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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 649 records · Page 36
All sourcesNASA NTRSDOE OSTI
DOE OSTI2013

Cyanine-based probe\tag-peptide pair fluorescence protein imaging and fluorescence protein imaging methods

A molecular probe comprises two arsenic atoms and at least one cyanine based moiety. A method of producing a molecular probe includes providing a molecule having a first formula, treating the molecule with HgOAc, and subsequently transmetallizing with AsCl.sub.3. The As is liganded to ethanedithiol to produce a probe having a second formula. A method of labeling a peptide includes providing a peptide comprising a tag sequence and contacting the peptide with a biarsenical molecular probe. A complex is formed comprising the tag sequence and the molecular probe. A method of studying a peptide includes providing a mixture containing a peptide comprising a peptide tag sequence, adding a biarsenical probe to the mixture, and monitoring the fluorescence of the mixture.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2013

Band excitation method applicable to scanning probe microscopy

Methods and apparatus are described for scanning probe microscopy. A method includes generating a band excitation (BE) signal having finite and predefined amplitude and phase spectrum in at least a first predefined frequency band; exciting a probe using the band excitation signal; obtaining data by measuring a response of the probe in at least a second predefined frequency band; and extracting at least one relevant dynamic parameter of the response of the probe in a predefined range including analyzing the obtained data. The BE signal can be synthesized prior to imaging (static band excitation), or adjusted at each pixel or spectroscopy step to accommodate changes in sample properties (adaptive band excitation). An apparatus includes a band excitation signal generator; a probe coupled to the band excitation signal generator; a detector coupled to the probe; and a relevant dynamic parameter extractor component coupled to the detector, the relevant dynamic parameter extractor including a processor that performs a mathematical transform selected from the group consisting of an integral transform and a discrete transform.

42 ENGINEERING↗
DOE OSTI2017

Full information acquisition in scanning probe microscopy and spectroscopy

Apparatus and methods are described for scanning probe microscopy and spectroscopy based on acquisition of full probe response. The full probe response contains valuable information about the probe-sample interaction that is lost in traditional scanning probe microscopy and spectroscopy methods. The full probe response is analyzed post data acquisition using fast Fourier transform and adaptive filtering, as well as multivariate analysis. The full response data is further compressed to retain only statistically significant components before being permanently stored.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Pump-probe ghost imaging with SASE FELs

In this paper we propose a new approach to measuring ultrafast dynamics with free-electron lasers (FELs). Ultrafast experiments are among the most promising avenues of research at x-ray FELs, with potential to reveal the chemical dynamics of charge separation, conical intersection crossing, and biologically mediated reactions. Pump-probe scanning is the standard approach to measure dynamics at x-ray FELs, but at the shortest time scales, and particularly for x-ray pump, x-ray probe experiments, the scans require challenging beam setups and can introduce systematic errors. Here we propose an alternative approach using the randomness of the self-amplified spontaneous emission (SASE) process to drive many simultaneous pump-probe experiments on each shot. Measuring the fluctuations in the incident beam’s time profile on a shot-to-shot basis enables reconstruction of ultrafast dynamics down to the coherence length of the FEL without the need for pump-probe scans. Due to similarity to ghost imaging, in which spatial properties are reconstructed by measuring the incident probe’s transverse properties, we call this ``pump-probe ghost imaging" (PPGI). In this paper we describe the method and simulate an example experiment. We also describe an alternative implementation that uses only spectral measurements, avoiding the need for direct time-domain diagnostics, and extending the method to the attosecond regime.

Ratner, Daniel Fried↗
DOE OSTI2022

Flexible electric probe

A flexible electric probe can include: a flexible substrate; and probe line conductors on the flexible substrate, the probe line conductors being essentially parallel to each other and having separations of about 5-50 microns. The flexible electric probe can further include connection conductors on the flexible substrate, the connection conductors and the probe line conductors electrically connected to each other, the probe line conductors positioned in first and second offset patterns with regard to the connection conductors.

Mazzeo, Brian A.↗
NASA NTRS2019

Nasa Glenn Icing Research Tunnel: 2018 Change in Drop-Sizing Equations Due to Change in Cloud Droplet Probe Sample Area

Although there has been no physical change to the cloud drop diameters in the NASA Glenn Icing Research Tunnel (IRT), the IRT cloud calibration team now has an improved understanding of the facility’s drop-sizing instrumentation, which has resulted in a recent change to the drop-sizing equations. Only the calculated values given in the previous calibration report have changed. In 2017, IRT staff found reason to believe that since at least 2014, the sample area for its Cloud Droplet Probe (CDP) (Droplet Measurement Technologies, Inc.) has been closer to 0.289 mm2, rather than the user manual’s suggested value of 0.24 mm2. In September 2017, the probe’s sample area was measured both before and after the probe was realigned, and the end sample area was measured to be 0.248 mm2. Following the probe’s realignment, drop size measurements were made in the IRT using the CDP as well as optical array probes OAP–230X and OAP–230Y (Particle Measurement Systems, Inc.). These measurements suggested that 0.289 mm2 was the more accurate value for historical measurements. When the CDP sample area used for calculations was changed from 0.24 to 0.289 mm2, distributions previously reported to have a median volumetric diameter (MVD) between 30 and 100 μm were instead calculated to have MVD values 10 to 18 percent higher. The analyses that led to these conclusions are reported in this paper, as well as the new drop-sizing equations that have been developed for the corrected measurement values. This report contains updates to drop-sizing data for the IRT’s “normal” operating conditions (MVD < 50 μm) and discusses the effects on the IRT’s “large-drop” conditions (Mod1 nozzles, Pair < 10 psig), but it does not include updates to the drop-sizing equations for those large-drop conditions.

Particle sizing↗
DOE OSTI2018

A BODIPY Based Fluorescent Probe for the Rapid Detection of Hypochlorite

A new boron-dipyrromethene (BODIPY) fluorescent dye aimed at sensitively detecting hypochlorite anion (ClO{sup −}) has been designed, synthesized and characterized. The probe is comprised of a BODIPY fluorophore unit and a ClO{sup −} specific reactive group of amidoxime. The addition of hypochlorite results in a red-shift of absorption and emission spectra of the probe accompanied by a decrease of intensity and spectra changes (A{sub 500} and 1/I{sub 512}) of the probe can achieve a good linearity to the concentration of ClO{sup −}. The fluorescence probe can react to ClO{sup −} rapidly (within 60 s) in a wide pH range (4–10) with high sensitivity (detection limit of 6.81 μM) and selectivity. The reaction mechanism has been proposed and confirmed by MS analysis, ClO{sup −} anion oxidizes amidoxime moiety to hydroxyl group and hydroxyl group is further oxidized to formyl group in the formation of a corresponding aldehyde compound. In addition, the probe has also been successfully applied to detect ClO{sup −} in tap water and river water samples by spiking a known amount of standard ClO{sup −}.

74 ATOMIC AND MOLECULAR PHYSICS↗
DOE OSTI2022

Collaborative Research Activities of the Arase and Van Allen Probes

This paper presents the highlights of joint observations of the inner magnetosphere by the Arase spacecraft, the Van Allen Probes spacecraft, and ground-based experiments integrated into spacecraft programs. The concurrent operation of the two missions in 2017–2019 facilitated the separation of the spatial and temporal structures of dynamic phenomena occurring in the inner magnetosphere. Because the orbital inclination angle of Arase is larger than that of Van Allen Probes, Arase collected observations at higher L-shells up to L ~ 10. After March 2017, similar variations in plasma and waves were detected by Van Allen Probes and Arase. We describe plasma wave observations at longitudinally separated locations in space and geomagnetically-conjugate locations in space and on the ground. The results of instrument intercalibrations between the two missions are also presented. Arase continued its normal operation after the scientific operation of Van Allen Probes completed in October 2019. The combined Van Allen Probes (2012-2019) and Arase (2017-present) observations will cover a full solar cycle. This will be the first comprehensive long-term observation of the inner magnetosphere and radiation belts.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2013

A direct Vlasov code to study the non-stationary current collection by a cylindrical Langmuir probe

The time-dependent current collection by a cylindrical Langmuir probe, whose bias is suddenly changed from zero to a positive or negative finite value, is studied with a novel direct Vlasov code. The numerical algorithm is based on finite-difference formulas to approximate spatial and velocity derivatives and the time integration is carried out with an explicit Runge-Kutta method, or in the case of probe radius small compared with the Debye length, by using the unconditionally stable backward Euler scheme. Both electrons and ions are treated kinetically by the code, which implements initial and boundary conditions that are consistent with the presence of the probe. Within the considered parameter range, the plasma sheath around the probe exhibited an overshoot and it later recovered a steady state. Phase space diagrams of the particle trajectories revealed the presence of a trapped population of particles. The dependence of this population as a function of the probe radius is presented as well as a comparison with the stationary theory. The performance of the code and a comparison with previously used particle-in-cell algorithms are discussed.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2013

Modeling of current characteristics of segmented Langmuir probe on DEMETER

We model the current characteristics of the DEMETER Segmented Langmuir probe (SLP). The probe is used to measure electron density and temperature in the ionosphere at an altitude of approximately 700 km. It is also used to measure the plasma flow velocity in the satellite frame of reference. The probe is partitioned into seven collectors: six electrically insulated spherical segments and a guard electrode (the rest of the sphere and the small post). Comparisons are made between the predictions of the model and DEMETER measurements for actual ionospheric plasma conditions encountered along the satellite orbit. Segment characteristics are computed numerically with PTetra, a three-dimensional particle in cell simulation code. In PTetra, space is discretized with an unstructured tetrahedral mesh, thus, enabling a good representation of the probe geometry. The model also accounts for several physical effects of importance in the interaction of spacecraft with the space environment. These include satellite charging, photoelectron, and secondary electron emissions. The model is electrostatic, but it accounts for the presence of a uniform background magnetic field. PTetra simulation results show different characteristics for the different probe segments. The current collected by each segment depends on its orientation with respect to the ram direction, the plasma composition, the magnitude, and the orientation of the magnetic field. It is observed that the presence of light H{sup +} ions leads to a significant increase in the ion current branch of the I-V curves of the negatively polarized SLP. The effect of the magnetic field is demonstrated by varying its magnitude and direction with respect to the reference magnetic field. It is found that the magnetic field appreciably affects the electron current branch of the I-V curves of certain segments on the SLP, whereas the ion current branch remains almost unaffected. PTetra simulations are validated by comparing the computed characteristics and their angular anisotropy with the DEMETER measurements, as simulation results are found to be in good agreement with the measurements.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2013

Magnetic dipole discharges. II. Cathode and anode spot discharges and probe diagnostics

The high current regime of a magnetron-type discharge has been investigated. The discharge uses a permanent magnet as a cold cathode which emits secondary electrons while the chamber wall or a grounded electrode serves as the anode. As the discharge voltage is increased, the magnet develops cathode spots, which are short duration arcs that provide copious electrons to increase the discharge current dramatically. Short (1 μs), high current (200 A) and high voltage (750 V) discharge pulses are produced in a relaxation instability between the plasma and a charging capacitor. Spots are also observed on a negatively biased plane Langmuir probe. The probe current pulses are as large as those on the magnet, implying that the high discharge current does not depend on the cathode surface area but on the properties of the spots. The fast current pulses produce large inductive voltages, which can reverse the electrical polarity of the magnet and temporarily operate it as an anode. The discharge current may also oscillate at the frequency determined by the charging capacitor and the discharge circuit inductance. Each half cycle of high-current current pulses exhibits a fast (≃10 ns) current rise when a spot is formed. It induces high frequency (10–100 MHz) transients and ringing oscillations in probes and current circuits. Most probes behave like unmatched antennas for the electromagnetic pulses of spot discharges. Examples are shown to distinguish the source of oscillations and some rf characteristics of Langmuir probes.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2013

A multichannel magnetic probe system for analysing magnetic fluctuations in helical axis plasmas

The need to understand the structure of magnetic fluctuations in H-1NF heliac [S. Hamberger et al., Fusion Technol. 17, 123 (1990)] plasmas has motivated the installation of a sixteen former, tri-axis helical magnetic probe Mirnov array (HMA). The new array complements two existing poloidal Mirnov arrays by providing polarisation information, higher frequency response, and improved toroidal resolution. The helical placement is ideal for helical axis plasmas because it positions the array as close as possible to the plasma in regions of varying degrees of favourable curvature in the magnetohydrodynamic sense, but almost constant magnetic angle. This makes phase variation with probe position near linear, greatly simplifying the analysis of the data. Several of the issues involved in the design, installation, data analysis, and calibration of this unique array are presented including probe coil design, frequency response measurements, mode number identification, orientation calculations, and mapping probe coil positions to magnetic coordinates. Details of specially designed digitally programmable pre-amplifiers, which allow gains and filters to be changed as part of the data acquisition initialisation sequence and stored with the probe signals, are also presented. The low shear heliac geometry [R. Jiménez-Gómez et al., Nucl. Fusion 51, 033001 (2011)], flexibility of the H-1NF heliac, and wealth of information provided by the HMA create a unique opportunity for detailed study of Alfvén eigenmodes, which could be a serious issue for future fusion reactors.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2014

Pump and probe spectroscopy with continuous wave quantum cascade lasers

This paper details infra-red pump and probe studies on nitric oxide conducted with two continuous wave quantum cascade lasers both operating around 5 μm. The pump laser prepares a velocity selected population in a chosen rotational quantum state of the v = 1 level which is subsequently probed using a second laser tuned to a rotational transition within the v = 2 ← v = 1 hot band. The rapid frequency scan of the probe (with respect to the molecular collision rate) in combination with the velocity selective pumping allows observation of marked rapid passage signatures in the transient absorption profiles from the polarized vibrationally excited sample. These coherent transient signals are influenced by the underlying hyperfine structure of the pump and probe transitions, the sample pressure, and the coherent properties of the lasers. Pulsed pump and probe studies show that the transient absorption signals decay within 1 μs at 50 mTorr total pressure, reflecting both the polarization and population dephasing times of the vibrationally excited sample. The experimental observations are supported by simulation based upon solving the optical Bloch equations for a two level system.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2014

Probe-rotating atomic force microscopy for determining material properties

In this paper, we propose a probe-rotating atomic force microscope that enables scan in an arbitrary direction in the contact imaging mode, which is difficult to achieve using a conventional atomic force microscope owing to the orientation-dependent probe and the inability to rotate the probe head. To enable rotation of the probe about its vertical axis, we employed a compact and light probe head, the sensor of which is made of an optical disk drive pickup unit. Our proposed mechanical configuration, operating principle, and control system enables axial and lateral scan in various directions.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2014

2D potential measurements by applying automatic beam adjustment system to heavy ion beam probe diagnostic on the Large Helical Device

Two-dimensional potential profiles in the Large Helical Device (LHD) were measured with heavy ion beam probe (HIBP). To measure the two-dimensional profile, the probe beam energy has to be changed. However, this task is not easy, because the beam transport line of LHD-HIBP system is very long (∼20 m), and the required beam adjustment consumes much time. To reduce the probe beam energy adjustment time, an automatic beam adjustment system has been developed. Using this system, required time to change the probe beam energy is dramatically reduced, such that two-dimensional potential profiles were able to be successfully measured with HIBP by changing the probe beam energy shot to shot.

43 PARTICLE ACCELERATORS↗
DOE OSTI2014

Langmuir probe analysis in electronegative plasmas

This paper compares two methods to analyze Langmuir probe data obtained in electronegative plasmas. The techniques are developed to allow investigations in plasmas, where the electronegativity α{sub 0} = n{sub –}/n{sub e} (the ratio between the negative ion and electron densities) varies strongly. The first technique uses an analytical model to express the Langmuir probe current-voltage (I-V) characteristic and its second derivative as a function of the electron and ion densities (n{sub e}, n{sub +}, n{sub –}), temperatures (T{sub e}, T{sub +}, T{sub –}), and masses (m{sub e}, m{sub +}, m{sub –}). The analytical curves are fitted to the experimental data by adjusting these variables and parameters. To reduce the number of fitted parameters, the ion masses are assumed constant within the source volume, and quasi-neutrality is assumed everywhere. In this theory, Maxwellian distributions are assumed for all charged species. We show that this data analysis can predict the various plasma parameters within 5–10%, including the ion temperatures when α{sub 0} > 100. However, the method is tedious, time consuming, and requires a precise measurement of the energy distribution function. A second technique is therefore developed for easier access to the electron and ion densities, but does not give access to the ion temperatures. Here, only the measured I-V characteristic is needed. The electron density, temperature, and ion saturation current for positive ions are determined by classical probe techniques. The electronegativity α{sub 0} and the ion densities are deduced via an iterative method since these variables are coupled via the modified Bohm velocity. For both techniques, a Child-Law sheath model for cylindrical probes has been developed and is presented to emphasize the importance of this model for small cylindrical Langmuir probes.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2015

Apertureless scanning microscope probe as a detector of semiconductor laser emission

An operating semiconductor laser has been studied using a scanning probe microscope. A shift of the resonance frequency of probe that is due to its heating by laser radiation has been analyzed. The observed shift is proportional to the absorbed radiation and can be used to measure the laser near field or its output power. A periodical dependence of the measured signal has been observed as a function of distance between the probe and the surface of the laser due to the interference of the outgoing and cantilever-reflected waves. Due to the multiple reflections resulting in the interference, the light absorption by the probe cantilever is greatly enhanced compared with a single pass case. Interaction of infrared emission of a diode laser with different probes has been studied.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2015

Matched dipole probe for magnetized low electron density laboratory plasma diagnostics

In this paper, a diagnostic method for magnetized and unmagnetized laboratory plasma is proposed, based on impedance measurements of a short matched dipole. The range of the measured electron densities is limited to low density plasmas (10{sup 12}–10{sup 15 }m{sup −3}), where other diagnostic methods have strong limitations on the magnetic field strength and topology, plasma dimensions, and boundary conditions. The method is designed for use in both large- and small-dimension plasma (<10 cm) without or with strong non-homogeneous magnetic field, which can be undefined within the probe size. The design of a matched dipole probe allows to suppress the sheath resonance effects and to reach high sensitivity at relatively small probe dimensions. Validation experiments are conducted in both magnetized (B ∼ 170 G) and unmagnetized (B = 0) low density (7 × 10{sup 12 }m{sup −3}–7 × 10{sup 13 }m{sup −3}) low pressure (1 mTorr) 10 cm scale plasmas. The experimentally measured data show very good agreement with an analytical theory both for a non-magnetized and a magnetized case. The electron density measured by the matched dipole and Langmuir probes in the range of 7 × 10{sup 12 }m{sup −3}–7 × 10{sup 13 }m{sup −3} show less than 30% difference. An experimentally measured tolerance/uncertainty of the dipole probe method is estimated to ±1% for plasma densities above 2 × 10{sup 13 }m{sup −3}. A spatial resolution is estimated from the experiments to be about 3d, where d is the dipole diameter. The diagnostic method is also validated by comparing the measured plasma impedance curves with results of analytical modelling.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗