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At least 703 records · Page 39

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DOE OSTI2022

Diffraction and thermal effect of a Bessel-Gaussian laser for Ag nanoparticle deposition

Nanoparticles are known to sinter at much lower temperatures than the corresponding bulk or micro size particles. A laser-assisted sintering process is considered in this study to sinter Ag nanoparticles by dispensing Ag paste onto an indium tin oxide-coated Si substrate. The Gaussian beam of a CO 2 laser source is propagated through axicon and biconvex lenses, and the resulting hollow beam is focused on the Ag paste with a hollow parabolic mirror. A Bessel-Gaussian irradiance distribution is obtained at the focal plane of the parabolic mirror due to the interference of the hollow laser cone. The Fresnel diffraction approximation is considered to determine the phasor of the laser and an analytical approach is implemented to calculate the irradiance distribution of the Bessel-Gaussian beam. This irradiance distribution is utilized as a heat source in a heat conduction model and the temperature distribution is analyzed for thin Ag films formed during the laser sintering of Ag nanoparticles. An analytical expression is obtained for the temperature distribution by solving the heat conduction equation using Fourier transform for finite media. The widths of the deposited Ag lines are predicted from the temperature profiles and the model predictions compare well with the experimental results. The isotherms are found to be geometrically noncongruent with convex and concave tips depending on the locally maximum and minimum irradiances of the Bessel-Gaussian beam, respectively. The convex and concave tips, however, appear in the same isotherm for sufficiently high substrate speed relative to the laser beam.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

DOE OSTI2025

SPRUCE Measurements of Fine Root Production and Chemistry from Root Ingrowth Cores, Marcell Experimental Forest, Minnesota, 2022-2023

This dataset contains fine root production and tissue chemistry measurements from root ingrowth cores. Ingrowth cores were deployed in peat from June 28, 2022 to June 24, 2023 (2022-06-28 to 2023-06-24) inside SPRUCE Experiment plots at the Marcell Experimental Forest in northern Minnesota. The warming and elevated carbon dioxide (CO2) treatments in this dataset include +0 degrees Celsius (C) (+0 and +500 parts per million (ppm) elevated CO2), +4.5 degrees C (+0 and +500 ppm elevated CO2) and +9 degrees C (+0 and +500 ppm elevated CO2) for both hummocks and hollows, as well as +2.25 degrees C (+0 and +500 ppm) and +6.75 degrees C (+0 and +500 ppm) for hollows from minimum 10 cm depth from the peat surface. Measurements include root average diameter, root length, root biomass, and root tissue nitrogen (%N and δ15N) and carbon (%C and δ13C) concentration per plant functional type and microtopographical feature. Root length and biomass are standardized to 10 cm depth. These data were used to assess the warming and elevated CO2 response of fine roots across different peatland microtopographical features (hummocks and hollows) and plant functional types (shrub, spruce and larch). This dataset contains one data file in comma separate (.csv) format. Additional metadata are provided: one data dictionary and a file-level metadata file in comma separate (.csv) format and a user guide in PDF (*.pdf) format.

ESS-DIVE CSV File Formatting Guidelines Reporting ↗

DOE OSTI2022

Pilot Test of a Nanoporous, Super-hydrophobic Membrane Contactor Process for Post-combustion CO 2 Capture

GTI Energy and Air Liquide Advanced Separations (ALaS) have been developing a novel hollow fiber membrane contactor (HFMC) technology for post-combustion CO 2 capture. The process combines advantageous features of both absorption and membrane-based separation processes to separate CO 2 from flue gas cost-effectively. The key component of the HFMC technology is the super-hydrophobic, porous hollow fiber, which is made from polyether ether ketone (PEEK). Compared to conventional absorption/desorption technologies, the critical advantage of the HFMC process is the high contact surface area provided by the hollow fibers enabling an increased volumetric mass-transfer rate. In the PEEK HFMC process, the specific surface area has been increased by an order of magnitude over structurally packed or trayed columns, resulting in compact systems with small footprints.

20 FOSSIL-FUELED POWER PLANTS↗

NASA NTRS1971

A survey of Kaufman thruster cathodes

A survey is presented of the various cathodes which were developed and used in the Kaufman ion thruster. The electron bombardment type ion source is briefly described. The general design, operating characteristics, and power requirements are shown for each type of cathode from the refractory metals used in 1960 to the plasma discharge hollow cathodes of today. A detailed discussion of the hollow cathode is given, including starting and cyclic operating characteristics as well as more fundamental design parameters. Tests to date show that the plasma hollow cathode is an efficient electron source with demonstrated durability over 10,000 hours.

Weigand, A. J.↗

NASA NTRS1971

A survey of Kaufman thruster cathodes.

A survey is presented of various cathodes which have been developed and used in the Kaufman ion thruster. The electron-bombardment type ion source used in the thruster is briefly described. The general design, operating characteristics, and power requirements are shown for each type of cathode from the refractory metals used in 1960 to the plasma discharge hollow cathodes of today. A detailed discussion of the hollow cathode is given describing starting and cyclic operating characteristics as well as more fundamental design parameters. Tests to date show that the plasma hollow cathode is an efficient electron source with demonstrated durability over 10,000 hours and should offer further performance and life improvements.

Weigand, A. J.↗

NASA NTRS1973

Effects of material composition on the ablation performance of low density elastomeric ablators

The ablation performance of materials composed of various concentrations of nylon, hollow silica spheres, hollow phenolic spheres, and four elastomeric resins was determined. Both blunt-body and flat-panel specimens were used, the cold-wall heating-rate ranges being 0.11 to 0.8 MW/sq m, respectively. The corresponding surface pressure ranges for these tests were 0.017 to 0.037 atmosphere and 0.004 to 0.005 atmosphere. Some of the results show that (1) the addition of nylon significantly improved the ablation performance, but the nylon was not compatible with one resin system; (2) panel and blunt-body specimen data do not show the same effect of phenolic sphere content on ablation effectiveness; and (3) there appears to be an optimum concentration of hollow silica spheres for good ablation performance. The composition of an efficient, nonproprietary ablator for lifting body application is identified and the ablation performance of this ablator is compared with the performance of three commercially available materials.

Tompkins, S. S.↗

NASA NTRS1974

Endurance testing of downstream cathodes on a low-power MPD thruster

A low-power MPD thruster with downstream cathode was tested for endurance with a series of hollow cathode designs. Failure modes and failure mechanisms were identified. A new hollow cathode (with rod inserts) has emerged which shows promise for long life. The downstream positioning of the cathode was also changed from an on-axis location to an off-axis location. Data are presented for a 1332-hour life test of this new hollow cathode located at the new off-axis location. Xenon propellant was used.

Burkhart, J. A.↗

NASA NTRS1973

Crystallization of plagioclase in mare basalts

A detailed study has been made of the morphology, zoning and major- and minor-element chemistry of plagioclase in mare basalt 12021 and for comparison, in several other mare basalts. Two types of plagioclase can be distinguished based on growth rate as expressed by the formation of hollow as opposed to lath-shaped crystals. The liquidus plagioclase is the most sodic part of the hollow crystals and is more sodic than the lath-shaped crystals. Hollow grains show oscillatory zoning, whereas the lath-shaped grains show normal zoning. The ratios FeO/(FeO + MgO) and K2O/(K2O + Na2O) increased in both types of plagioclase as they grew, and these ratios can be used as a guide to the crystallization history of the plagioclase. The FeO/(FeO + MgO) ratios are similar to those of coprecipitating pyroxene. The data presented here suggest the onset of plagioclase nucleation is primarily controlled by magma composition, and the point at which the magma becomes supersaturated with plagioclase.

Crawford, M. L.↗

NASA NTRS1975

Application of experimental stress analysis techniques to speed ball bearings

The object of the project was to determine experimentally the stress distribution in cylindrically hollow and spherically hollow balls. Ball models several times actual bearing ball size were fabricated. Strain gage rosettes will be mounted on the outside and inside surfaces of the models at specific locations and orientations. The models were subjected to a range of static loads simulating actual ball-race contact loads experienced in high-speed bearings operating at DN values from 2 to 4 million. The strain gages were read, and the principal strains determined for each load setting. Principal stresses were calculated and dimensionless stress coefficients determined to permit the evaluation of stresses in hollow balls of any size and load of geometrically similar configuration.

Nypan, L. J.↗

NASA NTRS1977

Inert gas thrusters

Inert gases, particularly argon and xenon, are of interest as possible alternatives to the usual electric thruster propellants of mercury and cesium. Hollow cathode data were obtained for a wide range of operating conditions. Some test conditions gave plasma coupling voltages at or below the sputtering threshold, hence should permit long operating lifetimes. All observations of hollow cathode operation were consistent with a single theory of operation, in which a significant amount of the total electron emission is from localized areas within the orifice. This mode of emission is also supported by scanning electron microscope photographs that indicate local temperatures at or near the melting temperature of the tungsten tip. Experimental hollow cathode performance was correlated for two orifice diameters, three inert gas propellants, and a range of flow rates for each propellant. The basic theory for the production of doubly ionized argon and xenon was completed. Experimental measurements of the doubly ionized fraction agree with theory within about plus or minus 20 percent. High voltage isolators were studied for the propellant feed line. The breakdown voltage per segment ranged from 300 to over 500 V with argon.

Kaufman, H. R.↗

NASA NTRS1978

Rotary leveling base platform

A leveling apparatus for the precise adjustment of a scientific instrument is reported. A base member is provided having a hollow cylindrical shape. A table for supporting the instrument rests on the base and has a shaft portion extending below the table. The upper portion of the shaft fits tightly into the hollow portion of the base member whereas the lower portion of the shaft is machined to fit loosely. The lower portion of the shaft is provided with a groove. Adjusting screws are threaded through the hollow cylindrical portion and are adapted to enter the groove. By adjusting the screws, the lower portion of the shaft is moved in a vertical plane since the shaft is loosely fitted into the cylinder. The upper portion of the shaft which is tightly fitted into the upper end of the cylinder causes the cylinder to deform slightly providing a fulcrum point which allows the table to be leveled in response to the adjustment of the adjusting screws.

Delaplaine, R. W.↗

NASA NTRS1980

Ion and advanced electric thruster research

A phenomenological model of the orificed, hollow cathode based on the field enhanced, thermionic mechanism of electron emission is presented. High frequency oscillations associated with the orificed, hollow cathode are shown to be a consequence of current flow through the cathode orifice. A procedure for Langmuir probing of the hollow cathode discharge and analyzing the resulting probe characteristics is discussed. The results of sputter yield measurements made for molybdenum, tantalum, type 304 stainless steel and copper surfaces being bombarded by low energy argon or mercury ions are also given. The effects of nitrogen and alternated copper layers on the sputter yields of molybdenum, tantalum and 304 stainless steel are also discussed. A dynamic model of electrothermal rocket and ramjet thrusters is developed. The gross performance of these devices is compared to that of an electromagnetic gun for the case of a high acceleration, Earth launch mission. The theoretical performance of electrothermal rockets and ramjets is shown to be comparable to that of the electromagnetic gun.

Wilbur, P. J.↗

NASA NTRS1981

Energy efficient engine. Volume 2. Appendix A: Component development and integration program

The large size and the requirement for precise lightening cavities in a considerable portion of the titanium fan blades necessitated the development of a new manufacturing method. The approach which was selected for development incorporated several technologies including HIP diffusion bonding of titanium sheet laminates containing removable cores and isothermal forging of the blade form. The technology bases established in HIP/DB for composite blades and in isothermal forging for fan blades were applicable for development of the manufacturing process. The process techniques and parameters for producing and inspecting the cored diffusion bonded titanium laminate blade preform were established. The method was demonstrated with the production of twelve hollow simulated blade shapes for evaluation. Evaluations of the critical experiments conducted to establish procedures to produce hollow structures by a laminate/core/diffusion bonding approach are included. In addition the transfer of this technology to produce a hollow fan blade is discussed.

Moracz, D. J.↗

NASA NTRS1986

Increasing the Deposition Rate of Silicon

Modified Siemens reactor enables chemical vapor deposition (CVD) of silicon to occur simultaneously on inner and outer surfaces of hollow cylinder, resulting in increase in mass of silicon deposited per unit time. Outer reactor for silicon deposition made from quartz or stainless steel. Hollow cylinder either single resistance-heated hollow cylinder about 5 to 10 cm or greater in diameter or 1-cm-diameter rods aligned in circular channels at top and bottom, initial circles being 5 to 10 cm in diameter or greater.

Lutwack, R.↗

NASA NTRS1986

Plasma contactors for electrodynamic tether

The role plasma contactors play in effective electrodynamic tether operation is discussed. Hollow cathodes and hollow cathode-based plasma sources have been identified as leading candidates for the electrodynamic tether plasma contactor. Present experimental efforts to evaluate the suitability of these devices as plasma contactors, conducted concurrently at NASA Lewis Research Center and Colorado State University, are reviewed. These research programs include the definition of preliminary plasma contactor designs, and the characterization of their operation both as electron emitters and electron collectors to and from a simulated space plasma. Results indicate that ampere-level electron currents, sufficient for electrodynamic tether operation, can be exchanged between hollow cathode-based plasma contactors and a dilute plasma.

Patterson, Michael J.↗

NASA NTRS1988

Advanced electric propulsion research

Results are presented which show that hollow cathodes can be operated on ammonia but that sustained operation in the high pressures where arcjet thrusters operate (of the order of 1000 Torr) is difficult to achieve. The concept of using contoured, fine wire meshes attached across the screen grid apertures in an ion thruster to effect control of the ion beam divergence is introduced. The concept is compared to conventional (free sheath) ion extraction and is shown to be potentially attractive. The performance related effects of changing the anode and cathode locations and of interchanging hollow cathode and refractory filament electron sources within an 8-cm diameter, argon, ring cusp ion thruster discharge chamber are examined. The effects induced in discharge chamber performance by changes in magnetic field strength and configuration and in propellant flow distribution are also measured. Results are presented in terms of changes in the parameters that describe the effectiveness of primary electron utilization and ion extraction into the beam. The apparatus and instrumentation used to study hollow cathode operation at high electron emission levels (of the order of 100 A) is described.

Wilbur, Paul J.↗

NASA NTRS1988

Personnel occupied woven envelope robot

The Personnel Occupied Woven Envelope Robot (POWER) provides an alternative to extravehicular activity (EVA) of space suited astronauts and/or use of long slender manipulator arms such as are used in the Shuttle Remote Manipulator System. POWER provides the capability for a shirt sleeved astronaut to perform such work by entering a control pod through air locks at both ends of an inflated flexible bellows (access tunnel). The exoskeleton of the tunnel is a series of six degrees of freedom (Six-DOF) articulated links compressible to 1/6 of their fully extended length. The operator can maneuver the control pod to almost any location within about 50 m of the base attachment to the space station. POWER can be envisioned as a series of hollow Six-DOF manipulator segments or arms wherein each arm grasps the shoulder of the next arm. Inside the hollow arms ia a bellow-type access tunnel. The control pod is the fist of the series of linked hollow arms. The fingers of the fist are conventional manipulator arms under direct visual control of the nearby operator in the pod. The applications and progress to date of the POWER system is given.

Wessling, Francis↗

NASA NTRS1958

Boundary-Layer Transition on an Open-Nose Cone at Mach 3.1

Comparison of transition locations for an open-nose cone, a conventional sharp cone, and a hollow cylinder showed that transition locations on the open-nose cone and the hollow cylinder were identical but differed greatly from those on the sharp cone. This is believed to be caused by the essentially two-dimensional character of leading edge of the open-nose cone. Bluntness effects on the open-nose cone observed on the hollow cylinder. Transition 2.2 times the sharp-cone transition distance by blunting the tip.

Brinich, Paul F↗