Mesoscale Modeling of Fiber-Reinforced Composites for Marine Energy Environments
Presentation on experimentation, idealized modeling and image-based modeling of composites subject to moisture uptake.
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Presentation on experimentation, idealized modeling and image-based modeling of composites subject to moisture uptake.
Final technical report summarizing the progress of membrane development for dye desalination
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Strain gage is installed during molding of composite and utilizes the adhesive properties of the matrix resin in the composite to bond the strain gage in place. Gages thus embedded provide data at all temperatures that the matrix can withstand.
Advanced composite standards, representing potential variations occurring when composites are processed into finished structures, were designed, fabricated and tested. Testing methods utilized were ultrasonic C-scan, radiography, and infrared.
Demonstration of high-structural-performance ARDEFORM cryoformed 301 stainless-steel glass-fiber-reinforced (GFR) vessels by room temperature tests of 13 1/2-in. diam spheres. Tests verified that the structural performance of ARDEFORM spherical GFR vessels not only exceeded that of all metal construction, but also bettered previous GFR experimental results by 50%. Achievement of essentially the full strength of fiberglass in a spherical wrap pattern was again verified. Significant weight advantages for this construction are projected for O2/N2 high-pressure gas tanks for Space Shuttle environmental control/life support system missions.
An engineering approach is proposed for predicting unnotched/notched laminate fatigue behavior from basic lamina fatigue data. The fatigue analysis procedure was used to determine the laminate property (strength/stiffness) degradation as a function of fatigue cycles in uniaxial tension and in plane shear. These properties were then introduced into the failure model for a notched laminate to obtain damage growth, residual strength, and failure mode. The approach is thus essentially a combination of the cumulative damage accumulation (akin to the Miner-Palmgren hypothesis and its derivatives) and the damage growth rate (similar to the fracture mechanics approach) philosophies. An analysis/experiment correlation appears to confirm the basic postulates of material wearout and the predictability of laminate fatigue properties from lamina fatigue data.
An investigation of delamination crack growth in a unidirectional composite laminate under static and fatigue loading conditions is presented. An experimental program was conducted to study failure mechanisms and characterize the crack growth rate; analytical modeling based on microscopic observations was carried out using an advanced singular finite element method of the hybrid-stress model. Using a mixed-mode failure criterion, the delamination growth under a monotonically increasing load can be predicted; the rate of delamination crack propagation under fatigue loading is directly related to the amplitudes of cyclic opening and shearing mode stress intensity factors by a power law relationship.
The acousto-ultrasonic technique combines advantageous aspects of acoustic emission and ultrasonic methodologies. Acousto-ultrasonics operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is complex, but it can be quantitized in terms of a 'stress wave factor.' The stress wave factor, which can be defined in a number of ways, is a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect appears in the stress wave factor.
The acousto-ultrasonic technique combines advantageous aspects of acoustic emission and ultrasonic methodologies. Acousto-ultrasonics operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is quite complex, but it can be quantitized in terms of a 'stress wave factor'. The stress wave factor, which can be defined in a number of ways, is essentially a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect will appear in the stress wave factor.
Annealing at temperatures below the glass transition temperature (sub-T/g/ annealing) in structural epoxy network glasses is found to affect long-term mechanical properties of symmetrically (+ or - 45 deg) reinforced 16-lamina graphite/epoxy composites. Post-cured specimens of Thornel 300 graphite/Narmco 5208 epoxy are sub-T(g) annealed at 140 C for about 10, 100, 1000, 10,000, and 100,000 min with a prior quenching above T(g). The ultimate tensile strength, strain-to-break, and static toughness of the composite materials are found to decrease as a function of sub-T(g) annealing time, while no weight loss is observed. Time-dependent changes in properties are explained by a physical aging concept based on free-volume decreases in the nonequilibrium glassy state of network epoxies, and results imply that changes in composite properties may occur with the service time.
Presented is a theory to predict the room-temperature shape of unsymmetric laminates. The theory is an extension of classical lamination theory and includes the effects of geometric nonlinearities. It is shown that the saddle shape predicted by the classical theory can actually be an unstable shape and a laminate will assume a cylindrical shape instead. The phenomena is coupled to the length, width, and thickness of the laminate.
The advantageous aspects of acoustic emission and ultrasonic methodologies are combined in a technique which operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is quite complex, but it can be quantitized in terms of a "stress wave factor". The stress wave factor, which can be defined in a number of ways, is essentially a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect will appear in the stress wave factor.
Graphite/epoxy (T300/5208) and graphite/polyimide composites (C6000/PMR 15) were exposed to various levels of 0.5 MeV electron radiation with the maximum dose being 10,000 Mrad. A three point bending test was used to evaluate the ultimate stress and modulus of the composites. In all composites except transverse samples of C6000/PMR 15 ultimate stress values remained approximately constant or increased slightly. The modulus values remained approximately constant for all composite types regardless of the radiation level. Interfacial aspects of composites were studied. Interlaminar shear tests were performed on T300/5208 and C6000/PMR 15 composites irradiated to 10,000 Mrad. There was an initial increase in interlaminar shear strength (up to 1,000 Mrad) followed by a sharp decrease with further radiation exposure. Using scanning electron microscopy no visual differences in the mode of fracture could be detected between ruptured control samples and those exposed to various levels of radiation. Electron spectroscopy for chemical analysis (ESCA) revealed little change in the surface elements present in control and highly irradiated T300/5208 composite samples.
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The objective of this project was to develop a user-friendly interactive computer program to be used as an analytical tool by structural designers. Its intent was to do preliminary, approximate stress analysis to help select or verify sizing choices for composite structural members. The approach to the project was to provide a subroutine which uses classical lamination theory to predict an effective elastic modulus for a laminate of arbitrary material and ply orientation. This effective elastic modulus can then be used in a family of other subroutines which employ the familiar basic structural analysis methods for isotropic materials. This method is simple and convenient to use but only approximate, as is appropriate for a preliminary design tool which will be subsequently verified by more sophisticated analysis. Additional subroutines have been provided to calculate laminate coefficient of thermal expansion and to calculate ply-by-ply strains within a laminate.
A technique is described that makes it possible to transmit and receive bulk ultrasonic waves launched from the same surface of a composite sheet by means of transducers mounted on variable angle blocks. A straightforward approach to measure the velocity and attenuation of this wave is presented. A bulk compressional wave of 930,000 cm/sec velocity was launched and received in this manner in an 8-ply unidirectional T-300-5208 epoxy composite. Preliminary results indicate that parameters associated with this wave might be sensitive to accumulated damage in a composite; thus, the technique has a potential for NDE in structures made from composite materials.
Report describes experimental approaches to quantification of fatigue damage in metal-matrix composites (MMC's). Discusses number of examples of development of damage and failure along with associated analytical models of behavior of MMC. Objectives of report are twofold. First, present experimental procedures and techniques for conducting meaningful fatigue tests to detect and quantify fatigue damage in MMC's. Second, present examples of how fatigue damage initiated and grows in various MMC's. Report furnishes some insight into what type of fatigue damage occurs and how damage quantified.