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DOE OSTI2020

Structural response of α-quartz under plate-impact shock compression

Because of its far-reaching applications in geophysics and materials science, quartz has been one of the most extensively examined materials under dynamic compression. Despite 50 years of active research, questions remain concerning the structure and transformation of SiO 2 under shock compression. Continuum gas-gun studies have established that under shock loading quartz transforms through an assumed mixed-phase region to a dense high-pressure phase. While it has often been assumed that this high-pressure phase corresponds to the stishovite structure observed in static experiments, there have been no crystal structure data confirming this. In this study, we use gas-gun shock compression coupled with in situ synchrotron x-ray diffraction to interrogate the crystal structure of shock-compressed α-quartz up to 65 GPa. Our results reveal that α-quartz undergoes a phase transformation to a disordered metastable phase as opposed to crystalline stishovite or an amorphous structure, challenging long-standing assumptions about the dynamic response of this fundamental material.

58 GEOSCIENCES↗

DOE OSTI2019

Experimental investigation of the effect of compliant pores on reservoir rocks under hydrostatic and triaxial compression stress states

The presence of compliant pores in rocks is important for understanding the stress–strain behaviors under different stress conditions. This paper describes findings on the effect of compliant pores on the mechanical behavior of a reservoir sandstone under hydrostatic and triaxial compression. Laboratory experiments were conducted at reservoir temperature on Weber Sandstone samples from the Rock Springs Uplift, Wyoming. Each experiment was conducted at three sequential stages: (stage 1) increase in the confining pressure while maintaining the pore pressure, (stage 2) increase in the pore pressure while maintaining the confining pressure, and (stage 3) application of the deviatoric load to failure. The nonlinear pore pressure – volumetric strain relationship governed by compliant pores under low confining pressure changes to a linear behavior governed by stiff pores under higher confining pressure. The estimated compressibilities of the matrix material in sandstone samples are close to the typical compressibility of quartz. Because of the change in pore structures during stage 1 and stage 2 loadings, the estimated bulk compressibilities of the sandstone sample under the lowest confining pressure decrease with increasing differential pressure. The increase in crack initiation stress is limited with increasing differential pressure because of similar total crack length governed by initial compliant porosity in sandstone samples.

Engineering↗

DOE OSTI2017

Oxidation Behavior of Matrix Graphite and Its Effect on Compressive Strength

Matrix graphite (MG) with incompletely graphitized binder used in high-temperature gas-cooled reactors (HTGRs) is commonly suspected to exhibit lower oxidation resistance in air. In order to reveal the oxidation performance, the oxidation behavior of newly developed A3-3 MG at the temperature range from 500 to 950°C in air was studied and the effect of oxidation on the compressive strength of oxidized MG specimens was characterized. Results show that temperature has a significant influence on the oxidation behavior of MG. The transition temperature between Regimes I and II is ~700°C and the activation energy ( E a ) in Regime I is around 185 kJ/mol, a little lower than that of nuclear graphite, which indicates MG is more vulnerable to oxidation. Oxidation at 550°C causes more damage to compressive strength of MG than oxidation at 900°C. Comparing with the strength of pristine MG specimens, the rate of compressive strength loss is 77.3% after oxidation at 550°C and only 12.5% for oxidation at 900°C. Microstructure images of SEM and porosity measurement by Mercury Porosimetry indicate that the significant compressive strength loss of MG oxidized at 550°C may be attributed to both the uniform pore formation throughout the bulk and the preferential oxidation of the binder.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2023

Out of distribution evaluation for neural image compression

Official code for the NeurIPS 2023 paper "Neural Image Compression: Generalization, Robustness, and Spectral Biases". This code can be used to: - Computing spectral distortion errors of images compressed with traditional codes or neural image compression models (as proposed in the aformentioned paper) - Visualize power spectral densities and fourier heatmaps (as proposed in the aformentioned paper) - Train and test a variety of neural image compression models

Lieberman, KelseyA↗

DOE OSTI2024

A graphics processing unit accelerated sparse direct solver and preconditioner with block low rank compression

We present the GPU implementation efforts and challenges of the sparse solver package STRUMPACK. The code is made publicly available on github with a permissive BSD license. STRUMPACK implements an approximate multifrontal solver, a sparse LU factorization which makes use of compression methods to accelerate time to solution and reduce memory usage. Multiple compression schemes based on rank-structured and hierarchical matrix approximations are supported, including hierarchically semi-separable, hierarchically off-diagonal butterfly, and block low rank. Here, in this paper, we present the GPU implementation of the block low rank (BLR) compression method within a multifrontal solver. Our GPU implementation relies on highly optimized vendor libraries such as cuBLAS and cuSOLVER for NVIDIA GPUs, rocBLAS and rocSOLVER for AMD GPUs and the Intel oneAPI Math Kernel Library (oneMKL) for Intel GPUs. Additionally, we rely on external open source libraries such as SLATE (Software for Linear Algebra Targeting Exascale), MAGMA (Matrix Algebra on GPU and Multi-core Architectures), and KBLAS (KAUST BLAS). SLATE is used as a GPU-capable ScaLAPACK replacement. From MAGMA we use variable sized batched dense linear algebra operations such as GEMM, TRSM and LU with partial pivoting. KBLAS provides efficient (batched) low rank matrix compression for NVIDIA GPUs using an adaptive randomized sampling scheme. The resulting sparse solver and preconditioner runs on NVIDIA, AMD and Intel GPUs. Interfaces are available from PETSc, Trilinos and MFEM, or the solver can be used directly in user code. We report results for a range of benchmark applications, using the Perlmutter system from NERSC, Frontier from ORNL, and Aurora from ALCF. For a high frequency wave equation on a regular mesh, using 32 Perlmutter compute nodes, the factorization phase of the exact GPU solver is about 6.5× faster compared to the CPU-only solver. The BLR-enabled GPU solver is about 13.8× faster than the CPU exact solver. For a collection of SuiteSparse matrices, the STRUMPACK exact factorization on a single GPU is on average 1.9× faster than NVIDIA’s cuDSS solver.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2026

Spectral broadening and compression of picosecond pulses in air using a multi-pass cell

We report the spectral broadening and post-compression of picosecond pulses using a multi-pass cell (MPC) operating in air. A 2 m-long bi-concave cavity with 41 reflections and 96.4% transmission was designed and implemented, optimized for the compression of 5.5 ps, 4.5 mJ pulses from a Yb:YAG laser operating at 1030 nm. A 19.3-fold spectral broadening was obtained, increasing the bandwidth from 0.3 nm to 5.8 nm, which enabled pulse compression down to 547 fs with a symmetric temporal profile close to the transform limit. These results demonstrate the feasibility of using open-air MPCs for high-energy picosecond pulse post-compression, without the need for sealed chambers, while preserving high mode quality and transmission. Scaling to pulse higher energy is discussed.

Zaldivar Escola, F. [Univ. of Buenos Aires (Argent↗

DOE OSTI2021

Effect of additives on carbon dioxide uptake and compressive strength of dry-cast concrete

The main thrust of the work reported herein is to study the effect of chemical additives to make beneficial use of carbon dioxide in enhancing the compressive strength of dry-cast concrete. The additives used in this investigation were calcium and magnesium oxides and silicates, nickel oxide, sodium hydroxide, sodium bicarbonate and strontium chloride. The experimental results showed that both the carbonation reactions and the compressive strength of dry-cast concrete mixtures were improved when using chemical additives. Experimental investigations for optimisation were also undertaken with selected additives to further increase the carbon dioxide uptake and improve the compressive strength. The best results were obtained when using calcium silicate in combination with calcium oxide. The early-age compressive strength of specimens made from the optimised mixture increased from 9·82 MPa to 13·32 MPa, and the specimens’ carbon dioxide uptake increased from 8·76% to 10·62% of cement weight.

Construction & Building Technology↗

DOE OSTI2024

Proposal for a proton-bunch compression experiment at IOTA in the strong space-charge regime

The longitudinal compression of intense proton bunches with strong space-charge force is an essential component of a proton-based muon source for a muon collider. This paper discusses a proton-bunch compression experiment at the Integrable Optics Test Accelerator (IOTA) storage ring at Fermilab to explore optimal radio frequency (RF) cavity and lattice configurations. IOTA is a compact fixed-energy storage ring that can circulate a 2.5-MeV proton beam with varying beam parameters and lattice configurations. The study will aim to demonstrate a bunch-compression factor of at least 2 in the IOTA ring while examining the impact of intense space-charge effects on the compression process.

43 PARTICLE ACCELERATORS↗

DOE OSTI2014

Compression of 1-mm-thick M9763 cellular silicone foam under lateral confinement

M9763 cellular silicone foam disks (1 mm thick, 28.68 mm diameter, 63% nominal porosity) were compressed under lateral confinement using the Instron Electropuls E10000 load frame. Five (5) loadunload cycles up to 65% compressive strain were performed at a test speed of 1.26 mm/min. Stress vs. strain curves were obtained. Additional specimens were compressed without lateral confinement for comparison. The stress vs. strain curve of the confined specimen essentially overlapped that of the unconfined specimen until ~60% strain when it began to increase more rapidly, indicating lock-up (bulk compression) and the onset of lateral expansion of the unconfined specimen. The slope of the stress vs. strain curve was equal to the Young’s modulus of the solid M9787 material comprising the foam at ~50% strain, which is below the expected 63% lock-up strain. The reason for the discrepancy between the two estimates of lock-up strain is not clear.

42 ENGINEERING↗

DOE OSTI2014

Oil-free centrifugal hydrogen compression technology demonstration

One of the key elements in realizing a mature market for hydrogen vehicles is the deployment of a safe and efficient hydrogen production and delivery infrastructure on a scale that can compete economically with current fuels. The challenge, however, is that hydrogen, being the lightest and smallest of gases with a lower viscosity and density than natural gas, readily migrates through small spaces and is difficult to compresses efficiently. While efficient and cost effective compression technology is crucial to effective pipeline delivery of hydrogen, the compression methods used currently rely on oil lubricated positive displacement (PD) machines. PD compression technology is very costly, has poor reliability and durability, especially for components subjected to wear (e.g., valves, rider bands and piston rings) and contaminates hydrogen with lubricating fluid. Even so called “oil-free” machines use oil lubricants that migrate into and contaminate the gas path. Due to the poor reliability of PD compressors, current hydrogen producers often install duplicate units in order to maintain on-line times of 98-99%. Such machine redundancy adds substantially to system capital costs. As such, DOE deemed that low capital cost, reliable, efficient and oil-free advanced compressor technologies are needed. MiTi’s solution is a completely oil-free, multi-stage, high-speed, centrifugal compressor designed for flow capacity of 500,000 kg/day with a discharge pressure of 1200 psig. The design employs oil-free compliant foil bearings and seals to allow for very high operating speeds, totally contamination free operation, long life and reliability. This design meets the DOE’s performance targets and achieves an extremely aggressive, specific power metric of 0.48 kW-hr/kg and provides significant improvements in reliability/durability, energy efficiency, sealing and freedom from contamination. The multi-stage compressor system concept has been validated through full scale performance testing of a single stage with helium similitude gas at full speed in accordance with ASME PTC-10. The experimental results indicated that aerodynamic performance, with respect to compressor discharge pressure, flow, power and efficiency exceeded theoretical prediction. Dynamic testing of a simulated multistage centrifugal compressor was also completed under a parallel program to validate the integrity and viability of the system concept. The results give strong confidence in the feasibility of the multi-stage design for use in hydrogen gas transportation and delivery from production locations to point of use.

08 HYDROGEN↗

DOE OSTI2015

Implementing and diagnosing magnetic flux compression on the Z pulsed power accelerator

We report on the progress made to date for a Laboratory Directed Research and Development (LDRD) project aimed at diagnosing magnetic flux compression on the Z pulsed-power accelerator (0-20 MA in 100 ns). Each experiment consisted of an initially solid Be or Al liner (cylindrical tube), which was imploded using the Z accelerator's drive current (0-20 MA in 100 ns). The imploding liner compresses a 10-T axial seed field, B z ( 0 ) , supplied by an independently driven Helmholtz coil pair. Assuming perfect flux conservation, the axial field amplification should be well described by B z ( t ) = B z ( 0 ) x [ R ( 0 ) / R ( t )] 2 , where R is the liner's inner surface radius. With perfect flux conservation, B z ( t ) and dB z / dt values exceeding 10 4 T and 10 12 T/s, respectively, are expected. These large values, the diminishing liner volume, and the harsh environment on Z, make it particularly challenging to measure these fields. We report on our latest efforts to do so using three primary techniques: (1) micro B-dot probes to measure the fringe fields associated with flux compression, (2) streaked visible Zeeman absorption spectroscopy, and (3) fiber-based Faraday rotation. We also mention two new techniques that make use of the neutron diagnostics suite on Z. These techniques were not developed under this LDRD, but they could influence how we prioritize our efforts to diagnose magnetic flux compression on Z in the future. The first technique is based on the yield ratio of secondary DT to primary DD reactions. The second technique makes use of the secondary DT neutron time-of-flight energy spectra. Both of these techniques have been used successfully to infer the degree of magnetization at stagnation in fully integrated Magnetized Liner Inertial Fusion (MagLIF) experiments on Z [P. F. Schmit et al. , Phys. Rev. Lett. 113 , 155004 (2014); P. F. Knapp et al. , Phys. Plasmas, 22 , 056312 (2015)]. Finally, we present some recent developments for designing and fabricating novel micro B-dot probes to measure B z ( t ) inside of an imploding liner. In one approach, the micro B-dot loops were fabricated on a printed circuit board (PCB). The PCB was then soldered to off-the-shelf 0.020- inch-diameter semi-rigid coaxial cables, which were terminated with standard SMA connectors. These probes were recently tested using the COBRA pulsed power generator (0-1 MA in 100 ns) at Cornell University. In another approach, we are planning to use new multi-material 3D printing capabilities to fabricate novel micro B-dot packages. In the near future, we plan to 3D print these probes and then test them on the COBRA generator. With successful operation demonstrated at 1-MA, we will then make plans to use these probes on a 20-MA Z experiment.

47 OTHER INSTRUMENTATION↗

DOE OSTI2017

Metal Hydride Compression

Conventional hydrogen compressors often contribute over half of the cost of hydrogen stations, have poor reliability, and have insufficient flow rates for a mature FCEV market. Fatigue associated with their moving parts including cracking of diaphragms and failure of seal leads to failure in conventional compressors, which is exacerbated by the repeated starts and stops expected at fueling stations. Furthermore, the conventional lubrication of these compressors with oil is generally unacceptable at fueling stations due to potential fuel contamination. Metal hydride (MH) technology offers a very good alternative to both conventional (mechanical) and newly developed (electrochemical, ionic liquid pistons) methods of hydrogen compression. Advantages of MH compression include simplicity in design and operation, absence of moving parts, compactness, safety and reliability, and the possibility to utilize waste industrial heat to power the compressor. Beyond conventional H2 supplies of pipelines or tanker trucks, another attractive scenario is the on-site generating, pressuring and delivering pure H 2 at pressure (≥ 875 bar) for refueling vehicles at electrolysis, wind, or solar generating production facilities in distributed locations that are too remote or widely distributed for cost effective bulk transport. MH hydrogen compression utilizes a reversible heat-driven interaction of a hydride-forming metal alloy with hydrogen gas to form the MH phase and is a promising process for hydrogen energy applications [1,2]. To deliver hydrogen continuously, each stage of the compressor must consist of multiple MH beds with synchronized hydrogenation & dehydrogenation cycles. Multistage pressurization allows achievement of greater compression ratios using reduced temperature swings compared to single stage compressors. The objectives of this project are to investigate and demonstrate on a laboratory scale a two-stage MH hydrogen (H 2 ) gas compressor with a feed pressure of >50 bar and a delivery pressure ≥ 875 bar of high purity H 2 gas using the scheme shown in Figure 1. Progress to date includes the selection of two candidate metal hydrides for each compressor stage, supplier engagement and synthesis of small samples, and the beginning of in-depth characterization of their thermodynamics, kinetics, and hydrogen capacities for optimal performance with respect to energy requirements and efficiency. Additionally, bed design trade studies are underway and will be finalized in FY18. Subsequently, the prototype two-stage compressor will be fabricated, assembled and experimentally evaluated in FY19.

08 HYDROGEN↗

DOE OSTI2018

Compressed sensing with sparse corruptions: Fault-tolerant sparse collocation approximations

The recovery of approximately sparse or compressible coefficients in a polynomial chaos expansion is a common goal in many modern parametric uncertainty quantification (UQ) problems. However, relatively little effort in UQ has been directed toward theoretical and computational strategies for addressing the sparse corruptions problem, where a small number of measurements are highly corrupted. Such a situation has become pertinent today since modern computational frameworks are sufficiently complex with many interdependent components that may introduce hardware and software failures, some of which can be difficult to detect and result in a highly polluted simulation result. In this paper we present a novel compressive sampling-based theoretical analysis for a regularized t1 minimization algorithm that aims to recover sparse expansion coefficients in the presence of measurement corruptions. Our recovery results are uniform (the theoretical guarantees hold for all compressible signals and compressible corruptions vectors), and prescribe algorithmic regularization parameters in terms of a user-defined a priori estimate on the ratio of measurements that are believed to be corrupted. We also propose an iteratively reweighted optimization algorithm that automatically refines the value of the regularization parameter, and empirically produces superior results. Our numerical results test our framework on several medium-to-high dimensional examples of solutions to parameterized differential equations, and demonstrate the effectiveness of our approach.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2018

Metal Hydride Compression

Conventional hydrogen compressors often contribute over half of the cost of hydrogen stations, have poor reliability, and have insufficient flow rates for a mature fuel cell vehicle market. Fatigue associated with their moving parts including cracking of diaphragms and failure of seals leads to failure in conventional compressors, which is exacerbated by the repeated starts and stops expected at fueling stations. Furthermore, the conventional lubrication of these compressors with oil is generally unacceptable at fueling stations due to potential fuel contamination. MH technology offers a very good alternative to both conventional (mechanical) and newly developed (electrochemical, ionic liquid pistons) methods of hydrogen compression. Advantages of MH compression include simplicity in design and operation, absence of moving parts, compactness, safety and reliability, and the possibility to utilize waste industrial heat to power the compressor. Beyond conventional H 2 supply via pipelines or tanker trucks, another attractive scenario is the on-site generation and delivery of pure H 2 at pressure (> 875 bar) for refueling vehicles at electrolysis, wind, or solar H 2 production facilities in distributed locations that are too remote or widely distributed for cost effective bulk transport. MH hydrogen compression utilizes a reversible heat-driven interaction of a hydride-forming metal alloy with hydrogen gas to form the MH phase and is a promising process for hydrogen energy applications. To deliver hydrogen continuously, each stage of the compressor must consist of multiple MH beds with synchronized hydrogenation & dehydrogenation cycles. Multistage pressurization allows achievement of greater compression ratios using reduced temperature swings compared to single stage compressors. The objectives of this project are to investigate and demonstrate on a laboratory scale a twostage MH hydrogen gas compressor with a feed pressure of >100 bar and a delivery pressure > 875 bar of high purity H 2 gas using the scheme shown in Figure 1. Progress to date includes the selection of metal hydrides for each compressor stage based on experimental characterization of their thermodynamics, kinetics, and hydrogen capacities for optimal performance with respect to energy requirements and efficiency. Additionally, final bed designs have been completed based on trade studies and all components have been ordered. The prototype two-stage compressor will be fabricated, assembled, and experimentally evaluated in FY19.

08 HYDROGEN↗

DOE OSTI2019

X-ray diffraction of dynamically compressed matter on Sandia's Z Pulsed Power Facility

Sandia's Z Pulsed Power Facility is able to dynamically compress matter to extreme states with exceptional uniformity, duration, and size, which are ideal for investigations of fundamental material properties of high energy density conditions. X-ray diffraction (XRD) is a key atomic scale probe since it provides direct observation of the compression and strain of the crystal lattice, and is used to detect, identify, and quantify phase transitions. Because of the destructive nature of Z-Dynamic Materials Properties (DMP) experiments and low signal vs background emission levels of XRD, it is very challenging to detect the XRD pattern close to the Z-DMP load and to recover the data. We developed a new Spherical Crystal Diffraction Imager (SCDI) diagnostic to relay and image the diffracted x-ray pattern away from the load debris field. The SCDI diagnostic utilizes the Z-Beamlet laser to generate 6.2-keV Mn-He c , x-rays to probe a shock-compressed sample on the Z-DMP load. A spherically bent crystal composed of highly oriented pyrolytic graphite is used to collect and focus the diffracted x-rays into a 1-inch thick tungsten housing, where an image plate is used to record the data. We performed experiments to implement the SCDI diagnostic on Z to measure the XRD pattern of shock compressed beryllium samples at pressures of 1.8-2.2 Mbar.

36 MATERIALS SCIENCE↗

DOE OSTI2017

Pressure-induced complexity in dynamically compressed calcium

In this project we studied the series of structural phase transitions that occurs in the alkali earth metal Ca as it transforms to increasingly complex arrangements with pressure. The experiments were designed specifically for the ultra-bright X-ray source of the LCLS and the optical capabilities of the MEC nanosecond drive laser. We studied in detail the unusual structural behavior near the minimum of Ca’s melt curve along the Hugoniot and investigated possible metastable phase formation as an explanation for large discrepancies in pressure-volume data from previous shock and static experiments. In total 200 data shots were taken. Using the laser pulse shaping capabilities for the MEC nanosecond laser permitted two thermodynamic compression paths to be explored: (i) Along the principal Hugoniot within the solid and liquid phases, (ii) along a double-shock path to access a cooler P-T compression path within the solid state. Probing the compressed Ca sample with the LCLS XFEL permitted structural determination of the Ca through x-ray diffraction. Pressure was determined with Doppler Interferometry (MEC VISAR diagnostic) and the known equation-of-state of Ca. These data represent the first direct measurements of lattice level rearrangement in Ca under shock compression. We observe the onset of melt, structure within the liquid and an evolution of crystal structure along off-Hugoniot paths up to 100 GPa. These experiments yield important insights into non-equilibrium phase formation under dynamic loading and the deviation away from nearly free electron like behavior, which has been found to be ubiquitous among the elements.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Proposal for a Proton-Bunch Compression Experiment at IOTA in the Strong Space-Charge Regime

43 PARTICLE ACCELERATORS↗

DOE OSTI2019

Dynamic Mode Decomposition for Compressive System Identification

Dynamic mode decomposition has emerged as a leading technique to identify spatiotemporal coherent structures from high-dimensional data, benefiting from a strong connection to nonlinear dynamical systems via the Koopman operator. In this work, we integrate and unify two recent innovations that extend DMD to systems with actuation [Proctor et al., 2016] and systems with heavily subsampled measurements [Brunton et al., 2015]. When combined, these methods yield a novel framework for compressive system identification [code is publicly available at: https://github.com/zhbai/cDMDc]. It is possible to identify a low-order model from limited input-output data and reconstruct the associated full-state dynamic modes with compressed sensing, adding interpretability to the state of the reduced-order model. Moreover, when full-state data is available, it is possible to dramatically accelerate downstream computations by first compressing the data. We demonstrate this unified framework on two model systems, investigating the effects of sensor noise, different types of measurements (e.g., point sensors, Gaussian random projections, etc.), compression ratios, and different choices of actuation (e.g., localized, broadband, etc.). In the first example, we explore this architecture on a test system with known low-rank dynamics and an artificially inflated state dimension. The second example consists of a real-world engineering application given by the fluid flow past a pitching airfoil at low Reynolds number. This example provides a challenging and realistic test-case for the proposed method, and results demonstrate that the dominant coherent structures are well characterized despite actuation and heavily subsampled data.

97 MATHEMATICS AND COMPUTING↗