Composite overwrapped metallic tanks
Tension, biaxial, and creep tests of 5Al-2.5Sn titanium alloy and computerized design for fiberglass-epoxy overwrapped titanium pressure vessel
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Tension, biaxial, and creep tests of 5Al-2.5Sn titanium alloy and computerized design for fiberglass-epoxy overwrapped titanium pressure vessel
Balloon-borne observation of X ray sources in northern sky, including Sco, Cyg and SN 1572
Sn additives effect on In thin film superconducting transmission lines, comparing with Pippard nonlocal theory for mean free path reduction
Debye-Waller factors for Nb and Sn atoms in intermetallic niobium stannide by X ray intensity measurements on single crystal
Superconducting Nb-Sn intermetallic compound synthesis from elemental powders by converging shock waves
Ti-Al-Sn and Al alloys thin sectioned specimens cryogenic fracture strength, discussing surface crack fracture behavior
Surface segregation, adhesion and friction of monocrystalline Cu-Al, Cu-Sn and Fe-Al alloys from Auger emission spectroscopy and low energy electron diffraction experiments
The effects on fracture and flaw growth of weld-induced residual stresses, combined bending and tension stresses, and stress fields adjacent to circular holes in 2219-T87 aluminum and 5AI-2.5Sn(ELI) titanium alloys were evaluated. Static fracture tests were conducted in liquid nitrogen; fatigue tests were performed in room air, liquid nitrogen, and liquid hydrogen. Evaluation of results was based on linear elastic fracture mechanics concepts and was directed to improving existing methods of estimating minimum fracture strength and fatigue lives for pressurized structure in spacecraft and booster systems. Effects of specimen design in plane-strain fracture toughness testing were investigated. Four different specimen types were tested in room air, liquid nitrogen and liquid hydrogen environments using the aluminum and titanium alloys. Interferometry and holograph were used to measure crack-opening displacements in surface-flawed plexiglass test specimens. Comparisons were made between stress intensities calculated using displacement measurements, and approximate analytical solutions.
Several alloys (Hastelloy X, AISI 347, A-286 bolts, Inconel 718, Al 7039-T63 and Ti-5Al-2.5Sn ELI) were irradiated in liquid nitrogen (140 R) to neutron fluences between 10 to the 17th power and 10 to the 19th power nvt (E greater than 1.0 Mev). After irradiation, tensile properties were obtained in liquid nitrogen without permitting any warmup except for some specimens which were annealed at 540 R. The usual trend of radiation damage typical for materials irradiated at and above room temperature was observed, such as an increase in strength and decrease in ductility. However, the damage at 140 R was greater because this temperature prevented the annealing of radiation-induced defects which occurs above 140 R.
Ten different conductive inks used in the fabrication of thick-film circuits were evaluated for their physical and handling properties. Viscosity, solid contents, and spectrographic analysis of the unfired inks were determined. Inks were screened on ceramic substrates and fired for varying times at specified temperatures. Selected substrates were given additional firings to simulate the heat exposure received if thick-film resistors were to be added to the same substrate. Data are presented covering the (1) printing characteristics, (2) solderability using Sn-63 and also a 4 percent silver solder, (3) leach resistance, (4) solder adhesion, and (5) wire bonding properties. Results obtained using different firing schedules were compared. A comparison was made between the various inks showing general results obtained for each ink. The changes in firing time or the application of a simulated resistor firing had little effect on the properties of most inks.
This paper considers the problem of irreversible dimensional changes of the order of one thousandth of an inch per inch in several candidate materials for orbiting observatories. Although there are a number of potential sources for such dimensional changes, those given major consideration here are applied stresses and residual stresses. Results of room-temperature microyield strength (MYS) and microcreep tests to detect permanent strains associated with both short- and long-duration loading are reported for several engineering materials, including four aluminum alloys (2024, 5456, 6061, and 2014), I400 beryllium, TZM molybdenum, AZ31 magnesium, two titanium alloys (Ti-6Al-4V and Ti-5Al-2.5Sn), 321 stainless steel, a graphite/epoxy composite, and low-expansion glass ceramics. The data indicate that: metallic materials have no true elastic limit; the MYS cannot be predicted reliably from, and is appreciably less than, the conventional yield strength: significant microcreep and stress relaxation can occur at stresses somewhat below the MYS.
The parameter values measured are in agreement with those reported by Mazelsky and Lubell (1963) and data of Bis and Dixon (1969). The measurements for SnTe introduce a large amount of data into a defect model analysis that shows that the ratio of the number of holes per tin-vacancy acceptor to the 77 K Hall factor is independent of the apparent hole concentration. The measurements reveal some interesting problems in handling the Sn-rich alloys in fine powder form due to the uptake of oxygen.
This experimental program was undertaken to determine the effects of combined cyclic/sustained loads, stress level, and crack shape on the fatigue crack growth rate behavior of cracks subjected to plane strain conditions. Material/environment combinations tested included: 2219-T87 aluminum plate in gaseous helium, room air, and 3.5% NaCl solution at room temperature, liquid nitrogen, and liquid hydrogen; 5Al-2.5 Sn (ELI) titanium plate in liquid nitrogen and liquid hydrogen and 6AL-4V (ELI) STA titanium plate in gaseous helium and methanol at room temperature. Most testing was accomplished using surface flawed specimens instrumented with a clip gage to continuously monitor crack opening displacements at the specimen surface. Tapered double cantilever beam specimens were also tested. Static fracture and ten hour sustained load tests were conducted to determine fracture toughness and apparent threshold stress intensity values. Cyclic tests were performed using sinusoidal loading profiles at 333 MHz (20 cpm) and trapezoidal loading profiles at both 8.3 MHz (0.5 cpm) and 3.3 MHz (0.2 cpm). Data were evaluated using modified linear elastic fracture mechanics parameters.
The Ni-Ni3Ta eutectic and a nickel-base alloy containing 30 wt pct Ta were solidified unidirectionally in an electron beam floating zone melting apparatus. It was found that the volume fraction of the Ni3Ta phase in the Ni-Ni3Ta eutectic mixture was increased from 7.6 to 36 volume pct in agreement with the theory as predicted. Tensile properties of the randomly solidified and unidirectionally solidified Ni-Ni3Ta eutectic were determined as function of solidification rate and temperature. It was found that the ultimate tensile strength decreased as both the test temperature and solidification rate increased. An elongation of 40 pct was obtained for a nickelbase alloy containing 30 wt at room temperature. This unusually large elongation was attributed to the superplastic behavior of the alloy. The critical currents versus the external fields at 2.5, 3.0, 3.5 and 4.2 deg for the unidirectionally solidified Pb-Sn eutectic were measured. The values of critical fields at zero critical currents were obtained by extrapolation.
The author has identified the following significant results. ERTS-1 prints have been used extensively in a geology of Alaska class to give a basic framework of the geology of the state. In addition, they have been intermittantly used in such diverse classes as: (1) Economic Geology (e.g. the Sn-bearing granites of the Seward Peninsula are particularly noticeable due to their wide contact metamorphic aureoles.) (2) A canned geology of Alaska lecture which has been given to two different introductory geology courses. (3) Structural Geology (e.g. the Fairweather and Denali faults are striking obvious). It was found most convenient for larger classes to prepare 35mm slides of the ERTS-1 prints that are used in conjunction with slides of the topographic and geologic maps at about the same scale. Thus the emphasis has been in integration of the ERTS-1 material into existing courses. As such, the ERTS-1 data has provided a unique and striking viewpoint that never fails to initiate favorable comment. In addition, prints have been examined by numerous researchers to develop a regional, integrated overview of such varied topics as regional geology to a background for local geologic mapping to studies of ore deposits and to the definition of a formation to be studied in detail at its type locality.
The discovery of superconductivity at 20.3 K in the Nb-Ga system by applying chemical vapor deposition (CVD) techniques to the materials preparation problem is reported. Films on ceramic substrates have been grown with superconducting onsets of up to 20.3 K. Critical fields at 4.2 K in excess of 300 kG and alpha's of 1100,000 T-A/sq cm have been obtained. The results confirm that the outstanding properties of Nb-Ga are due to an equilibrium configuration of the system, namely, the stoichiometric A-15 compound Nb3Ga, which is stable at relatively low temperatures. Practical materials preparation problems center on the codeposition of an adjacent Nb5Ga3 phase and the requirement that the deposition temperature be low. Some ternary alloys were also prepared, with part of the Ga replaced by Sn, Sb, Al, or Ge.
Irradiated and unirradiated tensile and fatigue specimens of AISI 310 stainless steel and Ti-5Al-2.5Sn were tested in the range of 100 to 10,000 cycles to failure to determine the applicability of the method of universal slopes to irradiated materials. Tensile data for both materials showed a decrease in ductility and increase in ultimate tensile strength due to irradiation. Irradiation caused a maximum change in fatigue life of only 15 to 20 percent for both materials. The method of universal slopes predicted all the fatigue data for the 310 SS (irradiated as well as unirradiated) within a life factor of 2. For the titanium alloy, 95 percent of the data was predicted within a life factor of 3.
Tensile, fracture toughness, threshold stress intensity for sustained-load crack growth, and cyclic and sustained load crack growth rate measurements were performed on a number of alloys in high-pressure hydrogen and helium environments. The results of tensile tests performed in 34.5 MN/m2 (5000 psi) hydrogen indicated that Inconel 625 was considerable embrittled at ambient temperature but was not embrittled at 144 K (-200 F). The tensile properties of AISI 321 stainless steel were slightly reduced at ambient temperature and 144 K (-200 F). The tensile properties of Ti-5Al-2.5 Sn ELI were essentially unaffected by hydrogen at 144 K (-200 F). OFHC copper was not embrittled by hydrogen at ambient temperature or at 144 K (-200 F).