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DOE OSTI2025

Contrasting Chemical Kinetic Parameters for Near In‐Service‐Temperature Aging and High‐Temperature Thermal Decomposition of Triaminotrinitrobenzene Formulations

Triaminotrinitrobenzene-based high explosives such as LX-17 offer high energy density and exceptional safety, yet their long-term aging behavior at low temperatures remains poorly understood. In this study, several legacy and new production lots of LX-17 were subjected to accelerated aging experiments below 100°C, during which the formation rate of the initial degradation product, monofurazan (F1), was monitored. Kinetic analysis was performed using a sample-age-aware computational approach, yielding activation energy estimates of 82–91 kJ mol −1 for the low-temperature initiation step—markedly lower than the ∼200 kJ mol −1 associated with high-temperature thermal decomposition. Extrapolation from established cookoff models supports the conclusion that the dominant degradation mechanism at low temperatures differs from that at high temperatures. In conclusion, our results provide a unified kinetic framework that bridges the gap between in-service conditions and high-temperature damage.

Chemistry - Chemical explosives↗

DOE OSTI2021

Observable proton decay in flipped SU(5)

We explore proton decay in a class of realistic supersymmetric flipped SU(5) models supplemented by a U(1) R symmetry which plays an essential role in implementing hybrid inflation. Two distinct neutrino mass models, based on inverse seesaw and type I seesaw, are identified, with the latter arising from the breaking of U(1) R by nonrenormalizable superpotential terms. Depending on the neutrino mass model an appropriate set of intermediate scale color triplets from the Higgs superfields play a key role in proton decay channels that include p → (e + , μ + ) π 0 , p → (e + , μ + ) K 0 , p → $\bar v$π + , and p → $\bar v$K + . We identify regions of the parameter space that yield proton lifetime estimates which are testable at Hyper-Kamiokande and other next generation experiments. We discuss how gauge coupling unification in the presence of intermediate scale particles is realized, and a Z 4 symmetry is utilized to show how such intermediate scales can arise in flipped SU(5). Finally, we compare our predictions for proton decay with previous work based on SU(5) and flipped SU(5).

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2025

Lepton flavor asymmetries: from the early Universe to BBN

Large primordial lepton flavor asymmetries with almost vanishing total baryon-minus-lepton number can evade the usual BBN and CMB constraints if neutrino oscillations lead to perfect flavor equilibration. Solving the momentum averaged quantum kinetic equations (QKEs) describing neutrino oscillations and interactions, we perform the first systematic investigation of this scenario, uncovering a rich flavor structure in stark contradiction to the assumption of simple flavor equilibration. We find (i) a particular direction in flavor space, ∆ne ≃ – 2/3 (– 1)∆n μ for normal (inverted) neutrino mass hierarchy, in which the flavor equilibration is efficient and primordial asymmetries are essentially unconstrained, (ii) a minimal washout factor, ∆$n_{e}^{2}$| BBN ≤ 0.03 (0.016) ∑ α ∆$n_{α}^{2}$| ini yielding a conservative estimate for the allowed primordial asymmetries in a generic flavor direction, and (iii) particularly strong or weak washout if one of the initial flavor asymmetries vanishes due to non-adiabatic muon- or electron-driven MSW transitions. These results open up the possibility of a first-order QCD phase transition facilitated by large lepton asymmetries as well as baryogenesis from large and compensated ∆n e = ∆n μ asymmetries. Our systematic approach of deriving momentum averaged QKEs includes collision terms beyond the damping approximation, energy transfer between the neutrino and electron-photon plasma, and provides a fast and reliable way to investigate the impact of primordial lepton asymmetries at the time of BBN. We publicly release the Mathematica code COFLASY-M on https://github.com/mariofnavarro/COFLASY which solves the QKEs numerically.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2021

Development and validation of a second-order thermal network model for residential buildings

Heating, Ventilation, and Air Conditioning (HVAC) systems can maintain the space air temperature of residential buildings, either directly by heating/cooling the air, or indirectly via heat transfer to and from the building structure that acts as a thermal mass. Hence, HVAC systems can help achieve load shifting, peak load reduction, and/or energy cost saving, thus enabling grid-interactive HVAC operation. A home thermal model that can accurately reflect the dynamics of the space air and interior wall surface temperatures, is therefore valuable. This paper develops such a model using the standard RC (resistance-capacitance) approach. The model contains a virtual envelope node and an internal space node and is thus second-order. A hybrid parameter identification scheme, made up of the least-squares and optimal search methods, is also developed. The proposed model and scheme were validated using data collected from a test home. It was found that a modest amount of training data was sufficient to yield reliable parameter estimates and accurate prediction. It was also found that when making 24-hour-ahead prediction of the space air temperature, both methods had comparable performances when the training data began in a transition season. However, when they began in an HVAC season, the optimal search method performed better. Furthermore, the least-squares method is recommended during a transition season due to its lower computational burden, while the optimal search method is recommended during an HVAC season due to its better estimation performance.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2021

Optimization of the microstructure and mechanical properties of electron beam welded high-strength medium-entropy alloy (NiCoCr) 94 Al 3 Ti 3

For this work, the weldability and effects of subsequent heat treatment on the microstructure and mechanical properties of the medium-entropy alloy (MEA) (NiCoCr) 94 Al 3 Ti 3 have been explored using electron beam welding (EBW). It was found that EBW joints consist of a supersaturated f.c.c. matrix with coarse, asymmetric columnar grains (17.7–24 μm). The fraction of twins and Σ3 n CSL boundaries in weld joints was only 10% of that in the base metal, a value which increased to 30% after aging at 800 °C. The aging also led to improvements in the hardness, tensile strength, and work hardening rate, a result of the precipitation of a high volume fraction (0.29–0.33) of ultrafine (15–17.4 nm dia.) coherent spherical L1 2 -structured particles. The contributions of the L1 2 nanoparticles and Hall-Petch strengthening to the yield strength were estimated to be 537–573 MPa and 105–123 MPa, respectively. The MEA shows excellent weldability and, after aging, good strength (YS~1098 MPa, UTS~1368 MPa) and elongation to failure (~11%) by ductile fracture.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Simulated Biomass Sorghum GHG Reduction Potential is Similar to Maize

Policy support for cellulosic biofuels is contingent on their achieving much greater reductions in life-cycle greenhouse gas emissions than corn starch ethanol. Biomass sorghum has been suggested as a genetically and agronomically tractable feedstock species to augment near-term cellulosic feedstock production. This study used DayCent modeling to investigate biomass sorghum production emissions relative to corn with and without stover utilization at 3,265 across the rainfed United States. Sorghum produced greater average feedstock dry matter (15.6±1.4 vs. 14.8±2.2 Mg ha -1 yr -1 ) and slightly lower estimated ethanol energy yields (10.6±1.0 vs. 11.8±2.9 MJ m -2 yr -1 ) as corn grain with 75% stover collection. The high biomass removals in both the sorghum and corn stover scenarios led to soil organic carbon losses on 90% and 100% of sites, respectively. Average feedstock production emissions intensities were similar between sorghum and corn with 75% stover removal (17.6±2.8 vs. 18.8±3.0 g CO 2 e MJ -1 ), but were notably lower under sorghum for sites in the southwestern study region (13.6±3.0 vs. 22.5±3.1 g CO 2 e MJ -1 ). Futhermore, these results suggest that biomass sorghum produces cellulosic feedstock with similar emissions to corn grain and at current yield levels is unlikely to meet the Renewable Fuel Standard emissions reduction threshold for cellulosic biofuels.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2020

Seismoacoustic analysis of underground explosions using the Rayleigh integral

SUMMARY A coupled seismoacoustic model is developed for the analysis of acoustic signals produced by underground explosive events with an aim to develop a means of improving estimated depth and yield for explosion monitoring. A ground spall model is used to predict surface motion characteristics produced by an underground explosion and the Rayleigh integral is applied to relate the surface motion to the acoustic signal some distance from surface ground zero. The low-frequency component of the ground motion associated with the prolonged free fall of lofted material during spall is found to dominate the acoustic signal propagating away from surface ground zero at shallow angles. The model is applied to observed ground motion and acoustic signals recorded during the Source Physics Experiment (SPE) with promising results. In addition to accurately predicting characteristics of the observed acoustic signals from several of the SPE events, the model provides a means of explaining the lack of signals observed during several events in the SPE due to the directionality of the higher frequency acoustic signals associated with the uplift and closure components as well as the lack of a spatially localized, longer duration dwell.

58 GEOSCIENCES↗

DOE OSTI2024

Particle production by a relativistic semitransparent mirror of finite size and thickness

Production of massless scalar particles by a relativistic semitransparent mirror of finite transverse size and longitudinal thickness in (1+3)D flat spacetime is studied. The derived particle spectrum formula is applied to two specific trajectories. One is the gravitational collapse trajectory invoked in (1+1)D perfectly reflecting moving mirror literature to mimic Hawking radiation, and the other is the plasma mirror trajectory proposed to be realizable in future experiments. It is found that the finiteness of the transverse size leads to diffraction, while the nontrivial thickness amplifies the production rate. We also estimated the particle yield as ~ 3000 in a 20-day data acquisition based on the parameters invoked in the proposed AnaBHEL experiment.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2026

BLUP and mean yields of selected top 25 high yielding half-sib families

BLUP and mean yields of selected top 25 high yielding half-sib families. The yield BLUP were estimated using mixed linear models. The family column indicates the families with progeny column showing the corresponding progenies to selected families. ‘Wat’ here has been used to denote Watkinsville, ‘Tif’ for Tifton and ‘TN’ for Tennessee.

09 BIOMASS FUELS↗

DOE OSTI2022

Shear Measurement with Poorly Resolved Images

Weak lensing studies typically require excellent seeing conditions for the purpose of maximizing the number density of well-resolved galaxy images. It is interesting to ask to what extent the seeing size limits the usefulness of the astronomical images in weak lensing. In this work, we study this issue with the data of the DECam Legacy Survey, which is a part of the target selection program for the Dark Energy Spectroscopic Instrument. Using the Fourier_Quad shear measurement pipeline, we demonstrate that images with relatively poor seeing conditions (~1$^"_.$5) can still yield accurate shear estimators. We do not find any correlation between systematic shear error and the image resolution.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2026

Total Cost of Ownership Reduction Using Passive Pre-Chamber Ignition in Natural Gas Engines

Spark plug durability is a factor affecting the total cost of ownership (TCO) of spark-ignited natural gas engines, with some heavy-duty platforms requiring plug replacement after only 750 hours of operation. The high ignition energy demand under lean or diluted conditions accelerates electrode wear, shortening plug life and increasing maintenance frequency. This work evaluates passive pre-chamber (PC) ignition operating at lowered spark energies as a strategy to reduce spark energy requirements and extend plug durability, thereby lowering TCO. Experiments were conducted on a medium-duty Cummins 6.7L ISB engine at 1600 RPM and 50% load under varying exhaust gas recirculation (EGR) dilution levels (0–40%). Two passive pre-chambers with 1.1 mm and 1.6 mm nozzle diameters were compared with conventional spark ignition (SI). SI was operated with a fixed coil dwell of 4 ms (~90 mJ), while the PC configuration was tested across 2–4 ms dwell times (~30–90 mJ). Cylinder pressure analysis revealed that PC ignition sustained stable combustion at significantly lower spark energies than SI, with improved combustion stability at ~30 mJ compared with SI at ~90 mJ. The PC system also extended the dilution tolerance beyond that achievable with SI, while delivering up to ~2% higher indicated thermal efficiency and reducing the COV by nearly 90% at 30% EGR. A TCO analysis was conducted to assess the economic benefit of adopting a passive PC system operating at reduced spark energies compared to SI. It was found that adopting a passive PC system could reduce TCO by approximately $11,000 per engine over a five-year operational period, primarily due to fuel savings, extended spark plug life, and reduced maintenance frequency. These projections were weighed against the additional hardware cost of the pre-chamber, yielding a rapid estimated return on investment of ~300 operating hours. Therefore, this work motivates continued research and development of passive PC technology and its commercial adoption in natural gas engines used in transportation applications.

Dhotre, Akash [University of Minnesota]↗

DOE OSTI2024

Offshore low-level jet observations and model representation using lidar buoy data off the California coast

Abstract. Low-level jets (LLJs) occur under a variety of atmospheric conditions and influence the available wind resource for wind energy projects. In 2020, lidar-mounted buoys owned by the US Department of Energy (DOE) were deployed off the California coast in two wind energy lease areas administered by the Bureau of Ocean Energy Management: Humboldt and Morro Bay. The wind profile observations from the lidars and collocated near-surface meteorological stations (4–240 m) provide valuable year-long analyses of offshore LLJ characteristics at heights relevant to wind turbines. At Humboldt, LLJs were associated with flow reversals and north-northeasterly winds, directions that are more aligned with terrain influences than the predominant northerly flow. At Morro Bay, coastal LLJs were observed primarily during northerly flow as opposed to the predominant north-northwesterly flow. LLJs were observed more frequently in colder seasons within the lowest 250 m a.s.l. (above sea level), in contrast with the summertime occurrence of the higher-altitude California coastal jet influenced by the North Pacific High, which typically occurs at heights of 300–400 m. The lidar buoy observations also validate LLJ representation in atmospheric models that estimate potential energy yield of offshore wind farms. The European Centre for Medium-Range Weather Forecasts Reanalysis version 5 (ERA5) was unsuccessful at identifying all observed LLJs at both buoy locations within the lowest 200 m. An extension of the National Renewable Energy Laboratory (NREL) 20-year wind resource dataset for the Outer Continental Shelf off the coast of California (CA20-Ext) yielded marginally greater captures of observed LLJs using the Mellor–Yamada–Nakanishi–Niino (MYNN) planetary boundary layer (PBL) scheme than the 2023 National Offshore Wind dataset (NOW-23), which uses the Yonsei University (YSU) scheme. However, CA20-Ext also produced the most LLJ false alarms, which are instances when a model identified an LLJ but no LLJ was observed. CA20-Ext and NOW-23 exhibited a tendency to overestimate the duration of LLJ events and underestimate LLJ core heights.

17 WIND ENERGY↗

NASA NTRS1972

Control of linear uncertain systems utilizing mismatched state observers

The control of linear continuous dynamical systems is investigated as a problem of limited state feedback control. The equations which describe the structure of an observer are developed constrained to time-invarient systems. The optimal control problem is formulated, accounting for the uncertainty in the design parameters. Expressions for bounds on closed loop stability are also developed. The results indicate that very little uncertainty may be tolerated before divergence occurs in the recursive computation algorithms, and the derived stability bound yields extremely conservative estimates of regions of allowable parameter variations.

Goldstein, B.↗

NASA NTRS1972

Discrete-time demodulation of continuous-time signals.

Nonlinear stochastic estimation theory is applied to the problem of obtaining discrete-time demodulator structures for the common types of analog communication signals. A stochastic communication model is presented that can be treated with current results in estimation theory. Approximate algorithms are developed for the estimation problem that yield mathematically realizable receiver structures for the cases of AM, PC, and FM. The digital receivers yield performance characteristics that compare favorably with those of their analog counterparts.

Kelly, C. N.↗

NASA NTRS1972

Maximization of the region of exponential absolute stability.

The problem of selecting a regulator vector which yields the largest estimate of the region of exponential absolute stability is considered. Reformulation of an extended version of the Popov frequency condition in terms of a nonnegative polynomial gives the desired algorithm in mathematical programming format.

Karmarkar, J. S.↗

NASA NTRS1972

A method for calculating aerodynamic heating on sounding rocket tangent ogive noses

A method is presented for calculating the aerodynamic heating and shear stresses at the wall for tangent ogive noses that are slender enough to maintain an attached nose shock through that portion of flight during which heat transfer from the boundary layer to the wall is significant. The lower entropy of the attached nose shock combined with the inclusion of the streamwise pressure gradient yields a reasonable estimate of the actual flow conditions. Both laminar and turbulent boundary layers are examined and an approximation of the effects of (up to) moderate angles-of-attack is included in the analysis. The analytical method has been programmed in FORTRAN 4 for an IBM 360/91 computer.

Wing, L. D.↗

NASA NTRS1972

Mariner 9 television observations of Phobos and Deimos.

Mariner 9 photographs of Phobos and Deimos have yielded new information about the orbits, rotation periods, sizes, shapes, and surface characteristics of the satellites. Both satellites appear to be in synchronous rotation. They are irregular, heavily cratered bodies whose shapes appear to have been determined largely by impact fragmentation and spalling. The surfaces of both satellites have crater densities close to saturation and nearly identical, very low albedos. Lower limits on the tensile and yield strengths are estimated, and it is concluded that both satellites may consist of well-consolidated, though possibly highly fractured material.

Pollack, J. B.↗

NASA NTRS1973

A method for calculating aerodynamic heating on sounding rocket tangent ogive noses.

Wing, L. D.↗