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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 649 records · Page 36
All sourcesNASA NTRSDOE OSTI
NASA NTRS1996

Advanced AE Techniques in Composite Materials Research

Advanced, waveform based acoustic emission (AE) techniques have been successfully used to evaluate damage mechanisms in laboratory testing of composite coupons. An example is presented in which the initiation of transverse matrix cracking was monitored. In these tests, broad band, high fidelity acoustic sensors were used to detect signals which were then digitized and stored for analysis. Analysis techniques were based on plate mode wave propagation characteristics. This approach, more recently referred to as Modal AE, provides an enhanced capability to discriminate and eliminate noise signals from those generated by damage mechanisms. This technique also allows much more precise source location than conventional, threshold crossing arrival time determination techniques. To apply Modal AE concepts to the interpretation of AE on larger composite specimens or structures, the effects of modal wave propagation over larger distances and through structural complexities must be well characterized and understood. To demonstrate these effects, measurements of the far field, peak amplitude attenuation of the extensional and flexural plate mode components of broad band simulated AE signals in large composite panels are discussed. These measurements demonstrated that the flexural mode attenuation is dominated by dispersion effects. Thus, it is significantly affected by the thickness of the composite plate. Furthermore, the flexural mode attenuation can be significantly larger than that of the extensional mode even though its peak amplitude consists of much lower frequency components.

Prosser, William H.↗
NASA NTRS1980

The viscoelastic behavior of the principal compliance matrix of a unidirectional graphite/epoxy composite

A testing program was conducted to determine the time-temperature response of the principal compliances of a unidirectional graphite/epoxy composite. It was shown that the two components of the compliance matrix are time and temperature independent. In addition, the compliance matrix is symmetric for the viscoelastic composite. The time-temperature superposition principle is used to determine shift factors. It was shown that the shift factors are independent of fiber orientation for fiber angles that vary from 10 to 90 deg with respect to the load direction.

Morris, D. H.↗
NASA NTRS1979

Graphite/polyimide tension tests at elevated and cryogenic temperatures

Interim results for characterizing tension properties of graphite/polyimide laminates are reported. Existing test procedures for resin-matrix composites were evaluated for use through the extreme temperature range indicated above. Of particular concern was the performance of resistance strain gages at the elevated temperatures and tests were carried out to compare their performance against that of a capacitive strain gage. Limited design data are reported for graphite/polyimide laminates which are being produced through the CASTS Project.

Chapman, A. J.↗
NASA NTRS2005

Correlating PMC-MMC Bonded Joint 3D FEA with Test

A viewgraph presentation on the correlation of Polymer Matrix Composites (PMC) and Metal Matrix Composites (MMC) bonded joints using three dimensional finite element analyses with materials tests is shown.

Jacobson, Mindy↗
NASA NTRS1991

Thermal-structural panel buckling tests

The buckling characteristics of a titanium matrix composite hat-stiffened panel were experimentally examined for various combinations of thermal and mechanical loads. Panel failure was prevented by maintaining the applied loads below real-time critical buckling predictions. The test techniques used to apply the loads, minimize boundary were shown to compare well with a finite-element buckling analysis for previous panels. Comparisons between test predictions and analysis for this panel are ongoing.

Thompson, Randolph C.↗
DOE OSTI2023

Integrating fiber optic sensors into metallic components for sensing in harsh environments

The integration of fiber optic sensors into high-temperature materials is critical for real-time monitoring and autonomous operation of engineering systems. This study demonstrated a spark plasma sintering (SPS)-assisted embedding process for integrating sapphire fiber optic sensors into stainless steel components during part fabrication. Optical fibers were encapsulated in stainless steel 316L powders which were sintered at different fabrication conditions using SPS to investigate the effects of sintering parameters on the embedment. Measurements of optical transmittance, combined with microstructural analysis (X-ray computed tomography and scanning electron microscopy) and mechanical testing (tensile and microhardness), were conducted to examine the fiber functionality, fiber–matrix bonding quality, and properties of the sintered materials. Here, the results show that under suitable fabrication conditions, intact optical fibers can be encapsulated in highly-densified (>98 % relative density) stainless steel components. These conditions also led to a good bond at the fiber–matrix interface with micron-sized material interdiffusion across the interface. The sintering parameters were observed to affect fiber optical attenuation, where high temperature, pressure, and hold time during SPS enhanced fiber–matrix bonding and adversely affected optical transmission. Tensile testing confirmed the superior tensile strength and ductility of the matrix fabricated by SPS. Furthermore, the materials exhibited limited strength reduction (~70 MPa) upon the integration of fibers. This study demonstrates the effectiveness of SPS for fiber-material integration for high-temperature applications.

36 MATERIALS SCIENCE↗
DOE OSTI2026

Intrusive Uncertainty Quantification and Optimal Experiment Design in the Open-Source Pyomo Ecosystem

This contribution describes ParmEst and Pyomo.DoE, two pillars of the open-source Python-based Pyomo ecosystem for computational optimization with (partial differential) algebraic equation mathematical models. Specifically, ParmEst facilitates intrusive frequentist parameter estimation (PE) and uncertainty quantification (UQ) through built-in features, such as covariance matrix estimation, bootstrapping, and likelihood ratio tests. Complementary, Pyomo.DoE enables optimal experiment design by maximizing various metrics of the Fisher information matrix, such as A-optimality (trace), D-optimality (determinant), E-optimality (minimum eigenvalue), and ME-optimality (condition number). ParmEst and Pyomo.DoE can solve high-dimensional optimization problems by leveraging the model structure and exact derivative information. Finally, we will discuss future opportunities to integrate PE and UQ capabilities with optimization under uncertainty, including robust optimization with non-convex models via PyROS.

97 MATHEMATICS AND COMPUTING↗
NASA NTRS1988

The bit-error rate performance of a satellite microwave matrix switch

The matrix switch is a critical element of communications satellites using multiple-beam antennas and on-board switching. Two proof-of-concept models of a microwave matrix switch have been developed under NASA-sponsored contracts. These switches have undergone extensive testing at NASA Lewis Research Center to determine their operating characteristics in a system environment. The results of these tests indicate the effect of the matrix switch on the overall system operation.

Kerczewski, Robert J.↗
NASA NTRS1988

The bit-error rate performance of a satellite microwave matrix switch

The matrix switch is a critical element of communications satellites employing multiple beam antennas and on-board switching. Two proof-of-concept models of a microwave matrix switch have been developed under NASA-sponsored contracts. These switches have undergone extensive testing at NASA Lewis Research Center to determine their operating characteristics in a system environment. The results of these tests indicate the effect of the matrix switch on the overall system operation.

Kerczewski, Robert J.↗
NASA NTRS2018

Influence of Thin-Film Adhesives in Pullout Tests Between Nickel-Titanium Shape Memory Alloy and Carbon Fiber-Reinforced Polymer Matrix Composites

Strips of nickel-titanium (NiTi) shape memory alloy (SMA) and carbon fiber-reinforced polymer matrix composite (PMC) were bonded together using multiple thin film adhesives and their mechanical strengths were evaluated under pullout test configuration. Tensile and lap shear tests were conducted to confirm the deformation of SMAs at room temperature and to evaluate the adhesive strength between the NiTi strips and the PMC. Optical and scanning electron microscopy techniques were used to examine the interfacial bonding after failure. Simple equations on composite tensile elongation were used to fit the experimental data on tensile properties. ABAQUS models were generated to show the effects of enhanced bond strength and the distribution of stress in SMA and PMC. The results revealed that the addition of thin film adhesives increased the average adhesive strength between SMA and PMC while halting the room temperature shape memory effect within the pullout specimen.

Polymer Matrix Composites↗
NASA NTRS2000

Regulation of Osteoblast Survival by the Extracellular Matrix and Gravity

Spaceflight adversely affects the skeleton, posing a substantial risk to astronaut's health during long duration missions. The reduced bone mass observed in growing animals following spaceflight is due at least in part to inadequate bone formation by osteoblasts. Thus, it is of central importance to identify basic cellular mechanisms underlying normal bone formation. The fundamental ideas underlying our research are that interactions between extracellular matrix proteins, integrin adhesion receptors, cytoplasmic signaling and cytoskeletal proteins are key ingredients for the proper functioning of osteoblasts, and that gravity impacts these interactions. As an in vitro model system we used primary fetal rat calvarial cells which faithfully recapitulate osteoblast differentiation characteristically observed in vivo. We showed that specific integrin receptors ((alpha)3(beta)1), ((alpha)5(beta)1), ((alpha)8(betal)1) and extracellular matrix proteins (fibronectin, laminin) were needed for the differentiation of immature osteoblasts. In the course of maturation, cultured osteoblasts switched from depending on fibronectin and laminin for differentiation to depending on these proteins for their very survival. Furthermore, we found that manipulating the gravity vector using ground-based models resulted in activation of key intracellular survival signals generated by integrin/extracellular matrix interactions. We are currently testing the in vivo relevance of some of these observations using targeted transgenic technology. In conclusion, mechanical factors including gravity may participate in regulating survival via cellular interactions with the extracellular matrix. This leads us to speculate that microgravity adversely affects the survival of osteoblasts and contributes to spaceflight-induced osteoporosis.

Globus. Ruth K.↗
DOE OSTI2022

Coreflood Tests to Evaluate Enhanced Oil Recovery Potential of Wettability-Altering Surfactants for Oil-Wet Heterogeneous Carbonate Reservoirs

Summary Oil-wetness and heterogeneity are two main factors that result in low oil recovery (OR) by waterflood in carbonate reservoirs. The injected water is likely to flow through high-permeability regions and bypass the oil in the low-permeability matrix. In this study, systematic coreflood tests were carried out in both “homogeneous” cores and “heterogeneous” cores with a wettability-altering surfactant. The homogeneous coreflood tests were conducted to evaluate surfactant retention, as well as to compare tertiary surfactant flooding with secondary surfactant flooding. The heterogeneous coreflood test was proposed to model bypassing in low-permeability matrix during waterfloods, and dynamic imbibition of surfactant into the low-permeability matrix. Surfactant retention results suggest that retention increases as initial oil saturation decreases. The retention of selected surfactant in the target reservoir cores was measured to be within a range of 0.07–0.12 mg/g-rock, which is economically acceptable. The results of homogeneous coreflood tests showed that both secondary waterflood and secondary surfactant flood can achieve high OR (>50%) from relatively homogeneous oil-wet cores. A shut-in phase after the surfactant injection resulted in a surge in oil production, which suggests that enough time should be given for wettability alteration by surfactants. The results of heterogeneous coreflood tests showed that more oil is bypassed in the tighter matrix by waterflood if the permeability is higher in the flooded layer and this bypassed oil is the target for the wettability-altering surfactant floods. Slow wettability-altering surfactant injection leads to imbibition into bypassed regions. When the oil-wet carbonate reservoirs have large unswept regions after waterflood, wettability-altering surfactants can significantly improve OR if enough time is given for imbibition.

Engineering↗
NASA NTRS1984

Siloxane containing addition polyimides. II - Acetylene terminated polyimides

Acetylene terminated polyimide oligomers having a range of molecular weights have been synthesized by reacting bis (gamma-aminopropyl) tetramethyldisiloxane, aminophenylacetylene and 3, 3', 4, 4' benzophenonetetracarboxylic dianhydride in different molar ratios. The prepolymers were isolated and characterized for melt flow and cure properties. They show promise as adhesives for bonding titanium to titanium and as matrix resins for graphite cloth reinforced composites. The most promising system has been blended in varying proportions with Thermid 600, a commercially available acetylene terminated polyimide oligomer, and the mixtures have been tested for application as composite matrix resins.

Maudgal, S.↗
DOE OSTI2023

Verification and Validation of the New MCNP6.3 Criticality Features [Slides]

This presentation touches on a separate MCNP6.3 V&V document reports on all the default calculations for all test suites. Here, we look at new optional features of the MCNP6.3 code with Fission-matrix-based options, Convergence and population testing, and Automated acceleration of the fission source additionally Doppler Broadening Resonance Correction. Also touched on are validation benchmarks: criticality, crit_expanded, and Rossi-α. All the new MCNP6.3 options give statistically equivalent results and either provide a reduction or no change in computational cost. We consider giving these new features a try and using them for all criticality calculations.

97 MATHEMATICS AND COMPUTING↗
NASA NTRS1973

Factors affecting miniature Izod impact strength of tungsten-fiber-metal-matrix

The miniature Izod and Charpy impact strengths of copper, copper-nickel, and nickel-base superalloy uniaxially reinforced with continuous tungsten fibers were studied. In most cases, impact strength was increased by increasing fiber or matrix toughness, decreasing fibermatrix reaction, increasing test temperature, hot working, or heat treating. Notch sensitivity was reduced by increasing fiber content or matrix toughness. An equation relating impact strength to fiber and matrix properties and fiber content was developed. Program results imply that tungsten alloy-fiber/superalloy matrix composites can be made with adequate impact resistance for turbine blade or vane applications.

Winsa, E. A.↗
NASA NTRS2021

Ambient Performance Testing of the CubeSat Infrared Atmospheric Sounder (CIRAS)

Hyperspectral infrared measurements of Earth’s atmosphere from space have proven their value for weather forecasting, climate science and atmospheric composition. The CubeSat Infrared Atmospheric Sounder (CIRAS) instrument will demonstrate a fully functional infrared temperature, water vapor and carbon monoxide sounder in a CubeSat sized volume for at least an order of magnitude lower cost than legacy systems. Design for a CubeSat significantly reduces cost of access to space and enables flight in a constellation to reduce revisit time and enable new measurements including 3D winds. A technology demonstration of CIRAS is currently under development at JPL. The effort has completed integration and ambient testing of a high fidelity brassboard, complete with the flight configured optics assembly developed by Ball Aerospace with a JPL Immersion Grating and Black Silicon Entrance Slit. The brassboard includes a flight-configured High Operating Temperature Barrier Infrared Detector (HOT-BIRD) mounted in an Integrated Dewar Cryocooler Assembly (IDCA), enabling testing in the ambient environment. Ambient testing included radiometric testing of the system to characterize the instrument operability and NEdT. Spatial testing was performed to characterize the system line spread function (LSF) in two axes and report FWHM of the LSF. Spectral testing involved an air path test to characterize the spectral/spatial transformation matrix, and an etalon was used to measure the Spectral Response Functions (SRFs). Results of the testing show the CIRAS performs exceptionally well and meets the key performance required of the system. The end result of testing is the CIRAS instrument now meets TRL 4 with confidence in a brassboard configuration ready for thermal vacuum (TVac) testing necessary to achieve TRL 5 for the system.

Wilson, Robert C.↗
NASA NTRS1993

From requirements to acceptance tests

From user requirements definition to accepted software system, the software project management wants to be sure that the system will meet the requirements. For the development of a telecommunication satellites Control Centre, C.N.E.S. has used new rules to make the use of tracing matrix easier. From Requirements to Acceptance Tests, each item of a document must have an identifier. A unique matrix traces the system and allows the tracking of the consequences of a change in the requirements. A tool has been developed, to import documents into a relational data base. Each record of the data base corresponds to an item of a document, the access key is the item identifier. Tracing matrix is also processed, providing automatically links between the different documents. It enables the reading on the same screen of traced items. For example one can read simultaneously the User Requirements items, the corresponding Software Requirements items and the Acceptance Tests.

Baize, Lionel↗
NASA NTRS1992

Interfacial stress state present in a 'thin-slice' fibre push-out test

An analysis of the stress distributions along the fiber-matrix interface in a 'thin-slice' fiber push-out test is presented for selected test geometries. For the small specimen thicknesses often required to displace large-diameter fibers with high interfacial shear strengths, finite element analysis indicates that large bending stresses may be present. The magnitude of these stresses and their spatial distribution can be very sensitive to the test configuration. For certain test geometries, the specimen configuration itself may alter the interfacial failure process from one which initiates due to a maximum in shear stress near the top surface adjacent to the indentor, to one which involves mixed mode crack growth up from the bottom surface and/or yielding within the matrix near the interface.

Kallas, M. N.↗