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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 685 records · Page 38
All sourcesNASA NTRSDOE OSTI
NASA NTRS1999

Scanning Mode Shock Position Sensor Invented and Demonstrated

A flow-visualizing system with a scanning optical beam offers greater advantages than the conventional approaches. In addition to a higher signal-to-noise ratio and lower source power, the scanning permits visualization of weak phenomena such as the scattering and diffraction of light on shocks. Scanning beam flow-visualization techniques were evaluated at the NASA Lewis Research Center for shock position sensing. In an effort to eliminate moving parts, a spectral scanning technique was invented and demonstrated.

Adamovsky, Grigory↗
DOE OSTI2017

Particle and chemical control using tunnel flow

An apparatus for contaminant control, having: a first optical assembly including: a first light homogenizer tunnel with: a first end connected to an extreme ultra-violet light source, a second end in communication with a destination chamber, a first enclosed space, and, a first gas input arranged to introduce a first gas such that the first gas flows in a first direction toward the first end and in a second direction toward the second end. The apparatus alternately having: a second optical assembly including: a second light homogenizer tunnel with: a third end connected to an extreme ultra-violet light source, a fourth end in communication with a destination chamber, a second enclosed space, a diffusion barrier tube including: a fifth end facing the fourth end and a sixth end in communication with a destination chamber, and a second gas input between the second light homogenizer tunnel and the diffusion tube.

42 ENGINEERING↗
DOE OSTI2013

A unified lense-thirring precession model for optical and X-ray quasi-periodic oscillations in black hole binaries

Recent observations of accreting black holes reveal the presence of quasi-periodic oscillations (QPO) in the optical power density spectra. The corresponding oscillation periods match those found in X-rays, implying a common origin. Among the numerous suggested X-ray QPO mechanisms, some may also work in the optical. However, their relevance to the broadband—optical through X-ray—spectral properties have not been investigated. For the first time, we discuss the QPO mechanism in the context of the self-consistent spectral model. We propose that the QPOs are produced by Lense-Thirring precession of the hot accretion flow, whose outer parts radiate in optical wavelengths. At the same time, its innermost parts are emitting X-rays, which explains the observed connection of QPO periods. We predict that the X-ray and optical QPOs should be either in phase or shifted by half a period, depending on the observer position. We investigate the QPO harmonic content and find that the variability amplitudes at the fundamental frequency are larger in the optical, while the X-rays are expected to have strong harmonics. We then discuss the QPO spectral dependence and compare the expectations to the existing data.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2014

Towards a Molecular Level Understanding of the Multi-Electron Catalysis of Water Oxidation on Metal Oxide Surfaces

Earth abundant metal oxides play a central role as catalysts in the essential chemical transformations of sunlight to fuel conversion, which are the oxidation of water and the reduction of carbon dioxide. The rapidly growing interest in renewable fuel generation by using the energy of the sun has recently led to substantial breakthroughs in the use of first row transition metal oxides as catalysts for oxygen evolution from water. Substantive improvements of rates and lowering of overpotentials have been achieved by exploiting materials properties on the nanoscale, or taking advantage of the synergy of multiple metals. Moreover, knowledge derived from mechanistic investigations with structure specific spectroscopy is accelerating efficiency improvements. Monitoring by time-resolved FT-infrared spectroscopy reveals the molecular nature of active sites, while in situ X-ray and optical spectroscopy under reaction conditions provides insights into the electronic structure of the surface metal centers participating in the catalysis. By combining the bond specificity of vibrational spectroscopy with the metal electronic structure specificity of optical, X-ray absorption or photoelectron spectroscopy, a complete understanding of active surface sites on metal oxides begins to emerge. Charge flow driving the chemical transformations probed by optical spectroscopy across time scales from ultrafast to very slow reveals the processes that control the productive use of charges delivered to the catalyst. Coupling of the water oxidation catalysis at a metal oxide catalyst with carbon dioxide reduction at a heterobinuclear chromophore, which is the goal of the artificial photosystem approach, is demonstrated by a well-defined all-inorganic polynuclear unit.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

High-precision chemical quantum sensing in flowing monodisperse microdroplets

A method is presented for high-precision chemical detection that integrates quantum sensing with droplet microfluidics. Using nanodiamonds (ND) with fluorescent nitrogen-vacancy (NV) centers as quantum sensors, rapidly flowing microdroplets containing analyte molecules are analyzed. A noise-suppressed mode of optically detected magnetic resonance is enabled by pairing controllable flow with microwave control of NV electronic spins, to detect analyte-induced signals of a few hundredths of a percent of the ND fluorescence. Using this method, paramagnetic ions in droplets are detected with low limit-of-detection using small analyte volumes, with exceptional measurement stability over >10 3 s. In addition, these droplets are used as microconfinement chambers by co-encapsulating ND quantum sensors with various analytes such as single cells, suggesting wide-ranging applications including single-cell metabolomics and real-time intracellular measurements from bioreactors. Important advances are enabled by this work, including portable chemical testing devices, amplification-free chemical assays, and chemical imaging tools for probing reactions within microenvironments.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2013

Properties of Ta{sub 2}O{sub 5} thin films prepared by ion-assisted deposition

Graphical abstract: - Highlights: • Investigating the effect of ion-beam parameters on optical properties. • Exploring the effect of ion-beam parameters on structural properties. • Studying XRD patterns of Ta{sub 2}O{sub 5} films deposited at different ion energies. - Abstract: Tantalum penta-oxide (Ta{sub 2}O{sub 5}) thin films were deposited onto highly polished and clean, fused silica glass substrates via ion beam-assisted deposition at room temperature using a high-vacuum coater equipped with an electron beam gun. The effects of ion beam parameters, oxygen flow rate, and deposition rate on the optical and structural properties as well as the stress of Ta{sub 2}O{sub 5} films were studied. It has been revealed that Ta{sub 2}O{sub 5} thin films deposited at 300 eV ion beam energy, 60 μA/cm{sup 2} ion current density, 20 sccm oxygen flow rate and 0.6 nm/s deposition rate demonstrated excellent optical, structural and compressive stress.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Dynamic Heat Flow and Current Distribution Analysis in the Bottom Anode of an Electric Arc Furnace Using Fiber-Optic Sensors

A reliable method for monitoring bottom anode wear during DC Electric Arc Furnace (DC-EAF) operation is of critical importance for safe and efficient steel production. Underestimation of bottom wear poses a serious safety risk that must be avoided, while overestimation of bottom wear also poses challenges, as premature anode replacement is expensive and affects EAF productivity. Previously, we demonstrated that fiber-optic sensors can be successfully deployed to create a spatially distributed temperature map to monitor the health of the anode. The present work explores the heat flow and current density distribution in bottom anode pins to predict bottom wear, steel penetration events, and monitor refractory erosion. Small dynamic variations in pin temperature induced by joule heating during arcing also provide a means to observe local current flows in each pin. When mapped, these measurements provide a real-time view of the non-uniform and dynamic current flow in the bottom anode during EAF operation that can affect bottom wear.

Bottom Anode↗
NASA NTRS1993

Development of separation due to interaction between a shock wave and a turbulent boundary layer perturbed by rarefaction waves

The interaction of a turbulent boundary layer with rarefaction and shock waves in flows past inclined steps was investigated experimentally and theoretically. The experiments were carried out in supersonic wind tunnels with test sections of 0.6 x 0.6 m and 0.2 x 0.2 m, with adiabatic conditions on the surface model. Based on detailed measurements of pressure fields, velocity, and surface friction, combined with results of optical visualization and analysis of limiting flow lines, three characteristic flow regimes are identified. These are (1) nonseparated flow at small step angles, (2) formation of a local separation zone with a free separation point at moderate step angles, and (3) formation of a large-scale separated flow with a fixed separation point at sufficiently large step angles. The quantitative gasdynamic schemes and surface pressure distributions for these flow regimes are shown for Mach 2.85.

Zheltovodov, A. A.↗
DOE OSTI2014

CLOAKED GAMMA-RAY BURSTS

It is suggested that many gamma-ray bursts (GRBs) are cloaked by an ultrarelativistic baryonic shell that has high optical depth when the photons are manufactured. Such a shell would not fully block photons reflected or emitted from its inner surface, because the radial velocity of the photons can be less than that of the shell. This avoids the standard problem associated with GRBs that the thermal component should be produced where the flow is still obscured by high optical depth. The radiation that escapes high optical depth obeys the Amati relation. Observational implications may include (1) anomalously high ratios of afterglow to prompt emission, such as may have been the case in the recently discovered PTF 11agg, and (2) ultrahigh-energy neutrino pulses that are non-coincident with detectable GRB. It is suggested that GRB 090510, a short, very hard GRB with very little afterglow, was an exposed GRB, in contrast to those cloaked by baryonic shells.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRSDate not supplied

Using Digital Image Correlation for Material Testing at Cryogenic Temperatures

Recent efforts were made to parametrize an aluminum alloy at cryogenic temperatures to calibrate finite element models simulating material deformation. Digital image correlation (DIC) was used to measure material properties using front/back strains of specimens during tensile tests. Data acquired from DIC was compared to physical extensometer measurements. Two camera pairs (front and back) were mounted via aluminum extrusion to the exterior of an environmental chamber of a hydraulic test stand. Images were taken through single-pane optical glass windows of the environment chamber. Positive pressure bags encased the cameras, attaching to the perimeter of the glass to keep out moisture and prevent windows from frosting. Figure 1 shows the environmental setup and the camera setup during cryogenic testing. Some of the challenges during testing at cryogenic temperatures include the gaseous flow of liquid nitrogen in the optical path of the mounted cameras, frost buildup on the windows as seen in Figure 1b, and frost on the test coupon. The temperature gradient present during the introduction of liquid nitrogen into the chamber can increase the projection error of images captured of the specimen. Figure 2 shows the estimated projection error from DIC as a function of temperature during the cool down process. This presentation addresses some of the concerns and observations when using DIC for testing at cryogenic temperatures using methods of isolated camera system and techniques for maintaining the glass panel clear from frost.

Joseph Cochran↗
DOE OSTI2019

Application of predictive data analytics to model daily hydrocarbon production using petrophysical, geomechanical, fiber-optic, completions, and surface data: A case study from the Marcellus Shale, North America

Predicting gas production from stimulated unconventional reservoirs has always been a challenge to oil and gas companies because the physics of fluid flow through such reservoirs is not well understood. On the other hand, modeling gas production from shale reservoirs is a complex multi-variate problem that requires proper integration of data from multiple disciplines, such as geology, petrophysics, geomechanics, completions, and surface-based measurements, etc. Here this study demonstrates the application of data-driven machine learning algorithms, integrating geoscientific, distributed acoustic sensing (DAS), distributed temperature sensing (DTS) fiber-optic, completions, flow scanner production log, and surface data to model daily gas production from a 28-stage stimulated horizontal well drilled in the Marcellus Shale of the Appalachian basin in North America. In addition, this study aims to utilize the data from a fiber-optic monitoring system, such as DAS and DTS to evaluate the well performance. We build supervised data-driven machine learning models using Random Forest (RF), Artificial Neural Network (ANN), and Support Vector Machine (SVM) algorithms to understand the well performance and forecast the daily gas production. The study compares the forecasted results, tests the level of accuracy, and addresses different issues with these machine learning algorithms. A spatio-temporal database is constructed and used to perform sensitivity analyses to identify the key drivers for gas production. The results show that RF and ANN algorithms can be used to predict daily gas production with significantly high accuracy; however, RF algorithm is the best predictor in terms of highest accuracy (96%), less computational time and cost. Based on sensitivity analysis, it appears that Poisson's ratio, minimum horizontal stress, DAS, casing pressure, gamma log are the most important parameters to predict gas production.

02 PETROLEUM↗
NASA NTRS1987

Determining Optical Axes of Uniaxial Crystals

Polarizing-microscope concept adapted for thick samples. Optical axis of crystal usually found by examining sample thinner than 1 mm between crossed polarizing plates. Frequently impractical to cut off small sample of crystal for testing, technique modified to accommodate large crystals. Ability to circumvent effect of birefringence has applications where laser beams must be transmitted through uniaxial crystals, as in laser diagnostics of contained flows in systems requiring windows for optical access.

Schock, H. J.↗
DOE OSTI2015

EVIDENCE OF THE DYNAMICS OF RELATIVISTIC JET LAUNCHING IN QUASARS

Hubble Space Telescope (HST) spectra of the EUV, the optically thick emission from the innermost accretion flow onto the central supermassive black hole, indicate that radio loud quasars (RLQs) tend to be EUV weak compared to the radio-quiet quasars; yet the remainder of the optically thick thermal continuum is indistinguishable. The deficit of EUV emission in RLQs has a straightforward interpretation as a missing or a suppressed innermost region of local energy dissipation in the accretion flow. This article is an examination of the evidence for a distribution of magnetic flux tubes in the innermost accretion flow that results in magnetically arrested accretion (MAA) and creates the EUV deficit. These same flux tubes and possibly the interior magnetic flux that they encircle are the sources of the jet power as well. In the MAA scenario, islands of large-scale vertical magnetic flux perforate the innermost accretion flow of RLQs. The first prediction of the theory that is supported by the HST data is that the strength of the (large-scale poloidal magnetic fields) jets in the MAA region is regulated by the ram pressure of the accretion flow in the quasar environment. The second prediction that is supported by the HST data is that the rotating magnetic islands remove energy from the accretion flow as a Poynting flux dominated jet in proportion to the square of the fraction of the EUV emitting gas that is displaced by these islands.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2023

Flow Injection Electrochemical Quartz Crystal Microbalance with ICP-OES Detection: Electroprecipitation and Stripping of Lanthanum and Neodymium in a Flow Cell

We used an improved version of our hyphenated analysis technique, flow injection electrochemical quartz crystal microbalance (EQCM) with inductively coupled optical emission spectroscopy, to investigate the electroprecipitation of lanthanum and neodymium from flowing solutions. The improved version has two independent flow injection circuits, allowing different conditions for electrochemical precipitation (pH=4.3 or 2.6) and quick stripping (2% HNO3) with EQCM mass detection and ICP-OES elemental analysis. Lanthanum or neodymium ions in a 500 uL sample were injected into a carrier stream and deposited onto an EQCM housed in a micro flow cell, owing to a localized high-pH layer. The deposits are subsequently stripped from the electrode using HNO3 and analyzed downstream using an ICP-OES. We found that using acidic solutions without supporting electrolyte leads to an increase of the amount of lanthanum detected by 4-fold. The enhanced deposition can be attributed to enhanced mass transfer by migration. Furthermore, we showed that by applying chronopotentiometry, we can detect a change in the hydrogen evolution reaction mechanism that enables the precipitation of lanthanides on the surface of the electrode. Understanding and enhancing the deposition of lanthanides is relevant for elemental or isotopic detection in nuclear forensics.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
NASA NTRS1980

A Scanning laser-velocimeter technique for measuring two-dimensional wake-vortex velocity distributions

A rapid scanning two dimensional laser velocimeter (LV) has been used to measure simultaneously the vortex vertical and axial velocity distributions in the Langley Vortex Research Facility. This system utilized a two dimensional Bragg cell for removing flow direction ambiguity by translating the optical frequency for each velocity component, which was separated by band-pass filters. A rotational scan mechanism provided an incremental rapid scan to compensate for the large displacement of the vortex with time. The data were processed with a digital counter and an on-line minicomputer. Vaporized kerosene (0.5 micron to 5 micron particle sizes) was used for flow visualization and LV scattering centers. The overall measured mean-velocity uncertainity is less than 2 percent. These measurements were obtained from ensemble averaging of individual realizations.

Gartrell, L. R.↗
NASA NTRS2021

Emission Spectroscopy Characterization of Electrodes Species in the Freestream Flow at the NASA Ames Miniature Arc Jet II Facility

The second generation miniature Arc Jet (mARC II) is a subscale arc jet at NASA Ames Research Center that is undergoing initial characterization. During its operation, the electrodes used to produce continuous plasma flows deteriorate and the flow purity decreases. The present work reports the use of optical emission spectroscopy as a characterization tool for impurities in the plasma flow. The discussion is focused on the interpretation of spectroscopic measurements and their evolution under different testing conditions. Special emphasis is given to copper and silver, the main atomic elements of the electrodes. The highest rate of anode deterioration is found to occur during the arc jet ignition, while cathode deterioration is constant throughout the entire run. Based on the experimental spectra, a preliminary numerical characterization of the plasma temperature, enthalpy and number density is conducted.

facility↗
NASA NTRS2011

Laser-Induced Thermal Acoustics Theory and Expected Experimental Errors when Applied to a Scramjet Isolator Model

A scramjet isolator model test apparatus is being assembled in the Isolator Dynamics Research Lab (IDRL) at the NASA Langley Research Center in Hampton, Virginia. The test apparatus is designed to support multiple measurement techniques for investigating the flow field in a scramjet isolator model. The test section is 1-inch high by 2-inch wide by 24-inch long and simulates a scramjet isolator with an aspect ratio of two. Unheated, dry air at a constant stagnation pressure and temperature is delivered to the isolator test section through a Mach 2.5 planar nozzle. The isolator test section is mechanically back-pressured to contain the resulting shock train within the 24-inch isolator length and supports temperature, static pressure, and high frequency pressure measurements at the wall. Additionally, nonintrusive methods including laser-induced thermal acoustics (LITA), spontaneous Raman scattering, particle image velocimetry, and schlieren imaging are being incorporated to measure off-wall fluid dynamic, thermodynamic, and transport properties of the flow field. Interchangeable glass and metallic sidewalls and optical access appendages permit making multiple measurements simultaneously. The measurements will be used to calibrate computational fluid dynamics turbulence models and characterize the back-pressured flow of a scramjet isolator. This paper describes the test apparatus, including the optical access appendages; the physics of the LITA method; and estimates of LITA measurement uncertainty for measurements of the speed of sound and temperature.

Middleton, Troy F.↗