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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 703 records · Page 39
All sourcesNASA NTRSDOE OSTI
DOE OSTI2011

Learning to Apply Metrology Principles to the Measurement of X-ray Intensities in the 500 eV to 110 keV Energy Range

National Security Technologies, LLC (NSTec), Livermore Operations, has two optical radiation calibration laboratories accredited by “the National Voluntary Laboratories Accreditation Program (NVLAP) which is the accrediting body of” the National Institute of Standards and Technology (NIST), and is now working towards accreditation for its X-ray laboratories. NSTec operates several laboratories with X-ray sources that generate X-rays in the energy range from 50 eV to 115 keV. These X-ray sources are used to characterize and calibrate diagnostics and diagnostic components used by the various national laboratories, particularly for plasma analysis on the Lawrence Livermore National Laboratory (LLNL) National Ignition Facility (NIF). Because X-ray photon flux measurement methods that can be accredited, i.e., traceable to NIST, have not been developed for sources operating in these energy ranges, NSTec, NIST, and the National Voluntary Accreditation Program (NVLAP) together have defined a path toward the development and validation of accredited metrology methods for X-ray energies. The methodology developed for the high energy X-ray (HEX) Laboratory was NSTec’s starting point for X-ray metrology accreditation and will be the basis for the accredited processes in the other X-ray laboratories. This paper will serve as a teaching tool, by way of this example using the NSTec X-ray sources, for the process and methods used in developing an accredited traceable metrology.

07 ISOTOPE AND RADIATION SOURCES↗
DOE OSTI2016

Special Analysis for the Disposal of the Idaho National Laboratory Regulated Asbestos Waste Stream at the Area 5 Radioactive Waste Management Site, Nevada National Security Site, Nye County, Nevada

This special analysis (SA) evaluates whether the Idaho National Laboratory (INL) Regulated Asbestos waste stream is suitable for disposal by shallow land burial at the Area 5 Radioactive Waste Management Site on the Nevada National Security Site (NNSS). The INL Regulated Asbestos waste stream consists of asbestos and asbestos-contaminated debris. The INL Regulated Asbestos waste stream requires an SA to resolve whether it is acceptable to dispose of tritium ( 3 H) at activity concentrations exceeding the NNSS Waste Acceptance Criteria Action Level.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS1981

Analysis and simulation of a magnetic bearing suspension system for a laboratory model annular momentum control device

A linear analysis and the results of a nonlinear simulation of a magnetic bearing suspension system which uses permanent magnet flux biasing are presented. The magnetic bearing suspension is part of a 4068 N-m-s (3000 lb-ft-sec) laboratory model annular momentum control device (AMCD). The simulation includes rigid body rim dynamics, linear and nonlinear axial actuators, linear radial actuators, axial and radial rim warp, and power supply and power driver current limits.

Groom, N. J.↗
DOE OSTI2016

Special Analysis for the Disposal of the Idaho National Laboratory Contact Handled Sealed Sources Waste Stream at the Area 5 Radioactive Waste Management Site, Nevada National Security Site, Nye County, Nevada

This special analysis (SA) evaluates whether the Idaho National Laboratory (INL) Contact Handled Sealed Sources waste stream is suitable for disposal by shallow land burial at the Area 5 Radioactive Waste Management Site (RWMS) on the Nevada National Security Site (NNSS). The INL Contact Handled Sealed Sources waste stream consists of sealed radioactive sources. The INL Contact Handled Sealed Sources waste stream requires an SA to determine whether the Area 5 RWMS can accept radium-226 ( 226 Ra), tritium ( 3 H), and europium-152 ( 152 Eu) at activity concentrations exceeding the NNSS Waste Acceptance Criteria Action Levels and whether to accept four long-lived radionuclides (curium-247 [ 247 Cm], 250 Cm, californium-249 [ 249 Cf], 251 Cf) without action levels.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2014

Study of boron detection limit using the in-air PIGE set-up at LAMFI-USP

The quantification of small amounts of boron in materials is of extreme importance in different areas of materials science. Boron is an important contaminant and also a silicon dopant in the semiconductor industry. Boron is also extensively used in nuclear power plants, either for neutron shielding or for safety control and boron is an essential nutrient for life, either vegetable or animal. The production of silicon solar cells, by refining metallurgical-grade silicon (MG-Si) requires the control and reduction of several silicon contaminants to very low concentration levels. Boron is one of the contaminants of solar-grade silicon (SG-Si) that must be controlled and quantified at sub-ppm levels. In the metallurgical purification, boron quantification is usually made by Inductive Coupled Plasma Mass Spectrometry, (ICP-MS) but the results need to be verified by an independent analytical method. In this work we present the results of the analysis of silicon samples by Particle Induced Gamma-Ray Emission (PIGE) aiming the quantification of low concentrations of boron. PIGE analysis was carried out using the in-air external beam line of the Laboratory for Materials Analysis with Ion Beams (LAMFI-USP) by the {sup 10}B(p,αγ({sup 7}Be nuclear reaction, and measuring the 429 keV γ-ray. The in-air PIGE measurements at LAMFI have a quantification limit of the order of 10{sup 16} at/cm{sup 2}.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1971

Lessons learned from a decade of international space cooperation.

A case history of the Alouette/ISIS series is presented, giving attention to aspects of U.S.-Canadian cooperation in this program. The project is only one example of a broad network of international cooperative relationships established by NASA over the past decade. Participation by other countries in important space science and applications projects is not limited to those providing flight hardware or conducting flight observations. Much valuable work is done on the ground, ranging from analysis in the laboratories of samples returned from the moon to correlated ground-based reception and analysis of radio beacon signals from satellites. It was found that cooperation is more likely to proceed smoothly and produce beneficial results if it is focused on projects that are clearly defined and agreed on in advance.

Barnes, R. J. H.↗
DOE OSTI2022

Caution on Using Tetrahydrofuran for Processing Crystalline Silica Samples From Engineered Stone for XRD Analysis

Abstract We conducted laboratory experiments to investigate a suspected effect of tetrahydrofuran (THF) on quantifying crystalline silica in samples collected from working with engineered stone when THF is used to process samples prior to the X-ray diffraction (XRD) analysis. Two groups of samples from grinding either engineered stone or granite were simultaneously taken from a laboratory testing system, with one group of samples using THF for processing and another group using muffle furnace for ashing. For each stone type, we also tested four levels of respirable dust loading on the samples by varying the grinding time from 1 to 8 min. Statistical analysis of the experimental results on crystalline silica contents of the two groups of samples showed that the difference between the two methods was not significant (P ≥ 0.05) for the granite at all four levels of respirable dust loading and for the engineered stone at the two levels of respirable dust loading greater than 0.5 mg. However, the crystalline silica content from using THF processing was significantly lower (P = 0.001) than that from using muffle furnace ashing for engineered stone when the respirable dust loading levels were less than 0.5 mg. For the engineered stone dust samples with grinding times of 1 and 2 min, the average respirable dust loading was about 0.19 and 0.34 mg, respectively; while the crystalline silica content from using THF processing was 30.9 and 21.5% lower than that from using muffle furnace ashing, respectively. Since most full-shift samples from field assessments in this industry are expected to have respirable dust loading less than 0.5 mg, muffle furnace or radio frequency plasma ashing should be specified as the preferred sample processing method instead of the THF processing method for quantification of crystalline silica when engineered stone is expected to present to avoid artificially reduced silica content values, which are likely caused by the reactions between THF and the resins in engineered stone.

Public, Environmental & Occupational Health↗
DOE OSTI2017

Quantitative Digital Autoradiography for Environmental Swipe Sample Prioritization: System design, Characterization, and Initial Measurements

Environmental sampling and sample analyses by the International Atomic Energy Agency’s (IAEA) Network of Analytical Laboratories (NWAL) is a critical technical tool used to detect facility misuse under a Comprehensive Safeguards Agreement and to verify the absence of undeclared nuclear material activities under an Additional Protocol. Currently all environmental swipe samples (ESS) are screened using gamma spectrometry and x-ray fluorescence to estimate the amount of U and/or Pu in the ESS, to guide further analysis, and to assist in the shipment of ESS to the NWAL. Quantitative Digital Autoradiography for Environmental Samples (QDARES) is being developed to complement existing techniques through the use of a portable, real-time, high-spatial-resolution camera called the Ionizing-radiation Quantum Imaging Detector (iQID). The iQID constructs a spatial map of radionuclides within a sample or surface in real-time as charged particles (betas) and photons (gamma/x-rays) are detected and localized on an event-by-event basis. Knowledge of the location and nature of radioactive hot spots on the ESS could provide information for subsequent laboratory analysis. As a nondestructive technique, QDARES does not compromise the ESS chain of custody or subsequent laboratory analysis. In this paper we will present the system design and construction, characterization measurements with calibration sources, and initial measurements of ESS.

McDonald, Benjamin S.↗
DOE OSTI2016

Special Analysis for the Disposal of the Idaho National Laboratory Idaho Chemical Processing Plant Low-Level Waste Stream at the Area 5 Radioactive Waste Management Site, Nevada National Security Site, Nye County, Nevada

This special analysis (SA) evaluates whether the Idaho National Laboratory (INL) Idaho Chemical Processing Plant (ICPP) Low-Level waste stream is suitable for disposal by shallow land burial at the Area 5 Radioactive Waste Management Site on the Nevada National Security Site (NNSS). The INL ICPP Low-Level waste stream consists of debris and solidified liquids. The INL ICPP Low-Level waste stream requires an SA to resolve two unreviewed disposal questions (UDQs). The first UDQ addresses whether it is acceptable to dispose of radium-226 (226Ra) at an activity concentration that exceeds the NNSS Waste Acceptance Criteria (WAC) Action Level. The second UDQ evaluates the acceptability of disposing of five long-lived radionuclides without WAC action levels. Long-lived radionuclides without action levels are radionuclides not evaluated in the performance assessment.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2017

Special Analysis for the Disposal of the Idaho National Laboratory U-233 Solidified Grinding Sludge and Associated Debris Waste Stream at the Area 5 Radioactive Waste Management Site, Nevada National Security Site, Nye County, Nevada

This special analysis report evaluates whether the Idaho National Laboratory (INL) Uranium-233 (233U) Solidified Grinding Sludge and Associated Debris waste stream is suitable for shallow land burial at the Area 5 Radioactive Waste Management Site on the Nevada National Security Site. Disposal of the INL 233U Solidified Grinding Sludge waste meets all DOE M 435.1-1 performance objectives. The INL 233U Solidified Grinding Sludge waste stream is recommended for acceptance with the condition that the total 233U inventory shall not exceed 2.3E13 Bq.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2026

DEMO-FTES: Development, Monitoring, and Control of Fracture Thermal Energy Storage in Crystalline Rock Formations (CRADA Final Report)

The DEMO-FTES project investigated the feasibility of Fracture Thermal Energy Storage (FTES) as a seasonal energy storage solution in crystalline rock formations. FTES leverages hydraulically induced fractures to exchange heat between circulating fluids and the surrounding rock mass, enabling long-term thermal energy retention due to the high specific heat and low thermal conductivity of rock. This approach has the potential to reduce heating and cooling energy demands and enhance building energy resilience. The project combined dimensional analysis, numerical modeling, laboratory experiments, and meso-scale field tests to evaluate FTES performance and advance its technology readiness level from 3 to 5. Scaling analysis identified key dimensionless parameters governing heat transfer and fluid flow, ensuring laboratory and field tests were representative of larger-scale systems. Numerical simulations using TOUGH and iTOUGH2 frameworks supported experiment design and interpretation, modeling fracture geometry, thermal-hydraulic behavior, and thermo-mechanical coupling. Laboratory tests at EPFL involved creating single and multiple fractures in 25 cm cubic samples of Gabbro and Granite under true triaxial stress.

25 ENERGY STORAGE↗