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All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Ni/SiO 2 catalysts for polyolefin deconstruction via the divergent hydrogenolysis mechanism

Noble metal-based hydrogenolysis is emerging as a key chemical deconstruction technology of polyolefins into valuable products. Still, the catalyst cost and availability are significant barriers to handling the large volume of plastics. Cheap earth-abundant metals have been deemed inactive for polyolefin hydrogenolysis. Herein, we report that Ni/SiO 2 is active in deconstructing low-density polyethylene to n-alkanes (C 6 -C 35 ) at mild conditions (300 °C, 30barH 2 ) with maximum liquid yields of 65 wt%. In this study, we expose a new mechanism of long-alkane hydrogenolysis that encompasses chain location-dependent single and multiple C-C bond cracking events and rationalizes product selectivity and molecular weight dependence. Ni/SiO 2 catalysts are reusable and can handle multiple plastics producing feedstock-dependent products (i.e., n-alkanes, iso-alkanes, cyclics, aromatics, etc.). The findings broaden the scope of viable catalysts polyolefin hydrogenolysis and unleash the potential to manage the volume of plastic waste.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Transmission history of SARS-CoV-2 in humans and white-tailed deer

The emergence of a novel pathogen in a susceptible population can cause rapid spread of infection. High prevalence of SARS-CoV-2 infection in white-tailed deer ( Odocoileus virginianus ) has been reported in multiple locations, likely resulting from several human-to-deer spillover events followed by deer-to-deer transmission. Knowledge of the risk and direction of SARS-CoV-2 transmission between humans and potential reservoir hosts is essential for effective disease control and prioritisation of interventions. Using genomic data, we reconstruct the transmission history of SARS-CoV-2 in humans and deer, estimate the case finding rate and attempt to infer relative rates of transmission between species. We found no evidence of direct or indirect transmission from deer to human. However, with an estimated case finding rate of only 4.2%, spillback to humans cannot be ruled out. The extensive transmission of SARS-CoV-2 within deer populations and the large number of unsampled cases highlights the need for active surveillance at the human–animal interface.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2024

Precise relative magnitude measurement improves fracture characterization during hydraulic fracturing

SUMMARY Microseismic monitoring is an important technique to obtain detailed knowledge of in-situ fracture size and orientation during stimulation to maximize fluid flow throughout the rock volume and optimize production. Furthermore, considering that the frequency of earthquake magnitudes empirically follows a power law (i.e. Gutenberg–Richter), the accuracy of microseismic event magnitude distributions is potentially crucial for seismic risk management. In this study, we analyse microseismicity observed during four hydraulic fracture treatments of the legacy Cotton Valley experiment in 1997 at the Carthage gas field of East Texas, where fractures were activated at the base of the sand-shale Upper Cotton Valley formation. We perform waveform cross-correlation to detect similar event clusters, measure relative amplitude from aligned waveform pairs with a principal component analysis, then measure precise relative magnitudes. The new magnitudes significantly reduce the deviations between magnitude differences and relative amplitudes of event pairs. This subsequently reduces the magnitude differences between clusters located at different depths. Reduction in magnitude differences between clusters suggests that some attenuation-related biases could be effectively mitigated with relative magnitude measurements. The maximum likelihood method is applied to understand the magnitude frequency distributions and quantify the seismogenic index of the clusters. Statistical analyses with new magnitudes suggest that fractures that are more favourably oriented for shear failure have lower b-value and higher seismogenic index, suggesting higher potential for relatively larger earthquakes, rather than fractures subparallel to maximum horizontal principal stress orientation.

58 GEOSCIENCES↗
DOE OSTI2026

SDN-Based Dynamic Cybersecurity Framework of IEC-61850 Communications in Smart Grid

In recent years, critical infrastructure and power grids have experienced a series of cyber-attacks, leading to temporary, widespread blackouts of considerable magnitude. Since most substations are unmanned and have limited physical security protection, cyber breaches into power grid substations present a risk. Nowadays, the susceptibility of SDN architecture to cyber-attacks has exhibited a notable increase in recent years, as indicated by research findings. This suggests a growing concern regarding the potential for cybersecurity breaches within the SDN framework. In this paper, we propose a hybrid intrusion detection system (IDS)-integrated SDN architecture for detecting and preventing the injection of malicious IEC 61850-based generic object-oriented system event (GOOSE) messages in a digital substation. Additionally, this program locates the fault’s location and, as a form of mitigation, disables a certain port. Furthermore, implementation examples are demonstrated and verified using a hardware-in-the-loop (HIL) testbed that mimics the functioning of a digital substation.

Liu, Chen-Ching [Virginia Tech] (ORCID:00000002894↗
DOE OSTI2026

Soil nitrogen mineralization rates, nutrient stocks, stable isotopes, and water volumetric measurements across terrestrial-aquatic interfaces from three wetlands at the Tanglewood Biological Station, Alabama

This dataset supports a broader study investigating wetland hydrologic and biogeochemical responses to inundation events. Soil samples were collected across four sampling events along terrestrial-aquatic gradients at three wetland sites located within the Tanglewood Biological Station in Alabama from April 2024 to June 2025. The contents in this data package include soil in-situ nitrogen mineralization rates (measurements of net nitrification, net ammonification, and net mineralization), nutrient stocks (total carbon, total nitrogen, and organic matter), stable isotopes (carbon and nitrogen), and water volumetric measurements (water-filled pore space). Water level data related to each wetland location can be found at https://data.ess-dive.lbl.gov/view/doi:10.15485/2530253 (Kirker et al., 2024), related water geochemistry data can be found at https://data.ess-dive.lbl.gov/datasets/doi:10.15485/3001967 (Forbes et al., 2025), and related surface water sediment chemistry data can be found at https://data.ess-dive.lbl.gov/datasets/doi:10.15485/3377325 (Molina Serpas et al., 2026). In addition to this readme, this data package also includes a file-level metadata (FLMD) file that describes each file and a data dictionary (DD) that describes all column/row headers and variable definitions. This dataset is comprised of (1) file-level metadata; (2) data dictionary; (3) field metadata and international generic sample numbers (IGSNs); (4) readme; (5) the field protocol; and (6) a subfolder with sample data. The sample data subfolder contains (1) net nitrification rate, (2) net ammonification rate, (3) areal net mineralization rate, (4) percent organic matter, (5) water-filled pore space, (6) total carbon content, (7) total nitrogen content, (8) stable carbon isotope (delta carbon-13), and (9) stable nitrogen isotope (delta nitrogen-15), and (10) methods codes. All files are .csv or .pdf.

13-C↗
DOE OSTI2020

An updated estimate of the Mu2e experiment sensitivity

The Mu2e experiment at Fermilab will search for the conversion of a negative muon into an electron inside the field of a nucleus. This process does not conserve charged-lepton flavour and is heavily suppressed in the Standard Model (SM), with a branching ratio < 10-50. Any evidence of it would be an undeniable evidence of new physics beyond the SM. The project sets out to achieve a single event sensitivity of $\sim 3 × 10^{-17}$ on the ratio between the probability for a conversion of a negative muon into an electron and the one for a muon capture by the nucleus. Such a sensitivity would represent a 4 orders of magnitude improvement on the previous upper limit for the process, making possible to test predictions of different extensions of the SM. Mu2e uses three superconducting solenoids to produce and measure the muon conversions. In the first solenoid, the Production Solenoid, pions and kaons are produced, together with other secondary products, by 8 GeV kinetic energy proton interactions in a tungsten target. A gradient magnetic field is specifically designed to direct low momentum particles into the Transport Solenoid, an S-shaped magnet that filters out particles with unwanted charge and momentum. Muons, produced by pion and kaon decays, finally reach the aluminum Stopping Target in the Detector Solenoid, where they eventually stop and convert. The result of the conversion process is a monochromatic electron of ~105 MeV/c momentum. The Detector Solenoid also hosts the two main detectors: a straw tube tracker and two CsI calorimeter disks, both providing measurement of event kinematics. A germanium detector and a LaBr crystal are located downstream of the Detector Solenoid to measure the X and gamma rays produced by the muon captures in the Stopping Target. A veto system of scintillators covering the Detector Solenoid and half of the Transport Solenoid is used to identify and reject cosmic rays interactions. With respect to the initial project, the Mu2e running plan has evolved to a staged configuration with 2 years at reduced intensity before the 2025 accelerator shutdown for the neutrino beam upgrade and 2 or 3 years at full intensity after that. This, together with geometry changes and a better knowledge of detector performances obtained by the first slice tests, has required a full revision of the signal over background selection that is the subject of this thesis. In order to achieve a new estimate of Mu2e sensitivity, the simulation of the data corresponding to the first 2 years of data acquisition has been performed. This includes both conversion electrons (CE) and the main sources of background: cosmics, decay-in orbits (DIO), radiative pion captures (RPC) and antiprotons. The characteristics of the signal and of the main backgrounds have been studied to define the best selection variables for CE. A special effort has been devoted to the evaluation of the antiproton background. The lack of experimental data for antiproton production cross section makes the systematic uncertainty on this background significant. A new parameterization of the cross section has been developed to fit the existing data and to provide a more reliable estimate of the systematic uncertainty by comparing the results of the old and the new model. A special effort has been devoted to the optimization of the antiprotons Monte Carlo generator. This study has also revealed that the dominant component within this background is represented by antiprotons produced in the opposite direction with respect to the Transport Solenoid entrance and then redirected to it by back-scattering processes in the Production Target. This ultimately highlights the sensitivity of the background estimate to the G4 handling of antiproton interactions in the 1 to 3 GeV/c momentum range. Finally, the final experimental sensitivity has been studied. The momentum and time selection have been optimized to obtain the 5-sigma discovery reach or, in case of no signal, the upper limit on conversion probability. The results confirm that, in the firs t two years of data taking, Mu2e will be able to improve the current experimental sensitivity for muon-to-electron conversion in an atomic field by more than 3 order of magnitudes.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2025

Size-resolved Eddy-Covariance Particle Flux Measurement during the TRACER Campaign (Final Report)

The main goal of the TRacking Aerosol Convection interactions ExpeRiment (TRACER) campaign was to study aerosol–cloud interactions during deep convection over the Houston area. This project deployed a suite of instrumentation with the aim to (1) quantify turbulent vertical particle fluxes during at DOE-ARM sites, including TRACER, (2) assess hygroscopic growth factors and hygroscopicity parameters of the material driving modal aerosol growth during new particle formation and growth events, (3) derive turbulent aerosol mass fluxes using co-located Doppler LIDAR measurements, and (4) create quality-controlled PI data products to support future research utilizing data collected during the TRACER campaign. This report summarized the main findings from the deployments at two DOE-ARM sites. Briefly, we found that new particle formation may occur aloft, in a residual layer, near the top of the boundary layer. Small grown particles appear later due to downward mixing with daytime turbulence. The species that are responsible for aerosol modal growth had hygroscopicity parameters varying between 0.05 and 0.34. These values systematically depended on the wind sector, suggesting that the chemical composition of the precursors differed. This work demonstrated that lidar retrievals of the elastic backscatter and Doppler velocity can be used to obtain surface number emissions of particles with a diameter greater than 0.53 µm. During TRACER, emission particle number fluxes peaked near ∼ 100 cm−2 s−1. Multiple quality-controlled PI data products that will support future TRACER related science were generated and made publically available.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2023

Overcoming genetic paucity of Camelina sativa : possibilities for interspecific hybridization conditioned by the genus evolution pathway

Camelina or false flax (Camelina sativa) is an emerging oilseed crop and a feedstock for biofuel production. This species is believed to originate from Western Asian and Eastern European regions, where the center of diversity of the Camelina genus is located. Cultivated Camelina species arose via a series of polyploidization events, serving as bottlenecks narrowing genetic diversity of the species. The genetic paucity of C. sativa is foreseen as the most crucial limitation for successful breeding and improvement of this crop. A potential solution to this challenge could be gene introgression from Camelina wild species or from resynthesized allohexaploid C. sativa. However, both approaches would require a complete comprehension of the evolutionary trajectories that led to the C. sativa origin. Although there are some studies discussing the origin and evolution of Camelina hexaploid species, final conclusions have not been made yet. Here, we propose the most complete integrated evolutionary model for the Camelina genus based on the most recently described findings, which enables efficient improvement of C. sativa via the interspecific hybridization with its wild relatives. We also discuss issues of interspecific and intergeneric hybridization, aimed on improving C. sativa and overcoming the genetic paucity of this crop. The proposed comprehensive evolutionary model of Camelina species indicates that a newly described species Camelina neglecta has a key role in origin of tetra- and hexaploids, all of which have two C. neglecta-based subgenomes. Understanding of species evolution within the Camelina genus provides insights into further research on C. sativa improvements via gene introgression from wild species, and a potential resynthesis of this emerging oilseed crop.

09 BIOMASS FUELS↗
NASA NTRS1976

Terrestrial kilometric radiation: 1: Spatial structures studies

Observations are presented of lunar occultations of the earth at 250 kHz obtained with the Radio-Astronomy-Explorer-2 satellite which were used to derive two dimensional maps of the location of the sources of terrestrial kilometric radiation (TKR). By examining the two dimensional source distributions as a function of the observer's location (lunar orbit) with respect to the magnetosphere, the average three dimensional location of the emission regions can be estimated. Although TKR events at 250 kHz can often be observed at projected distances corresponding to the 250 kHz electron gyro or plasma level (approximately 2 earth radii), many events are observed much farther from the earth (between 5 and 15 earth radii). Dayside emission apparently in the region of the polar cusp and the magnetosheath and night emission associated with regions of the magnetotail are examined. The nightside emission is suggestive of a mechanism involving plasma sheet electron precipitation in the pre-midnight sector.

Alexander, J. K.↗
NASA NTRS1976

Terrestrial kilometric radiation. I - Spatial structure studies

Observations of lunar occultations of earth at 250 kHz, obtained with the Radio Astronomy Explorer 2 satellite, have been used to derive two-dimensional maps of the location of the sources of terrestrial kilometric radiation (TKR). By examining the two-dimensional source distributions as a function of the observer's location (lunar orbit) with respect to the magnetosphere, the average three-dimensional location of the emission regions can be estimated. Although TKR events at 250 kHz can often be observed at projected distances corresponding to the 250-kHz electron gyro or plasma level (about 2 earth radii), many events are observed much farther from earth (about 5 to 15 radii). On the dayside, emission was apparently observed in the region of the polar cusp and the magnetosheath at a magnetic latitude of about 70 deg; in the night hemisphere, emission is found to be associated with regions of the magnetotail at latitudes of at least 70 deg. The nightside emission is suggestive of a mechanism involving plasma-sheet electron precipitation in the premidnight sector.

Alexander, J. K.↗
NASA NTRS1986

MHD simulation of the 'geoeffectiveness' of interplanetary disturbances

A series of examples is used to evaluate the 'geoeffectiveness' prediction technique that is based on the classical, initial boundary value problem of MHD. For the nonplanar simulation of a corotating stream, it is shown that the technique can compute relevant solar wind parameters at the earth's location. For the nonplanar simulation of a complex series of events, qualitative agreement is found for large-scale structures, but the phasing and amplitudes are not satisfactory. Preliminary work with a fully three-dimensional, time-dependent simulation of a flare-generated interplanetary shock wave shows that the effect of the latitudinal variation produces attenuation of the heliolongitudinal component of the IMF and of the radial velocity.

Dryer, M.↗
NASA NTRS1991

The microgravity environment of the Space Shuttle Columbia middeck during STS-32

Four hours of three-axis microgravity accelerometer data were successfully measured at the MA9F locker location in the Orbiter middeck of Columbia as part of the Microgravity Disturbances Experiment (MDE) on STS-32. These data were measured using the Honeywell In-Space Accelerometer, a small three-axis accelerometer that was hard-mounted onto the Fluid Experiment Apparatus to record the microgravity environment at the exact location of the MDE. Data were recorded during specific mission events such as Orbiter quiescent periods, crew exercise on the treadmill, and numerous Orbiter engine burns. Orbiter background levels were measured to be in the 3 x 10(exp -5) to 2 x 10(exp -4) G range, treadmill operations in the 6 x 10(exp -4) to 5 x 10(exp -3) G range, and Orbiter engine burns from 4 x 10(exp -3) to in excess of 1 x 10(exp -2) G. These data represent some of the first microgravity accelerometer data ever recorded in the middeck area of the Orbiter.

Dunbar, Bonnie J.↗
NASA NTRS1992

Solar cell arcing: The role of outgassing and contamination

The effect of outgassing, venting, and thruster firing events on spacecraft system performance has been a long standing issue. Recent laboratory measurements on negatively biased high voltage solar cells at Physical Sciences Inc. (PSI) suggest that some currently designed and certainly future space power systems must address/re-evaluate this issue. Our observations show that exposing these cells to moderate levels (10 exp -3 torr-min) of H2O vapor enhances the arcing frequency, while heating to 85 C to remove water vapor significantly reduces the arc frequency. The interaction of the adhesive used to attach the cover glass to the solar cell with ambient water vapor is the key factor in determining arcing rates. Elimination of adhesive exposed to the environmental plasma reduces the arc frequency more than two orders of magnitude, and eliminates any sensitivity to H2O exposure. The adhesive may also become a source of spacecraft contamination. Macroscopic amounts were observed to blow off some arc events, and (we assume) electrostatically precipitate at other negatively biased locations. Data, analysis, and potential impact for future space platforms are discussed.

Marinelli, W. J.↗
NASA NTRS1992

Coma imaging of comet P/Brorsen-Metcalf at Calar Alto in late July to mid August 1989

Comet P/Brorsen-Metcalf was observed on 1989/07/28+30 and on 1989/08/04+12(+14) with the 3.5 m telescope and the 0.8 m Schmidt camera at Calar Alto/Spain. The images exhibit a narrow plasma tail pointing into anti-solar direction. On 1989/07/30 a triple tail was found which can be interpreted as tail ray event. The coma isophotes show prominent asymmetries with the nucleus located on the tailward side of the isophote foci and with a slightly higher brightness in the Northern Hemisphere of the coma. A strong curved jet feature was detected in the coma on 1989/07/30. The jet extended at least 30,000 km into the sunward coma hemisphere. The rotation period of about 1.3 days, estimated from the curvature of the coma jet, needs verification by other observations.

Boehnhardt, Hermann↗
NASA NTRS1993

Structured plasma sheet thinning observed by Galileo and 1984-129

On December 8, 1990, the Galileo spacecraft used the Earth for a gravity assist on its way to Jupiter. Its trajectory was such that it crossed geosynchronous orbit at approximately local midnight between 1900 and 2000 UT. At the same time, spacecraft 1984-129 was also located at geosynchronous orbit near local midnight. Several flux dropout events were observed when the two spacecraft were in the near-Earth plasma sheet in the same local time sector. Flux dropout events are associated with plasma sheet thinning in the near-profile of the near-Earth plasma sheet while 1984-129 provided an azimuthal profile. With measurements from these two spacecraft we can distinguish between spatial structures and temporal change. Our observations confirm that the geosynchronous flux dropout events are consistent with plasma sheet thinning which changes the spacecraft's magnetic connection from the trapping region to the more distant plasma sheet. However, for this period, thinning occurred on two spatial and temporal scales. The geosynchronous dropouts were highly localized phenomena of 30 min duration superimposed on a more global reconfiguration of the tail lasting approximately 4 hours.

Reeves, G. D.↗
NASA NTRS2000

Soil Moisture and Mesoscale Convective Complex Development During the 1993 US Midwest Flood: Results from the MM5-PLACE Atmosphere/Land-Surface Model

The 1993 US Midwest Flood produced record levels of flooding, in the Mississippi River Basin. This flooding resulted from repeated frontal passages and mesoscale convective complexes (MCCs) during the months of June and July. A better understanding of processes that influenced MCC development during the 1993 Flood may lead to improved forecasts of heavy precipitation and flooding. Here, we consider the impact of soil moisture on MCC development during a two-day period (June 23-24) of the 1993 US Midwest Flood. The purpose of this study is to assess the importance of soil moisture distribution on the timing, intensity, and location of heavy precipitation. In this study, the MM5-PLACE Atmosphere/Land-Surface Model is utilized. The atmospheric component consists of the Penn State/NCAR MM5 mesoscale model, and the land-surface component consists of the Goddard Parameterization for Land Atmosphere-Cloud Exchange (PLACE). Initial soil moisture is provided from two sources: 1) NCEP reanalysis, and 2) Antecedent Precipitation Index (API) using NOAA rain gauge measurements as a proxy for soil moisture. NCEP reanalysis provides coarse resolution initial soil moisture (2.5 degree), while API provides high resolution initial soil moisture (10-200 km depending on NOAA rain gauge spacing). Initial results indicate that the distribution of soil moisture has a significant impact on the timing and location of heavy precipitation during this two-day flood event. Precipitation in simulations with high resolution initial soil moisture agrees more closely with observed precipitation. These results suggest that high resolution soil moisture observations are necessary to accurately predict severe storm development, heavy precipitation, and subsequent flooding.

Baker, R. David↗
NASA NTRS2004

Calibration of the Galactic Cosmic Ray Flux

We report first Xe data on the cross-calibration of I-129-Xe-129(sub n) ages with conventional CRE ages, a method which is expected to provide information on the long-term constancy of the galactic cosmic ray (GCR) flux. We studied isotopic signatures of Xe released in stepwise heating, decomposition and melting of troilites in the Cape York iron meteorite to identify isotopic shifts in Xe-129 and Xe-131 due to neutron capture in Te-128 and Te-130. We also resolve components due to extinct 129I, spallation and fission Xe. There has recently been much speculation on the constancy of GCR over long time scales, as may be inferred from iron meteorites. If GCRs originate from supernova events, this provides the basis for postulating increased fluxes at locations with higher than average densities of supernovae, specifically in OB-associations. The solar system at present appears to be inside a local bubble between spiral arms and may experience an increased GCR flux.

Mathew, K. J.↗
NASA NTRS2009

Automatic Determination of the Conic Coronal Mass Ejection Model Parameters

Characterization of the three-dimensional structure of solar transients using incomplete plane of sky data is a difficult problem whose solutions have potential for societal benefit in terms of space weather applications. In this paper transients are characterized in three dimensions by means of conic coronal mass ejection (CME) approximation. A novel method for the automatic determination of cone model parameters from observed halo CMEs is introduced. The method uses both standard image processing techniques to extract the CME mass from white-light coronagraph images and a novel inversion routine providing the final cone parameters. A bootstrap technique is used to provide model parameter distributions. When combined with heliospheric modeling, the cone model parameter distributions will provide direct means for ensemble predictions of transient propagation in the heliosphere. An initial validation of the automatic method is carried by comparison to manually determined cone model parameters. It is shown using 14 halo CME events that there is reasonable agreement, especially between the heliocentric locations of the cones derived with the two methods. It is argued that both the heliocentric locations and the opening half-angles of the automatically determined cones may be more realistic than those obtained from the manual analysis

Pulkkinen, A.↗