crystallographic studies and computational simulations demonstrate that the repurposed biocatalyst can suppress racemic background reaction and unselected side reactions, yielding enantioselectivity that is challenging to achieve by chemocatalysis.

Huang, Xiaoqiang↗
DOE OSTI2022

Analytic error analysis of cross section interpolation methods in nodal diffusion codes - I : Theory

This paper discusses two cross section interpolation methods commonly found in popular nodal codes; the partial derivatives and multiple tables models. The motivation for choosing a model, and thus a case matrix structure, is a trade off between accuracy and computational cost. Due to decades of experience, there are default structures that are sufficient for current light water reactor analysis. However, this is not necessarily the case for advanced reactor designs. Therefore, it is advantageous to understand the sources of error in cross section interpolation models so that the quality of a case matrix may be improved. A mathematical framework for these models is presented in this work that provides a more rigorous connection between the nuclear engineering field's cross section interpolation methods and the broader mathematical field of function approximation. The two cross section models examined in this paper were found to utilize Lagrange interpolation and are a subset of Lagrange tensor products. Classical results of Lagrange polynomial error analysis were then applied to the partial derivative and multiple tables models to derive expressions for the total point-wise error. The analytical results classify the total error into two parts: the model form error and interpolation error. Finally, based on our observations, a better foundation for improving the quality of a case matrix is proposed. (authors)

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2022

Simulating the X-ARAPUCA, DUNE's next generation light sensors

The word arapuca refers to a bird trap built by the indigenous peoples of Brazil. On the other hand, our ARAPUCA is a photon trap for Noble Gases' scintillation light and it is the sensitive element upon which DUNE's whole photon detection system is based on. Here we present a glimpse of our state-of-the-art simulation of such device, the ArapucaSim, highlighting its philosophy and main components. As an application, we present here one of the studies being carried out, on the effects of light reflections inside the light guide and how affects the overall photon detection efficiency. Based on these results, we are able to not only acquire a better understanding of the device but also impose limits on the quality of the mechanical polishing of such surfaces. The ArapucaSim was developed with two main goals in mind: to assist in R&D by allowing short turnout times between new ideas and experimental tests, and to bridge the gap between high-precision time-consuming hardware simulations and the full-scale models for DUNE's Photon Detection System. This research also led to the development new algorithms for simulating wavelength shifting/scintillation processes and dichroic filters, which will be properly described in future publications.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2022

SDSS J1058+5443: A Blue Quasar without Optical/NUV Broad Emission Lines

In this paper, the blue quasar SDSS J105816.19+544310.2 (=SDSS J1058+5443) at redshift 0.479 has been reported as the best true type 2 quasar candidate with the disappearance of central broad-line regions. There are no definite conclusions on the very existence of true type 2 active galactic nuclei (AGN), mainly due to detected optical broad emission lines in high-quality spectra of some previously classified true type 2 AGN candidates. Here, unlike previously reported true type 2 AGN candidates among narrow emission-line galaxies with weak AGN activities but strong stellar lights, the definitely blue quasar SDSS J1058+5443 can be well confirmed as a true type 2 quasar due to apparent quasar-shape blue continuum emissions but an apparent loss of both the optical broad Balmer emission lines and the near-UV (NUV) broad Mg II emission line. Based on different model functions and the F-test statistical technique, after considering blueshifted optical and UV Fe II emissions, there are no apparent broad optical Balmer emission lines and/or broad NUV Mg II lines, and the confidence level is smaller than 1σ in support of broad optical and NUV emission lines. Moreover, assuming the virialization assumption to broad-line emission clouds, the reconstructed broad emission lines strongly indicate that the probable intrinsic broad emission lines, if they exist, cannot be hidden or overwhelmed in the noise of the Sloan Digital Sky Survey spectrum of SDSS J1058+5443. Therefore, SDSS J1058+5443 is so far the best and most robust true type 2 quasar candidate, leading to the clear conclusion of the very existence of true type 2 AGN.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS1974

Hydrodynamic models of a cepheid atmosphere

A method for including the solution of the transfer equation in a standard Henyey type hydrodynamic code was developed. This modified Henyey method was used in an implicit hydrodynamic code to compute deep envelope models of a classical Cepheid with a period of 12(d) including radiative transfer effects in the optically thin zones. It was found that the velocity gradients in the atmosphere are not responsible for the large microturbulent velocities observed in Cepheids but may be responsible for the occurrence of supersonic microturbulence. It was found that the splitting of the cores of the strong lines is due to shock induced temperature inversions in the line forming region. The adopted light, color, and velocity curves were used to study three methods frequently used to determine the mean radii of Cepheids. It is concluded that an accuracy of 10% is possible only if high quality observations are used.

Karp, A. H.↗
NASA NTRS1984

Visual Systems for Remotely Controlled Vehicles

The Variable Acuity Remote Viewing System is discussed. It was conceived as a technique for resolving the field of view/resolution/ bandwidth tradeoffs that exist in remote viewing systems. This system is based on the fact that integration of the human eye acuity function shows only about 130,000 pixels are required to fully support the human vision. This quantity is well within the capabilities of conventional video systems. The technique utilizes a non-linear optical system in both the sensing and display equipment. The non-linearity is achieved by a special lens which translates a uniform pixel array on its image plane into the object field as a variable angular array. This lens will record the same angular detail the eye would see when viewing the same scene and compress this detail into a uniform matrix of equal sized picture elements on its image plane. This image can be scanned with a broadcast quality tv having a 525 line raster scan. Conventional transmission equipment can then also be used to send the image information to a remote location. When received, the image is projected by a light valve projector onto a hemispherical screen by an identical non-linear lens.

Rezek, T.↗
NASA NTRS1999

A Deployable Primary Mirror for Space Telescopes

NASA Langley Research Center, Composite Optics, Inc., and Nyma/ADF have developed jointly a deployable primary mirror for space telescopes that combines over five years of research on deployment of optical-precision structures and over ten years of development of fabrication techniques for optical-precision composite mirror panels and structures. The deployable mirror is directly applicable to a broad class of non-imaging "lidar" (light direction a nd ranging) telescopes whose figure-error requirements are in the range of one to ten microns RMS. Furthermore, the mirror design can be readily modified to accommodate imaging-quality reflector panels and active panel-alignment control mechanisms for application to imaging telescopes. The present paper: 1) describes the deployable mirror concept; 2) explains the status of the mirror development; and 3) provides some technical specifications for a 2.55- m-diameter, proof-of-concept mirror. Keywords: precision deployment, hinge joint, latch joint, deployable structures, fabrication, space telescopes, optical instruments, microdynamics.

Lake, Mark S.↗
NASA NTRS2006

Photorefractivity in WGM resonators

We report on observation of photorefractive effects in whispering gallery mode resonators made of as-grown and magnesium doped lithium niobate and lithium tantalate in the near as well as far infrared. The effects manifested themselves as dynamic modification of the spectra as well as quality factors of the resonators coupled to the laser radiation. We have observed a significant (exceeding 10-4) change of the ordinary index of refraction of all the materials exposed with 780 nm light. Photorefractive effects have also been detected at 1550 nm. Our experiments support the conclusion that the photorefractivity does not have a distinct red boundary. We show that the maximum saturated refractive index change in the infrared is of the same order of magnitude as in the visible light.

optical resonator↗
NASA NTRS2014

Early On-Orbit Performance of the Visible Infrared Imaging Radiometer Suite Onboard the Suomi National Polar-Orbiting Partnership (S-NPP) Satellite

The Visible Infrared Imaging Radiometer Suite (VIIRS) is one of the key environmental remote-sensing instruments onboard the Suomi National Polar-Orbiting Partnership spacecraft, which was successfully launched on October 28, 2011 from the Vandenberg Air Force Base, California. Following a series of spacecraft and sensor activation operations, the VIIRS nadir door was opened on November 21, 2011. The first VIIRS image acquired signifies a new generation of operational moderate resolution-imaging capabilities following the legacy of the advanced very high-resolution radiometer series on NOAA satellites and Terra and Aqua Moderate-Resolution Imaging Spectroradiometer for NASA's Earth Observing system. VIIRS provides significant enhancements to the operational environmental monitoring and numerical weather forecasting, with 22 imaging and radiometric bands covering wavelengths from 0.41 to 12.5 microns, providing the sensor data records for 23 environmental data records including aerosol, cloud properties, fire, albedo, snow and ice, vegetation, sea surface temperature, ocean color, and nigh-time visible-light-related applications. Preliminary results from the on-orbit verification in the postlaunch check-out and intensive calibration and validation have shown that VIIRS is performing well and producing high-quality images. This paper provides an overview of the onorbit performance of VIIRS, the calibration/validation (cal/val) activities and methodologies used. It presents an assessment of the sensor initial on-orbit calibration and performance based on the efforts from the VIIRS-SDR team. Known anomalies, issues, and future calibration efforts, including the long-term monitoring, and intercalibration are also discussed.

viirs↗
NASA NTRS2013

Calibration of the Mid-Infrared Tully-Fisher Relation

Distance measures on a coherent scale around the sky are required to address the outstanding cosmological problemsof the Hubble constant and of departures from the mean cosmic flow. The correlation between galaxy luminositiesand rotation rates can be used to determine the distances to many thousands of galaxies in a wide range ofenvironments potentially out to 200 Mpc. Mid-infrared (3.6m) photometry with the Spitzer Space Telescope isparticularly valuable as a source of luminosities because it provides products of uniform quality across the sky.From a perch above the atmosphere, essentially the total magnitude of targets can be registered in exposures ofa few minutes. Extinction is minimal and the flux is dominated by the light from old stars, which is expected tocorrelate with the mass of the targets.In spite of the superior photometry, the correlation between mid-infrared luminosities and rotation rates extractedfrom neutral hydrogen profiles is slightly degraded from the correlation found with I-band luminosities. A colorcorrection recovers a correlation that provides comparable accuracy to that available at the I band (20 1in an individual distance) while retaining the advantages identified above. Without color correction, the relationbetween linewidth and [3.6] magnitudes is Mb,i,k,a [3.6] 20.34 9.74(logWimx 2.5). This description is foundwith a sample of 213 galaxies in 13 clusters that define the slope and 26 galaxies with Cepheid or tip of the red giant branch distances that define the zero point. A color-corrected parameter MC[3.6] is constructed that has reduced scatter: MC[3.6] 20.34 9.13(logWimx 2.5). Consideration of the seven calibration clusters beyond 50 Mpc, outside the domain of obvious peculiar velocities, provides a preliminary Hubble constant estimate of H0 74 4 km s1 Mpc1.

Mid-Infrared↗
NASA NTRS2018

An Overall Assessment of JPSS-2 VIIRS Radiometric Performance Based on Pre-Launch Testing

The Visible Infrared Imaging Radiometer Suite (VIIRS) on-board the second Joint Polar Satellite System (JPSS) completed its sensor level testing in February 2018. The JPSS-2 (J2) mission is scheduled to launch in 2022 and will be very similar to its two predecessor missions, the Suomi National Polar-orbiting Partnership (SNPP) mission, launched on 28 October 2011 and JPSS-1 (renamed NOAA-20) launched on 18 November 2017. VIIRS instrument has 22 spectral bands covering the spectrum between 0.4 and 12.6 μm: 14 reflective solar bands (RSB), 7 thermal emissive bands (TEB) and one day-night band (DNB). It is a cross-track scanning radiometer capable of providing global measurements through observations at two spatial resolutions, 375 m and 750 m at nadir for the imaging bands and moderate bands, respectively. This paper will provide an overview of J2 VIIRS characterization methodologies and calibration performance during the pre-launch testing phases performed by the National Aeronautics and Space Administration (NASA) VIIRS Characterization Support Team (VCST) to evaluate the at-launch baseline radiometric performance and generate the parameters needed to populate the sensor data record (SDR) Look-Up-Tables (LUTs). Our analysis results confirmed the good performance of J2 VIIRS, in general as good as previous VIIRS instruments and all non-compliances are expected to have low impact on data quality. Key sensor performance metrics include the signal to noise ratio (SNR), radiance dynamic range, reflective and emissive bands calibration performance, polarization sensitivity, spectral performance, response versus scan-angle (RVS) and scattered light response. A set of performance metrics generated during the pre-launch testing program will be compared to both the SNPP and JPSS-1 VIIRS sensors.

Oudrari, Hassan↗
DOE OSTI2026

Development of electron source feedback for enhanced X-ray beam stability at NSLS-II

Future synchrotron light sources are being designed to deliver significantly higher brightness and coherence, enabling faster scanning and more advanced imaging techniques. However, realizing these capabilities requires improved X-ray beam stability, as vibrations directly limit measurement accuracy and image quality. At the NSLS-II Hard X-ray Nanoprobe (HXN), a local mechanical feedback system mitigates low-frequency motion but provides only limited suppression of dominant vibrations at 27 Hz and 120 Hz. To address this limitation, this work explores the use of the electron beam itself as the actuator for feedback by integrating X-ray beam position monitor signals into the fast orbit feedback system through a dedicated electrometer. Experimental results show that this approach effectively suppresses the dominant vibration peaks and enhances stability at the focusing point. Benchmark ptychography measurements further confirm that electron-beam-based feedback reduces background fluctuations and mitigates vibration-induced artifacts under fast-scanning conditions. These results establish the feasibility of using the electron beam as a feedback actuator for next-generation synchrotron applications and provide an experimental assessment of its potential and limitations.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Overall Performance Losses and Activated Mechanisms in Double Glass and Glass-backsheet Photovoltaic Modules with Monofacial and Bifacial PERC Cells, under Accelerated Exposures

Commercial PV modules have various packaging choices nowadays, which influence their long-term reliability. This study compared the degradation behaviors of sixteen module variants from two brands with varying encapsulant materials (EVA or POE), encapsulant types, module architectures (GB or DG), and cell types (monofacial or bifacial) using null hypothesis testing to determine statistical significant findings. The modules were exposed for 2,520 hours under two accelerated exposures: modified damp heat (mDH) and modified damp heat with full-spectrum light (mDH+FSL). For both brands, two DG module variants with UV-Cutoff rear encapsulant are found to have significantly lower average power loss than the module variants of EVA+GB with opaque rear encapsulant after each accelerated exposure. Metallization interconnect corrosion is identified as the primary degradation mechanism. Furthermore, unsupervised hierarchical clustering finds that the degradation behaviors of modules from one brand with a more strict manufacturing quality control depends on module architectures only.

14 SOLAR ENERGY↗
DOE OSTI2021

Tunable exciton-polaritons emerging from WS 2 monolayer excitons in a photonic lattice at room temperature

Engineering non-linear hybrid light-matter states in tailored lattices is a central research strategy for the simulation of complex Hamiltonians. Excitons in atomically thin crystals are an ideal active medium for such purposes, since they couple strongly with light and bear the potential to harness giant non-linearities and interactions while presenting a simple sample-processing and room temperature operability. We demonstrate lattice polaritons, based on an open, high-quality optical cavity, with an imprinted photonic lattice strongly coupled to excitons in a WS 2 monolayer. We experimentally observe the emergence of the canonical band-structure of particles in a one-dimensional lattice at room temperature, and demonstrate frequency reconfigurability over a spectral window exceeding 85 meV, as well as the systematic variation of the nearest-neighbour coupling, reflected by a tunability in the bandwidth of the p-band polaritons by 7 meV. The technology presented in this work is a critical demonstration towards reconfigurable photonic emulators operated with non-linear photonic fluids, offering a simple experimental implementation and working at ambient conditions.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Bulk Fermi surfaces of the Dirac type-II semimetallic candidate NiTe 2

Here, we present a study on the Fermi surface of the Dirac type-II semimetallic candidate NiTe 2 via the temperature and angular dependence of the de Haas–van Alphen (dHvA) effect measured in single crystals grown through Te flux. In contrast to its isostructural compounds like PtSe 2 , band-structure calculations predict NiTe 2 to display a tilted Dirac node very close to its Fermi level that is located along the Γ to A high-symmetry direction within its first Brillouin zone. The angular dependence of the dHvA frequencies is found to be in agreement with the first-principles calculations when the electronic bands are slightly shifted with respect to the Fermi level (ε F ), and therefore provide support for the existence of a Dirac type-II node in NiTe 2 . Nevertheless, we observed mild disagreements between experimental observations and density functional theory (DFT) calculations as, for example, nearly isotropic and light experimental effective masses. This indicates that the dispersion of the bands is not well captured by DFT. Despite the coexistence of Dirac-like fermions with topologically trivial carriers, samples of the highest quality display an anomalous and large either linear or sublinear magnetoresistivity. Finally, this suggests that Lorentz invariance breaking Dirac-like quasiparticles dominate the carrier transport in this compound.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗