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At least 649 records · Page 36
All sourcesNASA NTRSDOE OSTI
NASA NTRS1988

Advanced protein crystal growth flight hardware for the Space Station

The operational environment of the Space Station will differ considerably from the previous short term missions such as the Spacelabs. Limited crew availability combined with the near continuous operation of Space Station facilities will require a high degree of facility automation. This paper will discuss current efforts to develop automated flight hardware for advanced protein crystal growth on the Space Station. Particular areas discussed will be the automated monitoring of key growth parameters for vapor diffusion growth and proposed mechanisms for control of these parameters. A history of protein crystal growth efforts will be presented in addition to the rationale and need for improved protein crystals for X-ray diffraction. The facility will be capable of simultaneously processing several hundred protein samples at various temperatures, pH's, concentrations etc., and provide allowances for real time variance of growth parameters.

Herrmann, Frederick T.↗
NASA NTRS1993

Solar magnetic field studies using the 12 micron emission lines. II - Stokes profiles and vector field samples in sunspots

Polarimetric observations at 12 microns of two sunpots are reported. The horizontal distribution of parameters such as magnetic field strength, inclination, azimuth, and magnetic field filling factors are presented along with information about the height dependence of the magnetic field strength. Comparisons with contemporary magnetostatic sunspot models are made. The magnetic data are used to estimate the height of 12 micron line formation. From the data, it is concluded that within a stable sunspot there are no regions that are magnetically filamentary, in the sense of containing both strong-field and field-free regions.

Hewagama, Tilak↗
NASA NTRS1991

Optical constants of solid methane and ethane from 10,000 to 450/cm

Near- and mid-IR spectra of thin films of crystalling phase I and phase II C2H6 are presented using a combined least squares and Kramers-Kronig analysis. Complex refractive indices derived from these data are also presented. To obtain material in phase I, samples are annealed at 33 K for about 30 min; phase II is obtained by recooling below the transition temperature of 20.4 K. The derived optical parameters are shown. The infrared spectrum of phase I CH4 exhibits broad structureless absorptions at about 1300 and 2600/cm. On cooling the sample below 20.4 K (phase II), the absorptions are sharpened, and each band develops fine structure. The present results and those of Roux et al. (1979) are compared. The agreement with the real parts is found to be excellent; given the difference in resolution, the agreement with the imaginary parts is also good.

Pearl, J.↗
NASA NTRS2014

Updated Performance Evaluation of the ISS Water Processor Multifiltration Beds

The ISS Water Processor Assembly (WPA) produces potable water from a waste stream containing humidity condensate and urine distillate. The primary treatment process is achieved in the Multifiltration Beds, which include adsorbent media and ion exchange resin for the removal of dissolved organic and inorganic contaminants. Two Multifiltration Beds (MF Beds) were replaced on ISS in July 2010 after initial indication of inorganic breakthrough of the first bed and an increasing Total Organic Carbon (TOC) trend in the product water. The first bed was sampled and analyzed Sept 2011 through March 2012. The second MF Bed was sampled and analyzed June 2012 through August 2012. The water resident in the both beds was analyzed for various parameters to evaluate adsorbent loading, performance of the ion exchange resin, microbial activity, and generation of leachates from the ion exchange resin. Portions of the adsorbent media and ion exchange resin were sampled and subsequently desorbed to identify the primary contaminants removed at various points in the bed in addition to microbial analysis. Analysis of the second bed will be compared to results from the first bed to provide a comprehensive overview of how the Multifiltration Beds function on orbit. New data from the second bed supplements the analysis of the first bed (previously reported) and gives a more complete picture of breakthrough compounds, resin breakdown products, microbial activity, and difficult to remove compounds. The results of these investigations and implications to the operation of the WPA on ISS are documented in this paper.

Bowman, Elizabeth M.↗
NASA NTRS2018

Lunar Sample Return Entry Systems Analysis

The Lunar Prospector and Clementine missions have revealed deposits of water-ice located at the South Pole-Aitken Basin of the lunar surface. Due to the scarce amount of previous successful sample return missions and the recent discovery of water-ice, the National Research Council (NRC) Decadal Survey recommended prioritizing the development of a Lunar Sample Return Mission Architecture. The NRC Decadal survey ranked the return of cryogenic samples that could potentially aid in current scientific investigations and identify sites for in-situ resource utilization to support future exploration missions. This study aims to identify the key technical challenges and operational constraints involved in returning cryogenic samples in pristine condition. A detailed classification of defined ground rules and assumptions, justification of mission events and high level functional requirements reinforces the proposed concept of operations. In support of the drafted architecture, a comprehensive analysis on design and environmental constraints are documented for the Earth return vehicle, sample container and thermal protection entry system. The design and thermal analysis is comprised of quantitative dimensions for mass and volume, flight performance parameters and thermal system performance limitations. Further refinement of the high level functional requirements is imperative for determining the optimal approach for returning cryopreserved lunar samples.

Lunar Sample Return↗
NASA NTRS2003

Flight Planning for the International Space Station - Levitation Observation of Dendrite Evolution in Steel Ternary Alloy Rapid Solidification (LODESTARS)

During rapid solidification, a molten sample is cooled below its equilibrium solidification temperature to form a metastable liquid. Once nucleation is initiated, growth of the solid phase proceeds and can be seen as a sudden rise in temperature. The heat of fusion is rejected ahead of the growing dendrites into the undercooled liquid in a process known as recalescence. Fe-Cr-Ni alloys may form several equilibrium phases and the hypoeutectic alloys, with compositions near the commercially important 316 stainless steel alloy, are observed to solidify by way of a two-step process known as double recalescence. During double recalescence, the first temperature rise is associated with formation of the metastable ferritic solid phase with subsequent conversion to the stable austenitic phase during the second temperature rise. Selection of which phase grows into the undercooled melt during primary solidification may be accomplished by choice of the appropriate nucleation trigger material or by control of the processing parameters during rapid solidification. Due to the highly reactive nature of the molten sample material and in order to avoid contamination of the undercooled melt, a containerless electromagnetic levitation (EML) processing technique is used. In ground-based EML, the same forces that support the weight of the sample against gravity also drive convection in the liquid sample. However, in microgravity, the force required to position the sample is greatly reduced, so convection may be controlled over a wide range of internal flows. Space Shuttle experiments have shown that the double recalescence behavior of Fe-Cr-Ni alloys changes between ground and space EML experiments. This program is aimed at understanding how melt convection influences phase selection and the evolution of rapid solidification microstructures.

Flemings, Merton C.↗
NASA NTRS1981

Data-acquisition and control system for severe environments

Report evaluates control system by measuring accuracy and performance of system subcomponents, including interface wiring unit, power controller, and tape recorder. Test parameters establish variety of severe operation environments. Text features test program descriptions, sample readouts, and results. Summary of custom solar system simulator is included.

Source record↗
NASA NTRS1987

An evaluation of the communication system for the TAU mission study

The requirements for possible microwave and optical frequency communication systems to return 20 kbps from 1000 AU are compared and sample telemetry links are calculated. Microwave systems were found to have impractical parameter requirements, while the required optical system parameters are much more feasible. A first-level design of an optical communication link is presented; this design can be implemented with conservatively projected technology development. Optical background noise can be either tolerated or eliminated and it was found that TAU could detect a laser beacon from Earth even if Earth were in front of the Sun.

Metscher, B. D.↗
NASA NTRS1987

Rapid solidification of highly undercooled liquids

Melt undercooling is considered as a fundamental processing parameter for powders and for melt-spun and surface-melted samples. With reference to experimental results for Mn, Al, Al-Be, Al-Fe, and InSb-Sb powders, it is shown that the undercooling behavior in droplets is influenced by powder size, coating, melt superheat, and cooling rate. Droplet sample microstructures can be compared directly with those of rapidly quenched powders to establish the application of laboratory-scale studies to large-scale processing.

Perepezko, J. H.↗
NASA NTRS1993

The ROSAT All-Sky Survey of active binary coronae. I - Quiescent fluxes for the RS Canum Venaticorum systems

One hundred and thirty-six RS CV(n) active binary systems were observed with the ROSAT Position Sensitive Proportional Counter (PSPC) during the All-Sky Survey component of the mission. The entire sky was surveyed, which represents the largest sample of RS CV(n) systems observed to date at any wavelength, including X-rays. X-ray surface fluxes for the RS CV(n) systems are found to lie in the range 10 exp 4 to 10 exp 8 ergs/sq cm seconds. Surface flux as a function of (B - V) color is reported. A decrease in surface flux with increasing rotation period for the entire sample is observed. The rotation period provides the best stellar or orbital parameter to predict the X-ray surface flux level. The absence of correlation of F(x) or L(x) with Gamma is noted due to the fact that the coronal heating mechanism for these active stars must be magnetic in character, and the magnetic field depends on the interaction between convection and differential rotation inside the star. X-ray properties of the RS CV(n) systems with 6 cm radio and C IV UV emission systems is compared.

Dempsey, Robert C.↗
NASA NTRS1998

CFL3D User's Manual (Version 5.0)

This document is the User's Manual for the CFL3D computer code, a thin-layer Reynolds-averaged Navier-Stokes flow solver for structured multiple-zone grids. Descriptions of the code's input parameters, non-dimensionalizations, file formats, boundary conditions, and equations are included. Sample 2-D and 3-D test cases are also described, and many helpful hints for using the code are provided.

Krist, Sherrie L.↗
NASA NTRS1975

Material Response of One-Dimensional, Steady-State Transpiration Cooling in Radiative and Convective Environments

A simplified analytical solution for thermal response of a transpiration-cooled porous heat-shield material in an intense radiative-convective heating environment is presented. Essential features of this approach are "two-flux method" for radiative transfer process and "two-temperature" assumption for solid and gas temperatures. Incident radiative-convective heatings are specified as boundary conditions. Sample results are shown using porous silica with CO2 transpiration and some parameters quantitatively show the effect on this transpiration cooling system. Summarized maps for mass injection rate, porosity and blowing correction factor for radiation are obtained in order to realize such a cooling system.

Kubota, Hirotoshi↗
NASA NTRS1998

The Effect of Solution Parameters on Lysozyme Nucleation Rates and Crystal Quality

In the pursuit of strongly diffracting high quality macromolecule crystals of suitable volume, this study investigates how the formation of macromolecules in solution and their growth characteristics effect crystal volume and diffracting quality. We systematically investigated the effect of solution conditions on lysozyme nucleation rates and the volume of crystals produced. Batch crystallization plates were used in combination with a video microscope system to measure nucleation rates and crystal volume. As expected from classical nucleation theory, crystal numbers were found to increase with increases in temperature and supersaturation. Small changes in solution pH, at constant supersaturation values were found, however, to dramatically effect the number of crystals nucleated in the wells varying from 1000s to 10s in the pH range 4.0 to 5.2. Having optimized the conditions required to produce an appropriate number of crystals of a suitable volume for X-ray analysis, a large number of uniform crystals were produced under exactly the same conditions. In the X-ray analysis of more than 50 such crystals there was found a wide variation in crystal lattice parameters and data quality. The variation in X-ray quality crystal samples is thought to be related to the growth rate variation caused by growth rate dispersion seen in lysozyme crystal growth experiments.

Judge, R. A.↗
NASA NTRS2000

Estimating Long Term Surface Soil Moisture in the GCIP Area From Satellite Microwave Observations

Soil moisture is an important component of the water and energy balances of the Earth's surface. Furthermore, it has been identified as a parameter of significant potential for improving the accuracy of large-scale land surface-atmosphere interaction models. However, accurate estimates of surface soil moisture are often difficult to make, especially at large spatial scales. Soil moisture is a highly variable land surface parameter, and while point measurements are usually accurate, they are representative only of the immediate site which was sampled. Simple averaging of point values to obtain spatial means often leads to substantial errors. Since remotely sensed observations are already a spatially averaged or areally integrated value, they are ideally suited for measuring land surface parameters, and as such, are a logical input to regional or larger scale land process models. A nine-year database of surface soil moisture is being developed for the Central United States from satellite microwave observations. This region forms much of the GCIP study area, and contains most of the Mississippi, Rio Grande, and Red River drainages. Daytime and nighttime microwave brightness temperatures were observed at a frequency of 6.6 GHz, by the Scanning Multichannel Microwave Radiometer (SMMR), onboard the Nimbus 7 satellite. The life of the SMMR instrument spanned from Nov. 1978 to Aug. 1987. At 6.6 GHz, the instrument provided a spatial resolution of approximately 150 km, and an orbital frequency over any pixel-sized area of about 2 daytime and 2 nighttime passes per week. Ground measurements of surface soil moisture from various locations throughout the study area are used to calibrate the microwave observations. Because ground measurements are usually only single point values, and since the time of satellite coverage does not always coincide with the ground measurements, the soil moisture data were used to calibrate a regional water balance for the top 1, 5, and 10 cm surface layers in order to interpolate daily surface moisture values. Such a climate-based approach is often more appropriate for estimating large-area spatially averaged soil moisture because meteorological data are generally more spatially representative than isolated point measurements of soil moisture. Vegetation radiative transfer characteristics, such as the canopy transmissivity, were estimated from vegetation indices such as the Normalized Difference Vegetation Index (NDVI) and the 37 GHz Microwave Polarization Difference Index (MPDI). Passive microwave remote sensing presents the greatest potential for providing regular spatially representative estimates of surface soil moisture at global scales. Real time estimates should improve weather and climate modelling efforts, while the development of historical data sets will provide necessary information for simulation and validation of long-term climate and global change studies.

Owe, Manfred↗
NASA NTRS2002

The Steady Flow Resistance of Perforated Sheet Materials in High Speed Grazing Flows

A study was conducted to determine the effects of high speed grazing air flow on the acoustic resistance of perforated sheet materials used in the construction of acoustically absorptive liners placed in commercial aircraft engine nacelles. Since DC flow resistance of porous sheet materials is known to be a major component of the acoustic resistance of sound suppression liners, the DC flow resistance of a set of perforated face-sheets and linear 'wiremesh' face-sheets was measured in a flow duct apparatus (up to Mach 0.8). Samples were fabricated to cover typical variations in perforated face-sheet parameters, such as hole diameter, porosity and sheet thickness, as well as those due to different manufacturing processes. The DC flow resistance data from perforated sheets were found to correlate strongly with the grazing flow Mach number and the face-sheet porosity. The data also show correlation against the boundary layer displacement thickness to hole-diameter ratio. The increase in resistance with grazing flow for punched aluminum sheets is in good agreement with published results up to Mach 0.4, but is significantly larger than expected above Mach 0.4. Finally, the tests demonstrated that there is a significant increase in the resistance of linear 'wiremesh' type face-sheet materials.

Syed, Asif A.↗
NASA NTRS2006

Comparison of the Effects of Tool Geometry for Friction Stir Welding Thin Sheet Aluminum Alloys for Aerospace Applications

In this presentation, the results of a recent study on the effect of pin tool design for friction stir welding thin sheets (0.040") of aluminum alloys 2024 and 7075 are provided. The objective of this study was to investigate and document the effect of tool shoulder and pin diameter, as well as the presence of pin flutes, on the resultant microstructure and mechanical properties at both room temperature and cryogenic temperature. Specifically, the comparison between three tools will include: FSW process load analysis (tool forces required to fabricate the welds), Static Mechanical Properties (ultimate tensile strength, yield strength, and elongation), and Process window documenting the range of parameters that can be used with the three pin tools investigated. All samples were naturally aged for a period greater than 10 days. Prior research has shown 7075 may require post weld heat treatment. Therefore, an additional pair of room temperature and cryogenic temperature samples was post-weld aged to the 7075-T7 condition prior to mechanical testing.

Merry, Josh↗
NASA NTRS2006

Aerosol Indirect Effect Studies at Southern Great Plains During the May 2003 Intensive Operations Period

During May 2003 the Department of Energy's Atmospheric Radiation Measurement Program conducted an Intensive Operations Period (IOP) to measure the radiative effects of aerosol and clouds. A suite of both in situ and remote sensing measurements were available to measure aerosol and cloud parameters. This paper has three main goals: First, it focuses on comparison between in situ retrievals of the radiatively important drop effective radius r(sub e) and various satellite, airborne, and surface remote sensing retrievals of the same parameter. On 17 May 2003, there was a fortuitous, near-simultaneous sampling of a stratus cloud by five different methods. The retrievals of r(sub e) agree with one another to within approx.20%, which is approximately the error estimate for most methods. Second, a methodology for deriving a best estimate of r(sub e) from these different instruments, with their different physical properties and sampling volumes, is proposed and applied to the 17 May event. Third, the paper examines the response of r(sub e) to changes in aerosol on 3 days during the experiment and examines the consistency of remote sensing and in situ measurements of the effect of aerosol on r(sub e). It is shown that in spite of the generally good agreement in derived r(sub e), the magnitude of the response of r(sub e), to changes in aerosol is quite sensitive to the method of retrieving r(sub e) and to the aerosol proxy for cloud condensation nuclei. Nonphysical responses are sometimes noted, and it is suggested that further work needs to be done to refine these techniques.

Feingold, Graham↗
NASA NTRS2007

Stress Rupture Life Reliability Measures for Composite Overwrapped Pressure Vessels

Composite Overwrapped Pressure Vessels (COPVs) are often used for storing pressurant gases onboard spacecraft. Kevlar (DuPont), glass, carbon and other more recent fibers have all been used as overwraps. Due to the fact that overwraps are subjected to sustained loads for an extended period during a mission, stress rupture failure is a major concern. It is therefore important to ascertain the reliability of these vessels by analysis, since the testing of each flight design cannot be completed on a practical time scale. The present paper examines specifically a Weibull statistics based stress rupture model and considers the various uncertainties associated with the model parameters. The paper also examines several reliability estimate measures that would be of use for the purpose of recertification and for qualifying flight worthiness of these vessels. Specifically, deterministic values for a point estimate, mean estimate and 90/95 percent confidence estimates of the reliability are all examined for a typical flight quality vessel under constant stress. The mean and the 90/95 percent confidence estimates are computed using Monte-Carlo simulation techniques by assuming distribution statistics of model parameters based also on simulation and on the available data, especially the sample sizes represented in the data. The data for the stress rupture model are obtained from the Lawrence Livermore National Laboratories (LLNL) stress rupture testing program, carried out for the past 35 years. Deterministic as well as probabilistic sensitivities are examined.

Murthy, Pappu L. N.↗