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At least 667 records · Page 37

A new approach for measuring the carbon and oxygen content of atmospherically relevant compounds and mixtures

Abstract. Due to its complexity, gas- and particle-phase organic carbon in the atmosphere is often classified by its bulk physicochemical properties. However, there is a dearth of robust, moderate-cost approaches to measure the bulk chemical composition of organic carbon in the atmosphere. This is particularly true for the degree of oxygenation, which critically affects the properties and impacts of organic carbon but for which routine measurement approaches are lacking. This gap has limited the understanding of a wide range of atmospheric components, including particulate matter, the mass of which is monitored worldwide due to its health and environmental effects but the chemical characterization of which requires relatively high capital costs and complex operation by highly trained technical personnel. In this work, we demonstrate a new approach to estimate the mass of carbon and oxygen in analytes and mixtures that relies only on robust, moderate-cost detectors designed for use with gas chromatography. Organic compounds entering a flame ionization detector were found to be converted with approximately complete efficiency to CO2, which was analyzed downstream using an infrared detector to measure the mass of carbon analyzed. The ratio of the flame ionization detector (FID) signal generated to CO2 formed (FID∕CO2) was shown to be strongly correlated (R2=0.89) to the oxygen-to-carbon ratio (O∕C) of the analyte. Furthermore, simple mixtures of analytes behaved as the weighted average of their components, indicating that this correlation extends to mixtures. These properties were also observed to correlate well with the sensitivity of the FID estimated by structure activity relationships (quantified as the relative effective carbon number). The relationships between measured FID∕CO2, analyte O∕C, and FID sensitivity allow the estimation of one property from another with <15 % error for mixtures and <20 % error for most individual analytes. The approach opens the possibility of field-deployable, autonomous measurement of the carbon and oxygen content of particulate matter using time-tested, low-maintenance detectors, though such an application would require some additional testing on complex mixtures. With some instrumental modifications, similar measurements on gas-phase species may be feasible. Moreover, the potential expansion to additional gas chromatography detectors may provide concurrent measurement of other elements (e.g., sulfur, nitrogen).

42 ENGINEERING↗

Evaluation of 3D pixel silicon sensors for the CMS Phase-2 Inner Tracker

The high-luminosity upgrade of the CERN LHC requires the replacement of the CMS tracking detector to cope with the increased radiation fluence while maintaining its excellent performance. An extensive R&D program, aiming at using 3D pixel silicon sensors in the innermost barrel layer of the detector, has been carried out by CMS in collaboration with the FBK (Trento, Italy) and CNM (Barcelona, Spain) foundries. The sensors will feature a pixel cell size of 25 × 100 µm 2 , with a centrally located electrode connected to the readout chip. The sensors are read out by the RD53A and CROCv1 chips, developed in 65 nm CMOS technology by the RD53 Collaboration, a joint effort between the ATLAS and CMS groups. This paper reports the results achieved in beam test experiments before and after irradiation, up to a fluence of approximately 2 . 6 × 1 0 16 n eq /cm 2 . Measurements of assemblies irradiated to a fluence of 1 × 10 16 n˙eq/cm 2 show a hit detection efficiency higher than 96% at normal incidence, with fewer than 2% of channels masked, across a bias voltage range greater than 50 V . Even after irradiation to a higher fluence of 1.6 × 10 16 n˙eq/cm 2 , similar performance is maintained over a bias voltage range of 30 V , remaining well within CMS requirements.

3D pixel↗

Production of muonic kaon atoms at high-energy colliders

We develop a framework for the formation of exotic muonic kaon atoms ($K\mu$) in semileptonic $D^{0}$ decays, using the effective weak Hamiltonian, a helicity-based treatment of the leptonic current, and a nonrelativistic bound-state projection. The resulting branching ratio, $\mathrm{BR}(D^{0}\!\to(K\mu )\nu_{\mu})=2.29\times10^{-10}$, is implemented in a ROOT-based code to estimate yields at RHIC, LHC, and STCF. We show quantitatively that $K\mu$ atoms—also produced through coalescence in the quark--gluon plasma (QGP)—provide a sensitive probe of low-momentum primordial muons and early-time electromagnetic radiation, offering complementary constraints in an otherwise unexplored phase space for thermal dilepton and photon emission. Newly estimated dissociation cross sections in detector material indicate that secondary‑vertex reconstruction should be experimentally feasible, allowing clean experimental identification of the atoms. Projected yields from QGP coalescence in LHC and RHIC heavy-ion collisions, and from $D^{0}$ decays in LHC high-luminosity $p+p$ collisions indicate that the first observation of $K\mu$ atoms is within reach. Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI. Article funded by SCOAP3 and published under licence by Chinese Physical Society and the Institute of High Energy Physics of the Chinese Academy of Science and the Institute of Modern Physics of the Chinese Academy of Sciences and IOP Publishing Ltd.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

Measurement of directed flow in Au + Au collisions at $\sqrt{s{NN}}$ = 19.6 and 27 GeV with the STAR event plane detector

In heavy-ion collision experiments, the global collectivity of final-state particles can be quantified by anisotropic flow coefficients (𝑣 𝑛 ) . The first-order flow coefficient, also referred to as the directed flow (𝑣 1 ), describes the collective sideward motion of produced particles and nuclear fragments in heavy-ion collisions. It carries information on the very early stage of the collision, especially at large pseudorapidity (𝜂), where it is believed to be generated during the nuclear passage time. Directed flow therefore probes the onset of bulk collective dynamics during thermalization, providing valuable experimental guidance to models of the pre-equilibrium stage. In 2018, the Event Plane Detector (EPD) was installed in STAR and used for the Beam Energy Scan phase-II (BES-II) data taking. The combination of EPD (2.1 < |𝜂| < 5.1) and high-statistics BES-II data enables us to extend the 𝑣 1 measurement to the forward and backward 𝜂 regions. In this paper, we present the measurement of 𝑣 1 over a wide 𝜂 range in Au + Au collisions at $\sqrt{s_{NN}}$ = 19.6 and 27 GeV using the STAR EPD. The results of the analysis at $\sqrt{s_{NN}}$ = 19.6 GeV exhibit excellent consistency with the previous PHOBOS measurement, while elevating the precision of the overall measurement. The increased precision of the measurement also revealed finer structures in heavy-ion collisions, including a potential observation of the first-order event-plane decorrelation. Multiple physics models were compared to the experimental results. Only a transport model and a three-fluid hybrid model can reproduce a sizable 𝑣 1 at large 𝜂 as was observed experimentally. The model comparison also indicates 𝑣 1 at large 𝜂 might be sensitive to the QGP phase transition.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

TomoTwin: A simple digital twin for synchrotron tomography

A digital twin for synchrotron-based tomography for generating synthetic datasets from ground-truth phantoms. The code outputs greyscale projection images / tomographic volumes with realistic artifacts such as noise and phase-contrast and emulates their dependence on the acquisition parameters defining the beam and detector configuration. Some ground-truth phantoms are included with the code.

TEKAWADE, ANIKET↗

Nonlocal subpicosecond delay metrology using spectral quantum interference

Precise knowledge of position and timing information is critical to support elementary protocols such as entanglement swapping on quantum networks. While approaches have been devised to use quantum light for such metrology, they largely rely on time-of-flight (ToF) measurements with single-photon detectors and, therefore, are limited to picosecond-scale resolution owing to detector jitter. In this work, we demonstrate an approach to distributed sensing that leverages phase modulation to map changes in the spectral phase to coincidence probability, thereby overcoming the limits imposed by single-photon detection. By extracting information about the joint biphoton phase, we measure a generalized delay—the difference in signal–idler arrival, relative to local radio frequency (RF) phase modulation. For nonlocal ranging measurements, we achieve (2$σ$) precision of ±0.04 ps and for measurements of the relative RF phase, (2$σ$) precision of ±0.7°. We complement this fine timing information with ToF data from single-photon time-tagging to demonstrate absolute measurement of time delay. By relying on off-the-shelf telecommunications equipment and standard quantum resources, this approach has the potential to reduce overhead in practical quantum networks.

42 ENGINEERING↗

Circuit suppresses spurious sidebands

Circuitry requires modulated subcarrier to be split, part going to a phase modulator, and part going to a new circuit which utilizes a square law detector, a balanced mixer, and an amplifier to remove spurious sidebands. A summer recombines the two outputs, and final signal no longer includes spures.

Ready, P. J.↗

All-digital phase-lock loops for noise-free signals

Bit-synchronizers utilize all-digital phase-lock loops that are referenced to a high frequency digital clock. Phase-lock loop of first design acquires frequency within nominal range and tracks phase; second design is modified for random binary data by addition of simple transition detector; and third design acquires frequency over wide dynamic range.

Anderson, T. O.↗

Evidence that pitch angle scattering is an important loss mechanism for energetic electrons in the inner radiation belt of Jupiter

Analysis of data from the Pioneer 10 flyby discloses that pitch angle scattering plays an important part in determining the distribution of energetic electrons in the inner magnetosphere of Jupiter. Angular distributions measured by a Cerenkov detector reveal that redistribution takes place in pitch angle. Additionally, the radial profile of phase space density along the equator demands simultaneous particle losses. The loss rates are too high to be accounted for by synchrotron radiation loss, but are reasonably attributed to pitch angle scattering into the planetary loss cone.

Fillius, W.↗

Deferred electronic heterodyne moire deflectometry: A method for transient density fields measurement

Effects of spherical aberrations of the mirror used in the moire system on the angular resolution of the system are investigated. It is shown that the spherical aberrations may reduce significantly the performance of the conventional moire deflectometer. However, due to the heterodyne procedure, this is not the case with the heterodyne moire system. A moire system with a constant speed moving grating is demonstrated. It is shown that the system readout is linear and the system does not need calibration. In addition, the repeatability of the measurements is improved in this system as compared to the sinusoidally moving grating setup. The problem of the photographic plates alignment is solved by using a mechanical system in which the plate is held firmly throughout the experiment and accurately replaced after removing for photographic processing. The effect of a circular detector's aperture size on readout was tested. It is shown that the spatial phase variations, observed when scanning along a straight moire fringe, may considerably be reduced. At present we may say that both the on-line and the deferred heterodyne moire techniques may reliably be used. The errors of phase readings are 1 deg and 5 deg for the on-line and deferred methods. The total error due to subtraction of two readings at each position is, therefore, 1.4 deg and 7 deg, respectively. Further research for improving the deferred system is suggested.

Stricker, Josef↗

Ion flux oscillations associated with a radially polarized transverse Pc 5 magnetic pulsation

The AMPTE CCE spacecraft observed a transverse Pc 5 magnetic pulsation (period of about 200 s) at 2155-2310 UT on November 20, 1985, at a radial distance of 5.7 - 7.0 earth radii, at a magnetic latitude of 1.2 - 19 deg, and near 1300 magnetic local time. The magnetic pulsation exhibits properties consistent with a standing Alfven wave with a second-harmonic standing structure along the ambient magnetic field. The amplitude and the phase of the flux pulsation are found to be a function of the particle detector look direction and the particle energy. The observed energy dependence of the shift is interpreted as the result of a drift-bounce resonance of the ions with the wave. From this interpretation it follows that the wave propagated westward with an azimuthal wave number of approximately 100. Thus the study demonstrates that particle data can be useful for determining the spatial structure of some types of ULF waves.

Takahashi, K.↗

Surface roughness measurements

The Optics Division is currently in the research phase of producing grazing-incidence mirrors to be used in x-ray detector applications. The traditional method of construction involves labor-intensive glass grinding. This also culminates in a relatively heavy mirror. For lower resolution applications, the mirrors may be of a replicated design which involves milling a mandrel as a negative of the final shape and electroplating the cylindrical mirror onto it. The mirror is then separated from the mandrel by cooling. The mandrel will shrink more than the 'shell' (mirror) allowing it to be pulled from the mandrel. Ulmer (2) describes this technique and its variations in more detail. To date, several mirrors have been tested at MSFC by the Optical Fabrication Branch by focusing x-ray energy onto a detector with limited success. Little is known about the surface roughness of the actual mirror. Hence, the attempt to gather data on these surfaces. The test involves profiling the surface of a sample, replicating the surface as described above, and then profiling the replicated surface.

Howard, Thomas G.↗

Small Vocabulary Recognition Using Surface Electromyography in an Acoustically Harsh Environment

This paper presents results of electromyographic-based (EMG-based) speech recognition on a small vocabulary of 15 English words. The work was motivated in part by a desire to mitigate the effects of high acoustic noise on speech intelligibility in communication systems used by first responders. Both an off-line and a real-time system were constructed. Data were collected from a single male subject wearing a fireghter's self-contained breathing apparatus. A single channel of EMG data was used, collected via surface sensors at a rate of 104 samples/s. The signal processing core consisted of an activity detector, a feature extractor, and a neural network classifier. In the off-line phase, 150 examples of each word were collected from the subject. Generalization testing, conducted using bootstrapping, produced an overall average correct classification rate on the 15 words of 74%, with a 95% confidence interval of [71%, 77%]. Once the classifier was trained, the subject used the real-time system to communicate and to control a robotic device. The real-time system was tested with the subject exposed to an ambient noise level of approximately 95 decibels.

Betts, Bradley J.↗

LWIR detector research in InAsSb/InAs

The InAsSb/InSb strained-layer system forms a type-II superlattice in the Sb-rich region of the phase diagram. The band gap of InAsSb/InSb strained-layer superlattices grown on lattice-matched buffers can be varied continuously to produce semiconducting systems with band gaps ranging from that of InSb (0.23 eV with an absorption edge at 5.5 microns at 77 K) to 0. The semiconductor to semimetal transition occurs at As concentrations of approximately 33 percent, with the precise value dependent upon the strain and quantum well dimensions. At higher As content, the system is a semimetal. The authors fabricated photovoltaic detectors with high D asterisk at 77 K at wavelengths beyond 10 microns, and both photovoltaic and photoconductive detectors have been demonstrated with response to 15 microns. The photoconductive detectors exhibit gain of up to 100. Details of the materials growth, studies of the band structure and properties, device processing and the detector performance observed to date in these systems are discussed.

Peercy, Paul S.↗

Implementing a Digital Phasemeter in an FPGA

Firmware for implementing a digital phasemeter within a field-programmable gate array (FPGA) has been devised. In the original application of this firmware, the phase that one seeks to measure is the difference between the phases of two nominally-equal-frequency heterodyne signals generated by two interferometers. In that application, zero-crossing detectors convert the heterodyne signals to trains of rectangular pulses, the two pulse trains are fed to a fringe counter (the major part of the phasemeter) controlled by a clock signal having a frequency greater than the heterodyne frequency, and the fringe counter computes a time-averaged estimate of the difference between the phases of the two pulse trains. The firmware also does the following: Causes the FPGA to compute the frequencies of the input signals; Causes the FPGA to implement an Ethernet (or equivalent) transmitter for readout of phase and frequency values; and Provides data for use in diagnosis of communication failures. The readout rate can be set, by programming, to a value between 250 Hz and 1 kHz. Network addresses can be programmed by the user.

Rao, Shanti R.↗

NOvA in 10 Minutes

NOvA is a long-baseline neutrino oscillation experiment that utilizes the NuMI beamline at Fermilab. The experiment consists of two functionally identical, segmented liquid scintillator detectors. A 300-ton near detector sits at Fermilab, while a 14-kiloton far detector is located 810 km away in Ash River, Minnesota. Both are situated 14.6 mrad off the beam axis to peak the neutrino energy spectrum near the first oscillation maximum. NOvA measures muon neutrino disappearance and electron neutrino appearance in both neutrino and antineutrino beam modes, providing sensitivity to the neutrino mass ordering, the octant of the atmospheric mixing angle \theta_{23}, and the CP-violating phase \delta_{CP}. In this talk, I will give a concise overview of the NOvA experiment and its detectors, followed by highlights from recent oscillation analyses. I will also highlight notable cross-section measurements at the near detector. Finally, I will briefly introduce ongoing analyses beyond the standard three-flavor oscillation framework, including searches for sterile neutrinos and non-standard interactions, as well as exotic signatures such as magnetic monopoles, light dark matter, neutrino magnetic moments, and cosmic-ray muon studies.

Khanam, Aklima [Syracuse U. (main)] (ORCID:0009000↗

How the discovery of Cold Noise delayed the production of ATLAS ITk strip tracker modules by a year

Here, the construction of the ATLAS strip tracker barrel will require the assembly of 12,000 barrel detector modules over the course of 3.5 years. In 2022, during the module pre-production phase, modules were found to display clusters of noisy channels outside required specifications when tested at operating temperatures (-35°C), called “Cold Noise”. Extensive investigations into the cause and mechanism of Cold Noise interrupted pre-production and occupied most barrel module assembly sites. This contribution presents an overview of the year-long investigations into Cold Noise, the final identification of the underlying mechanism and necessary changes for the transition to production.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

X-Ray Polarization Capabilities of a Small Explorer Mission

X-ray polarization measurements hold great promise for studying the geometry and emission mechanisms in the strong gravitational and magnetic fields that surround black holes and neutron stars. In spite of this, the observational situation remains very limited; the last instrument dedicated to X-ray polarimetry flew decades ago on OSO-8, and the few recent measurements have been made by instruments optimized for other purposes. However, the technical capabilities to greatly advance the observational situation are in hand. Recent developments in micro-pattern gas detectors allow use of the polarization sensitivity of the photo-electric effect, which is the dominant interaction in the band above 2 keV. We present the scientific and technical requirements for an X-ray polarization observatory consistent with the scope of a NASA Small Explorer (SMEX) mission, along with a representative catalog of what the observational capabilities and expected sensitivities for the first year of operation could be. The mission is based on the technically robust design of the Gravity and Extreme Magnetism SMEX (GEMS) which completed a Phase B study and Preliminary Design Review in 2012. The GEMS mission is enabled by time projection detectors sensitive to the photo-electric effect. Prototype detectors have been designed, and provide engineering and performance data which support the mission design. The detectors are further characterized by low background, modest spectral resolution, and sub-millisecond timing resolution. The mission also incorporates high efficiency grazing incidence X-ray mirrors, design features that reduce systematic errors (identical telescopes at different azimuthal angles with respect to the look axis, and mounted on a rotating spacecraft platform), and a moderate capability to perform Target of Opportunity observations. The mission operates autonomously in a low earth, low inclination orbit with one to ten downlinks per day and one or more uplinks per week. Data and calibration products will be made available through the High Energy Astrophysics Science and Archival Research Center (HEASARC).

GEMS↗