Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “Particle characterization”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 685 records · Page 38
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Instrumentation development and testing of a wind turbine blade for sub-scale wake studies

Wind turbine blade aerodynamics and the resulting wake flow are complex, and wind tunnel testing of these flows can provide critical insight. The data from such tests are also valuable for validation of numerical models. For experiments using sub-scale turbines to be useful, the blade aerodynamics and wakes must exhibit the important features observed in utility-scale turbine flows. In this work, ~1 m blades designed to produce physics relevant to larger scale turbines were manufactured and affixed to an existing turbine. One of the blades was instrumented for blade surface pressure measurements. Time-dependent surface pressure measurements coupled with instantaneous measurements of the inflow with Cobra probes and the wake with particle image velocimetry allowed for characterization of the inflow, blade flow, and near wake. The results demonstrate that the instrumentation was effective in characterizing the blade loading and the flow field. For the one test case discussed in this paper, the measurements of inflow, blade loading, and wake properties facilitate understanding of the wake's behavior.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2022

A study of space charge induced non-linearity in the Single Line Of Sight camera

We report a new generation of gated x-ray detectors at the National Ignition Facility has brought faster, enhanced imaging capabilities. Their performance is currently limited by the amount of signal they can be operated with before space charge effects in their electron tube start to compromise their temporal and spatial response. We present a technique to characterize this phenomenon and apply it to a prototype of such systems, the Single Line Of Sight camera. Results of this characterization are used to benchmark Particle In Cell simulations of the electrons drifting inside the detector, which are found to well reproduce experimental data. These simulations are then employed to predict the optimum photon flux to the camera, with the goal to increase the quality of the images obtained on an experimental campaign while preventing the appearance of deleterious effects. They also offer some insight into some of the improvements that can be brought to the new pulse-dilation systems being built at Lawrence Livermore National Laboratory

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2024

The ion-gas-neutral interactions with surfaces-2 (IGNIS-2) facility for the study of plasma–material interactions

The Ion-Gas-Neutral Interactions with Surfaces-2 (IGNIS-2) surface science facility has been designed at the Pennsylvania State University with the specific purpose of enabling experiments to study plasma–material interactions. This in situ surface modification and characterization facility consists of multiple reconfigurable substations that are connected through a central transfer chamber. This fully connected vacuum system ensures that the physical and chemical properties of samples are not altered between surface modification and analysis. The modification techniques in IGNIS-2 include a low-energy (<300 eV), high-flux (up to 1016 cm−2 s−1) broad-beam ion source, a liquid metal dropper, a lithium injection system, an RF sputter source, and an evaporator. Its characterization techniques include charged particle-based techniques, such as low-energy ion scattering (enabled by two <5 keV ion sources) and x-ray photoelectron spectroscopy, and photon and light-based techniques, such as x-ray fluorescence, multi-beam optical stress sensors, and optical cameras. All of these techniques can be utilized up to mTorr pressures, allowing both in situ and in operando studies to be conducted. Results are presented on lithium wetting experiments of argon-irradiated tungsten-based composites, surface stress measurements of tungsten films during deuterium ion irradiation, and temperature-programmed desorption of deuterium-irradiated graphite to demonstrate the in situ capabilities of this new facility.

Instruments & Instrumentation↗
DOE OSTI2021

Cross-correlation analysis of X-ray photon correlation spectroscopy to extract rotational diffusion coefficients

Coefficients for translational and rotational diffusion characterize the Brownian motion of particles. Emerging X-ray photon correlation spectroscopy (XPCS) experiments probe a broad range of length scales and time scales and are well-suited for investigation of Brownian motion. While methods for estimating the translational diffusion coefficients from XPCS are well-developed, there are no algorithms for measuring the rotational diffusion coefficients based on XPCS, even though the required raw data are accessible from such experiments. In this paper, we propose angular-temporal cross-correlation analysis of XPCS data and show that this information can be used to design a numerical algorithm (Multi-Tiered Estimation for Correlation Spectroscopy [MTECS]) for predicting the rotational diffusion coefficient utilizing the cross-correlation: This approach is applicable to other wavelengths beyond this regime. We verify the accuracy of this algorithmic approach across a range of simulated data.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2019

Multicomponent mutual diffusion in the warm, dense matter regime

In this work, we present the formulation, simulations, and results for multicomponent mutual diffusion coefficients in the warm, dense matter regime. While binary mixtures have received considerable attention for mass transport, far fewer studies have addressed ternary and more complex systems. We therefore explicitly examine ternary systems utilizing the Maxwell-Stefan formulation that relates diffusion to gradients in the chemical potential. Onsager coefficients then connect the macroscopic diffusion to microscopic particle motions, evinced in trajectories characterized by positions and velocities, through various autocorrelation functions (ACFs). These trajectories are generated by molecular dynamics (MD) simulations either through the Born-Oppenheimer approximation, which treats the ions classically and the electrons quantum-mechanically by an orbital-free density-functional theory, or through a classical MD approach with Yukawa pair-potentials, whose effective ionizations and electron screening length derive from quantal considerations. We employ the reference-mean form of the ACFs and determine the center-of-mass coefficients through a simple reference-frame-dependent similarity transformation. The Onsager terms in turn determine the mutual diffusion coefficients. We examine a representative sample of ternary mixtures as a function of density and temperature from those with only light elements (D-Li-C, D-Li-Al) to those with highly asymmetric mass components (D-Li-Cu, D-Li-Ag, H-C-Ag). We also follow trends in the diffusion as a function of number concentration and evaluated the efficacy of various approximations such as the Darken approximation.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2025

Ink-sprayed transparent ceramic multilayer planar waveguides for ribbon lasers

Multilayer transparent ceramic planar waveguides were fabricated using a newly developed particle-loaded ink spraying method, characterized, and lased. Waveguides with five Yb:YAG gain regions and four Lu:YAG index-matched regions were produced for application as a “ribbon laser,” as well as a homogeneous Yb:YAG waveguide. Elemental mapping revealed that the waveguide thicknesses varied from 40 to 69 μm, comprised of layers of less than 10 µm. The Yb concentration profiles were fit to a diffusion profile. The homogeneous and multilayer waveguides were tested in a laser cavity and produced similar slope efficiencies, with a maximum of 31% achieved. In conclusion, their beam profiles provided evidence of the ribbon structure affecting the preferred mode.

Osborne, Ross [Lawrence Livermore National Laborat↗
DOE OSTI2018

FY18 J23X PSDT Final Report: Shock Initiation of PBX 9502 Lot HOL88H891-008

This report details a series of plate impact experiments on the insensitive explosive PBX 9502 (95% TATB, 5% Kel-F 800) with lot number HOL88H891-008. This is a ’virgin’ lot (no recycled material used), for which many detonation performance measurements are available; the addition of these 1-D shock initiation experiments will aid model calibration efforts for this material. Samples were machined from isostatically-pressed billets with anominal density of 1.89 g/cc. The evolution of the shock to a detonation was characterized by 9 embedded magnetic particle velocity gauges, and 116 embedded magnetic time of arrival gauges (AKA shock trackers). Pho-ton Doppler velocimetry (PDV) with a LiF window was used at the back surface of the samples to capture the wave profile exiting the sample. Six experiments were performed, covering a pressure range of 10.8–18.6 GPa and run distances to detonation of 2.7–12.2+ mm. The shock initiation of this lot is found to be consistent with Pop plots reported for other lots of PBX 9502. All data have been uploaded to the LANL Small Scale Database for use by the research community.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗
DOE OSTI2018

FY18 J23X PDZG Final Report: Double Shock Initiation of PBX 9502 Lot HOL88H891-008

Heterogeneous high explosives subjected to sub-critical shock waves are known to exhibit desensitization to later shock inputs. While it is believed that this phenomenon is due to the removal of hot spot forming features in the explosive by the initial sub-critical shock, the effect of the time delay between the shocks is poorly understood. This report details a series of double shock plate impact experiments that vary the time between similar shocks to explore the time dependance of this shock desensitization process. These experiments were performed on the insensitive explosive PBX 9502 (95% TATB, 5% Kel-F 800) with lot number HOL88H891-008. The evolution of the shocks to a detonation was characterized by 9 embedded magnetic particle velocity gauges, and 116 embedded magnetic time of arrival gauges (AKA shock trackers). Photon Doppler velocimetry (PDV) with a LiF window was used at the back surface of the samples to capture the wave profile exiting the sample. Three double shock experiments were performed, with first and second shock pressures of 8.3 GPa and 16.5 GPa, respectively. An analogous single shock experiment at 16.3 GPa was also performed. The double shock experiments exhibited small levels of reaction during the initial shock,and shock desensitization to the second shock. Run distances after shock coalescence were shorter than those expected for a single shock, indicating the shock to detonation transition (SDT) process was slightly further along due to partial reaction in the first shock wave. These data will be used to calibrate model behavior under multiple-shock conditions. Additional double shock data will be collected to further explore this area in FY2019. All data have been uploaded to the LANL Small Scale Database for use by the research community.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗
DOE OSTI2020

Examining the Ice-Nucleating Particles from the Southern Great Plains Field Campaign Report

The recent U.S. Department of Energy (DOE) Atmospheric Radiation Measurement (ARM) user facility field campaign, named Examining the Ice-Nucleating Particles from Southern Great Plains (ExINP-SGP), targeted experimentally characterizing abundance and other properties of ambient ice-nucleating particles (INPs) at the SGP site in Oklahoma (36° 36' 18" N, 97° 29' 6" W) during the period of October 1 to November 14, 2019. This campaign was funded through the DOE Office of Science Early Career Research Program (DE-SC0018979) as one of three major campaigns to be conducted at three ARM observatories, including the Eastern North Atlantic (ENA) station in 2020–2021 and North Slope of Alaska (NSA) site in 2021–2023, besides SGP. Different INP episodes were assessed to develop an SGP-relevant ice nucleation parameterization that would help understand convective and mixed-phase cloud systems typically observed in this region.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2024

AGR-2 TRISO Layer Thickness Imaging Archive

As a part of fuel quality control characterization, optical microscopy images of particle cross sections near midplane were acquired at Oak Ridge National Laboratory (ORNL). These particles were produced by the Advanced Gas Reactor Fuel Development and Qualification (AGR) Program’s AGR-2 irradiation campaign. These images may be of use for the development of image processing algorithms with the benchmark values measured at ORNL. This report provides those benchmark values, along with the raw images and data generated by the ORNL particle layer thickness analysis process.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2024

AGR-2 TRISO Shadow Imaging Archive

As a part of fuel quality control characterization, backlit shadow images of particles produced by the Advanced Gas Reactor Fuel Development and Qualification (AGR) Program’s AGR-2 irradiation campaign were acquired at Oak Ridge National Laboratory (ORNL). These images may be of use for the development of image processing algorithms with the benchmark values measured at ORNL. This report provides those benchmark values, along with the raw images and data generated by the ORNL shadow imaging process.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS1974

Artificial meteor ablation studies - Olivine

Artificial meteor ablation has been performed on a Mg-rich olivine sample by means of an arc-heated plasma of ionized air. Experimental conditions simulated a meteor traveling about 12 km/sec at an altitude of 70 km. The mineral content of the original olivine was 98% olivine (including traces of olivine alteration products) and 2% chromite. The forsterite content of the original olivine was Fo 89 and increased to Fo 94 in the recrystallized olivine after ablation. In addition, lamella-like intergrowths of magnetite were prevalent. Wherever magnetite occurred, Mg increased and Fe decreased in the recrystallized olivine. The Fe for the magnetite exsolved from the original olivine crystals. Individual particles (i.e., spherules) were also characterized by magnetite intergrowths. Fusion crusts on the Allende and Murchison meteorites were compared with the fusion crust on the olivine sample. The Allende fusion crust consisted of a recrystallized olivine, richer in Mg and deficient in Fe in comparison with the original meteorite's olivine, and abundant magnetite grains.

Blanchard, M. B.↗
NASA NTRS1974

Study of the use of Metal-Oxide-Silicon (MOS) devices for particulate detection and monitoring in the earth's atmosphere

A metal-oxide-silicon (MOS) capacitor-type particulate sensor was evaluated for use in atmospheric measurements. An accelerator system was designed and tested for the purpose of providing the necessary energy to trigger the MOS-type sensor. The accelerator system and the MOS sensor were characterized as a function of particle size and velocity. Diamond particles were used as particulate sources in laboratory tests. Preliminary tests were performed in which the detector was mounted on an aircraft and flown in the vicinity of coal-fired electric generating plants.

Brooks, A. D.↗
NASA NTRS1978

Atmospheric scavenging of solid rocket exhaust effluents

Solid propellant rocket exhaust was directly utilized to ascertain raindrop scavenging rates for hydrogen chloride. Two chambers were used to conduct the experiments; a large, rigid walled, spherical chamber stored the exhaust constituents, while the smaller chamber housing all the experiments was charged as required with rocket exhaust HCl. Surface uptake experiments demonstrated an HCl concentration dependence for distilled water. Sea water and brackish water HCl uptake was below the detection limit of the chlorine-ion analysis technique used. Plant life HCl uptake experiments were limited to corn and soybeans. Plant age effectively correlated the HCl uptake data. Metallic corrosion was not significant for single 20 minute exposures to the exhaust HCl under varying relative humidity. Characterization of the aluminum oxide particles substantiated the similarity between the constituents of the small scale rocket and the full size vehicles.

Fenton, D. L.↗
NASA NTRS1979

The Production of Solar Cell Grade Silicon from Bromosilanes

A continuous Flow Reactor (CFR) process based on the hydrogen reduction of the bromosilanes SiBr4 and SiHBr3 was proposed. Initial experiments carried and directed at obtaining overall yield data for bromosilane reduction in the CFR, indicated the need for increased reactor residence time and deposition substrate particle packing density to fully characterize the kinetics (rate) and thermodynamics (yield) of observed silicon production. Fluidized bed experiments were therefore initiated to overcome these experimental difficulties, which showed both thermal decomposition and hydrogen reduction of SiHBr3 in a fluid bed reactor to present attractive closed-loop processes for producing solar cell grade polycrystalline silicon. No process selection could be made however due to the fact that preliminary optimization of 2 of 3 process stages in each case during the course of the experimental program showed comparable attainment of cost element objectives.

Schumacher, J. C.↗
NASA NTRS1987

Magnetotail research - The early years

The history of observations and theoretical modeling of the geomagnetic tail in the period 1961-1971 is reviewed. Particular attention is given to the contributions of the IMP-1 (Explorer 18) satellite (launched in 1963) and the Pioneer 7 and 8 probes. Typical data are presented in extensive graphs and diagrams and discussed in detail. Major topics considered include the discovery of the permanent tail and the imbedded plasma and neutral sheet, the determination of the average configuration and dynamical changes, estimates of the tail length, and the characterization of interplanetary-charged-particle access to the polar caps.

Ness, N. F.↗
NASA NTRS1989

Titanium carbide and titania phases on Antarctic ice particles of probable extraterrrestrial origin

Two unique titania-rich particles, found within ancient Antarctic ice have been discovered and characterized, and are believed to be of extraterrestrial origin. Both particles contain abundant submicron-sized crystals of Magneli phases (Ti(n)O(2n-1). In addition, one particle contains a core of TiC. Whereas the Magneli phases would have been stable in the early solar nebula, and so probably formed there, the TiC is more likely to have condensed in the cool, dusty, carbon-rich outer shell of a red giant star. It is suggested that both particles are interplanetary dust particles whose Magneli phases carry a record of the PO2-T conditions of the early solar nebula. It is further suggested that the TiC grain in particle 705 is remnant interstellar dust.

Zolensky, M. E.↗
NASA NTRS1992

Viscoelastic Response Of A Highly Filled Polymer

Report describes experimental and theoretical studies of nonlinear viscoelastic response of elastomeric binder material filled with small particles of different material. Studies characterize response with sufficient accuracy for use in designing parts subjected to high strains.

Peng, Steven T. J.↗