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At least 667 records · Page 37

Deep crustal deformation by sheath folding in the Adirondack Mountains, USA

As described by McLelland and Isachsen, the southern half of the Adirondacks are underlain by major isoclinal (F sub 1) and open-upright (F sub 2) folds whose axes are parallel, trend approximately E-W, and plunge gently about the horizontal. These large structures are themselves folded by open upright folds trending NNE (F sub 3). It is pointed out that elongation lineations in these rocks are parallel to X of the finite strain ellipsoid developed during progressive rotational strain. The parallelism between F sub 1 and F sub 2 fold axes and elongation lineations led to the hypothesis that progressive rotational strain, with a west-directed tectonic transport, rotated earlier F sub 1-folds into parallelism with the evolving elongation lineation. Rotation is accomplished by ductile, passive flow of F sub 1-axes into extremely arcuate, E-W hinges. In order to test these hypotheses a number of large folds were mapped in the eastern Adirondacks. Other evidence supporting the existence of sheath folds in the Adirondacks is the presence, on a map scale, of synforms whose limbs pass through the vertical and into antiforms. This type of outcrop pattern is best explained by intersecting a horizontal plane with the double curvature of sheath folds. It is proposed that sheath folding is a common response of hot, ductile rocks to rotational strain at deep crustal levels. The recognition of sheath folds in the Adirondacks reconciles the E-W orientation of fold axes with an E-W elongation lineation.

Mclelland, J. M.↗

Potential for NiAl based alloys for high temperature applications

The B2 nickel aluminide, NiAl, is of potential use for high temperature structural applications because of its high melting point, low density, and oxidation resistance. An overview of recent attempts to improve the low temperature ductility as well as the high temperature strength of this alloy is presented. Room temperature tensile ductility of 2.5 percent can be obtained in a stoichiometric binary alloy by careful control of the composition and processing conditions. Alloying additions to improve high temperature creep resistance are most effective when fine distributions of ternary intermetallic phases can be obtained. A promising direction for exploiting the advantages of this alloy may be as a matrix for composite materials.

Vedula, K.↗

The effects of hydrogen embrittlement of titanium

Titanium alloys, by virtue of their attractive strength to density ratio, fatigue, fracture toughness and corrosion resistance are now commonly used in various aerospace and marine applications. The cost, once very expensive, has been reduced, making titanium even more of a competitive material today. Titanium and titanium alloys have a great affinity to several elements. Hydrogen, even in small amounts, can cause embrittlement, which in turn causes a reduction in strength and ductility. The reduction of strength and ductility is the subject of this investigation.

Taylor, Delbert J.↗

A study of hydrogen environment effects on microstructure property behavior of NASA-23 alloy and related alloy systems

This work is part of the overall advanced main combustion chamber (AMCC) casting characterization program of the Materials and Processes Laboratory of the Marshall Space Flight Center. The influence of hydrogen on the tensile properties and ductility behavior of NASA-23 alloy were analyzed. NASA-23 and other referenced alloys in cast and hipped conditions were solution treated and aged under selected conditions and characterized using optical metallography, scanning electron microscopy, and electron microprobe analysis techniques. The yield strength of NASA-23 is not affected much by hydrogen under tensile tests carried at 5000 psig conditions; however, the ultimate strength and ductility properties are degraded. This implies that the physical mechanisms operating would be related to the plastic deformation process. The fracture surfaces characteristics of NASA-23 specimens tensile tested in hydrogen, helium, and air were also analyzed. These revealed surface cracks around specimen periphery with the fracture surface showing a combination of intergranular and transgranular modes of fracture. It is seen that the specimens charged in hydrogen seem to favor a more brittle fracture mode in comparison to air and helium charged specimens. The AMCC casting characterization program is to be analyzed for their hydrogen behavior. As a result of this program, the basic microstructural factors and fracture characteristics in some cases were analyzed.

Diwan, Ravinder M.↗

Tensile and fatigue behavior of tungsten/copper composites

Work on W/Cu unidirectional composites was initiated to study the behavior of this ductile-ductile composite system under thermomechanical fatigue and to examine the applicability of fatigue-life prediction methods for thermomechanical fatigue of this metal matrix composite. The first step was to characterize the tensile behavior of four ply, 10 vol. percent W/Cu plates at room and elevated temperatures. Fatigue tests were conducted in load control on 0 degree specimens at 260 C. The maximum cyclic stress was varied but the minimum cyclic stress was kept constant. All tests were performed in vacuum. The strain at failure increased with increasing maximum cyclic stress.

Verrilli, Michael J.↗

Microstructural evolution during aging of an Al-Cu-Li-Ag-Mg-Zr alloy

Alloys in the Al-Cu-Li Ag-Mg subsystem were developed that exhibit desirable combinations of strength and ductility. These Weldalite (trademark) alloys, are unique for Al-Cu-Li alloys in that with or without a prior cold stretching operation, they obtain excellent strength-ductility combinations upon natural and artificial aging. This is significant because it enables complex, near-net shape products such as forgings and super plastically formed parts to be heat treated to ultra-high strengths. On the other hand, commercial extrusions, rolled plates and sheets of other Al-Cu-Li alloys are typically subjected to a cold stretching operation before artificial aging to the highest strength tempers to introduce dislocations that provide low-energy nucleation sites for strengthening precipitates such as the T(sub 1) phase. The variation in yield strength (YS) with Li content in the near-peak aged condition for these Weldalite (trademark) alloys and the associated microstructures were examined, and the results are discussed.

Kumar, K. S.↗

Mechanical characterization and modeling of non-linear deformation and fracture of a fiber reinforced metal matrix composite

The nonlinear anisotropic mechanical behavior of an aluminum alloy metal matrix composite reinforced with continuous alumina fibers was determined experimentally. The mechanical behavior of the composite were modeled by assuming that the composite has a periodical microstructure. The resulting unit cell problem was solved with the finite element method. Excellent agreement was found between theoretically predicted and measured stress-strain responses for various tensile and shear loadings. The stress-strain responses for transverse and inplane shear were found to be identical and this will provide a simplification of the constitutive equations for the composite. The composite has a very low ductility in transverse tension and a limited ductility in transverse shear that was correlated to high hydrostatic stresses that develop in the matrix. The shape of the initial yield surface was calculated and good agreement was found between the calculated shape and the experimentally determined shape.

Jansson, S.↗

The role of the gamma/gamma-prime eutectic and porosity on the tensile behavior of a single-crystal nickel-base superalloy

The microstructure of a single-crystal nickel-base superalloy, PWA 1480, has been varied by heat treatment and hot isostatic pressing in order to study the role of the gamma/gamma-prime eutectic and porosity on subsequent tensile behavior. The level of porosity was found not to affect any of the tensile properties, while the gamma/gamma-prime eutectic strongly influenced ductility. Eliminating the gamma/gamma-prime eutectic increased ductility which was attributed to the cleavage fracture of this constituent. It is proposed that such cleavage of the gamma/gamma-prime eutectic is initiated by the stress created from impinging slip bands, promoting shear localization, and final fracture along 111 slip planes. The precise nature of this fracture process is discussed, with emphasis on the role of the gamma/gamma-prime microstructure. The deformation structure of PWA 1480 was also studied, and while different in some respects from many other single-crystal superalloys, its fracture process appears to be similar.

Walston, W. S.↗

The influence of chromium on structure and mechanical properties of B2 nickel aluminide alloys

Major obstacles to the use of NiAl-based alloys and composites are low ductility and toughness. These shortcomings result in part from a lack of sufficient slip systems to accommodate plastic deformation of polycrystalline material (von Mises Criterion). It has been reported that minor additions of chromium to polycrystalline NiAl cause the predominant slip system to shift from the usual. If true, then a major step toward increasing ductility in this compound may be realized. The purpose of the present study was to verify this phenomenon, characterize it with respect to chromium level and Ni to Al ratio, and correlate any change in slip system with microstructure and mechanical properties. Compression and tensile specimens were prepared from alloys containing 0 to 5 percent chromium and 45 to 55 percent aluminum. Following about one percent strain, transmission electron microscopy foils were produced and the slip systems determined using the g x b = 0 invisibility criterion. Contrary to previous results, chromium was found to have no effect on the preferred slip system of any of the alloys studied. Possible reasons for the inconsistency of the current results with previous work are considered. Composition-structure-property relationships are discerned for the alloys, and good correlation are demonstrated in terms of conventional strengthening models for metallic systems.

Cotton, James Dean↗

Composites of low-density trialuminides: Particulate and long fiber reinforcements

An examination of the ternary L1(sub 2) trialuminides, Al66Ti25Mn9, Al67Ti25Cr8, and Al22Ti8Fe3 in compression, bending, and tension revealed that none of these compounds exhibited a desirable balance of strength, ductility, and oxidation resistance. Subsequently, specific quaternary and quinary compositions were cast, homogenized, and isothermally forged. Both, the monolithic material and its particulate reinforced counterparts were examined in compression, three point bend, and tension as a function of temperature, and at high temperatures as a function of strain rate. An alternate approach that was examined in this program to enhance the low temperature damage tolerance of these materials was to incorporate long refractory metal wires in the matrix. In summary, it appears that of the various matrix compositions examined, ternary Al66Ti25Mn9 exhibits the best balance in strength, ductility, and oxidation resistance. Although the idea of refractory metal wire reinforcement is an attractive one, a successful combination remains to be identified.

Kumar, K. S.↗

The effect of matrix mechanical properties on (0)8 unidirectional SiC/Ti composite fatigue resistance

The relationship between constituent and MMC properties in fatigue loading is investigated with low-cycle fatigue-resistance testing of an alloy Ti-15-3 matrix reinforced with SiC SCS-6 fibers. The fabrication of the composite is described, and specimens are generated that are weak and ductile (WD), strong and moderately ductile (SM), or strong and brittle (SB). Strain is measured during MMC fatigue tests at a constant load amplitude with a load-controlled waveform and during matrix-alloy fatigue tests at a constant strain amplitude using a strain-controlled waveform. The fatigue resistance of the (0)8 SiC/Ti-15-3 composite is found to be slightly influenced by matrix mechanical properties, and the composite- and matrix-alloy fatigue lives are not correlated. This finding is suggested to relate to the different crack-initiation and -growth processes in MMCs and matrix alloys.

Gabb, T. P.↗

The Mechanical Properties of a Ni-30Al-20Fe-0.05Zr Intermetallic Alloy in the Temperature Range 300-1200 K

Tensile tests were conducted on an extruded Ni-30(at. pct)Al-20Fe-0.05Zr intermetallic alloy in the temperature range 300-1200 K, and the microstructures were characterized by optical, scanning, and transmission electron microscopy. The alloy did not exhibit any room temperature ductility and failed by transgranular cleavage at a stress of about 710 MPa. This mode of fracture was observed at and below 873 K with the total ductility being less than 2.5 percent. However, the failure mode changed to dimpled fracture, triple point cracking, and rupture above 873 K. Scanning electron microscopy of the fracture surfaces revealed that transgranular cleavage failure had always originated at preexisting defects. In these cases, the fracture stress exhibited a good correlation with the defect size, in accordance with linear elastic fracture mechanics, where the critical stress intensity factor was estimated to be about 4 MPa sq rt m.

Raj, S. V.↗

Fracture behavior of a B2 Ni-30Al-20Fe-0.05Zr intermetallic alloy in the temperature range 300 to 1300 K

The fracture behavior of a B2 Ni-30Al-20Fe-0.05Zr (at. pct) alloy was investigated using results of tensile tests conducted in the temperature range 300-1300 K under initial strain rates that varied between 10 exp -6 and 10 exp -3/sec, together with results of deformation measurements reported by Raj et al. (1992). Microstructural observations revealed that the alloy had failed by transgranular cleavage fracture below 873 K and by ductile fracture, power-law cavitation, triple point cracking, and rupture above this temperautre. The fracture map constructed using fracture results is compared with those for other classes of materials, showing that the atomic bonding plays a significant role in the low-temperature ductility of NiAl-based alloys.

Raj, S. V.↗

Deformation behavior of a Ni-30Al-20Fe-0.05Zr intermetallic alloy in the temperature range 300 to 1300 K

The deformation properties of an extruded Ni-30Al-20Fe-0.05Zr (at. pct) alloy in the temperature range 300-1300 K were investigated under initial tensile strain rates that varied between 10 exp -6 and 10 exp -3/sec and in constant load compression creep between 1073 and 1300 K. Three deformation regimes were observed: region I, occurring between 400 and 673 K, which consisted of an athermal regime of less than 0.3 percent tensile ductility; region II, between 673 and 1073, where exponential creep was dominant; and region III, between 1073 and 1300 K, where a significant improvement in tensile ductility was observed.

Raj, S. V.↗

Tensile behavior of the L(1)2 compound Al67Ti25Cr8

Temperature-related variations in tensile yield strength and ductility were studied on cast, homogenized and isothermally forged Al67Ti25Cr8. Yield strength dropped discontinuously between 623 K and 773 K and then decreased gradually with increasing temperature. Below 623 K, fracture occurred prior to macroscopic yielding. Ductility decreased from 0.2 percent at 623 K to zero at 773 K, but increased again at higher temperatures. At 1073 K, an elongation of 19 percent was obtainable, and ultimate tensile strength and localized necking were observed. Fracture surfaces and deformed microstructures were examined. The 1073 K tensile specimen that exhibited 19 percent elongation showed grain boundary serrations and some evidence of recrystallization (likely dynamic) although fracture occurred predominantly via an intergranular mode.

Kumar, K. S.↗

Rheology of water-silicate mixtures at low temperatures

Lab studies of the effects of hard particulates on the rheology of ice have been mainly directed at the evolution of the Galilean satellites, but yield results that may be applicable to the rheology of the Martian polar caps. The experiments have explored the ductile rheology as well as brittle behavior of water + particulate (mainly quartz) mixtures in particulate volume fractions ranging from 0.001 to 0.56, particulate sizes 1 to 150 microns, temperatures 77 to 224 K, and deformation rates 3.5 x 10(exp -7) to 3.5 x 10(exp -4)/s, under confining pressures of 50 to 100 MPa. Particulates act mainly to strengthen the material in the ductile field, although work by others has shown that very close to the melting temperature hard particulates can actually cause softening. So called dispersion hardening by the Orowan mechanism of pinning glide dislocations, often exploited in metallurgy for strengthening materials, appears not to be an issue in ice except at very low temperatures, less than approx. 135 K.

Durham, William B.↗

Low cycle fatigue behavior of polycrystalline NiAl at 300 and 1000 K

The low cycle fatigue behavior of polycrystalline NiAl was determined at 300 and 1000 K - temperatures below and above the brittle- to-ductile transition temperature (BDTT). Fully reversed, plastic strain-controlled fatigue tests were conducted on two differently fabricated alloy samples: hot isostatically pressed (HIP'ed) prealloyed powder and hot extruded castings. HIP'ed powder (HP) samples were tested only at 1000 K, whereas the more ductile cast-and-extruded (C+E) NiAl samples were tested at both 1000 and 300 K. Plastic strain ranges of 0.06 to 0.2 percent were used. The C+E NiAl cyclically hardened until fracture, reaching stress levels approximately 60 percent greater than the ultimate tensile strength of the alloy. Compared on a strain basis, NiAl had a much longer fatigue life than other B2 ordered compounds in which fracture initiated at processing-related defects. These defects controlled fatigue life at 300 K, with fracture occurring rapidly once a critical stress level was reached. At 1000 K, above the BDTT, both the C+E and HP samples cyclically softened during most of the fatigue tests in air and were insensitive to processing defects. The processing method did not have a major effect on fatigue life; the lives of the HP samples were about a factor of three shorter than the C+E NiAl, but this was attributed to the lower stress response of the C+E material. The C+E NiAl underwent dynamic grain growth, whereas the HP material maintained a constant grain size during testing. In both materials, fatigue life was controlled by intergranular cavitation and creep processes, which led to fatigue crack growth that was primarily intergranular in nature. Final fracture by overload was transgranular in nature. Also, HP samples tested in vacuum had a life three times longer than their counterparts tested in air and, in contrast to those tested in air, hardened continuously over half of the sample life, thereby indicating an environmentally assisted fatigue damage mechanism. The C+E samples were tested only in air. At 1000 K, NiAl exhibited a superior fatigue life when compared to most superalloys on a plastic strain basis, but was inferior to most superalloys on a stress basis.

Lerch, Bradley A.↗

Room Temperature Cyclic Deformation Behavior of Cast and Extruded NiAl

The fully reversed, strain controlled fatigue behavior of cast and extruded NiAl was evaluated at room temperature for plastic strain ranges of 0.0006 to 0.0002 to provide baseline data on the fatigue life of NiAl and to investigate whether the low ductility of NiAl would result in poor low-cycle fatigue behavior. Except at the smallest plastic strain range investigated, NiAl work hardened continuously until failure with a final fracture stress under cyclic conditions which was at least 60 percent greater than the monotonic fracture strength of NiAl. Fatigue fracture initiation occurred at large internal tear-shaped pores, and fatigue life was controlled or limited by the presence of these processing-related defects. Even with the processing defects present in this material and the limited ductility of NiAl in general, cast and extruded NiAl exhibited much greater fatigue life at room temperature than comparable B2 ordered compounds when compared on a strain range basis.

Noebe, R. D.↗