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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 649 records · Page 36
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Investigations on the Origin of Topotactic Phase Transition of LaCoO 3 Thin Films with In Situ XRD and Ambient Pressure Hard X-ray Photoelectron Spectroscopy

With the applications of in situ X-ray diffraction (XRD), electrical I–V measurement, and ambient pressure hard X-ray photoelectron spectroscopy (AP-HAXPES), the characteristics of the topotactic phase transition of LaCoO 3 (LCO) thin films are examined. XRD measurements show clear evidence of structural phase transition (SPT) of the LCO thin films from the perovskite (PV) LaCoO 3 to the brownmillerite (BM) La 2 Co 2 O 5 phases through the intermediate La 3 Co 3 O 8 phase at a temperature of 350 °C under high-vacuum conditions, ~10 –5 mbar. The reverse SPT from BM to PV phases is also found under ambient pressure (>100 mbar) of air near 100 °C. Both observed SPTs in XRD are also identified in the electrical I–V measurements, i.e., the metallic PV phase to the insulating BM phase and vice versa. During the onset of SPTs, the bulk chemical and electronic states of LCO thin films are monitored with AP-HAXPES. The oxidation states in Co 2p spectra indicate that the oxygen vacancies are closely related to the SPT of LCO thin films. Also, the presence of enlarged band gap is observed as the SPT from PV to BM phases takes place, revealing the modified electronic properties of LCO due to the creation of oxygen vacancies. In conclusion, the analysis of valence band structures is further compared to the I–V measurements.

36 MATERIALS SCIENCE↗
DOE OSTI2026

One Beam, Dual Insights: Simultaneous Chemical and Structural Changes in Nanopatterned Ceria under Reaction Conditions

Ceria’s interaction with hydrogen can proceed through multiple chemical forms (hydride, hydroxyl, and oxyhydroxide-like), with consequences for the oxidation state, density, and morphology that are rarely tracked in the same evolving state. Here, in this work, we show that under mild H 2 (and H 2 and CO 2 ) environments nanopatterned ceria undergoes oxidation-state changes accompanied by hydrogen incorporation that increases the effective electron density, establishing the following order: CeO 2 Hy > CeO 2 > CeO 2–x Hy > CeO 2–x . In parallel, the surface roughens in a chemically specific manner, with the largest changes coinciding with conditions where incorporated hydrogen is driven to react with oxygen supplied either by air exposure between experiments or by added CO 2 . We obtained these insights by using a single X-ray beam to simultaneously perform ambient-pressure X-ray photoelectron spectroscopy and grazing-incidence X-ray scattering on the same sample spot. Single-mode measurements can miss key ceria–H 2 transformations relevant to optimizing ceria-based hydrogenation catalysts and supports.

anions↗
DOE OSTI2019

Mercury Speciation and Quantification of Hanford 241-AP-107 Tank Waste Feed and Treated Samples

This report describes the second phase of a multi year project to adapt and develop an analytical technique for the low-level determination of total mercury (HgT), elemental mercury (Hg0), and monomethyl mercury (MeHg, hereafter referred to as methyl mercury) in Hanford tank waste. The focus of Phase II was to quantify the mercury (Hg) species total, elemental, and methyl mercury from a raw sample and treated (i.e., filtered and cesium-decontaminated) waste samples originating from Hanford waste tank 241-AP 107. The focus of Phase I work was to determine if mercury species can be preconcentrated from aqueous Hanford tank waste solution onto a solid adsorbent while simultaneously eliminating or very significantly reducing the parent radionuclide activity. This was demonstrated by developing protocols for the preparation, separation, and collection of total mercury and methyl mercury onto solid adsorbents, then measuring the adsorbents for radiological content at Pacific Northwest National Laboratory’s (PNNL’s) Radiochemical Processing Laboratory (RPL) on the Hanford Site. During Phase II, the Hanford tank waste material was preserved, separated (through distillation or digestion), then collected as either solid adsorbents or into liquid distillate form at the RPL and transferred to the PNNL Marine Sciences Laboratory (MSL) in Sequim, Washington, for analysis and quantification. Quantification of total, elemental, and methyl mercury was conducted under radiological control at the MSL using the ultra trace analytical capabilities available there.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2026

Quantifying the Operational Impacts of Cyber Events on Enterprise Network Environments

The "Quantifying the Operational Impacts of Cyber Events on Enterprise Network Environments" Feasibility Study addressed the question: Can an existing (novel) class of network characterization and change detection algorithms previously developed at LLNL for internal enterprise datasets, be effectively applied to assess and measure the analytic value of features derived from datasets composed of passively collected RF and wireless network data?

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2025

Validation of a Custom Ball-on-Ring Apparatus and Consideration of Common Issues for Use in Further Testing (SULI Deliverables)

Ceramic materials are well-known for their high hardness and strength but are limited in their application due to low toughness and sudden failure. As a potential solution, inspiration can be taken from dental enamel nanostructure, where undulating rods cause cracks to branch or deflect, increasing the energy needed to cause total fracture of a ceramic part. Following the dental enamel structure, a novel ceramic which uses 3D printed Yttria stabilized Zirconia rods in an alumina matrix was developed. To test this bio-inspired ceramic material, a proper testing apparatus needed to be created and tested to verify its accuracy. For this project, a bespoke ball on ring testing apparatus was created and tested using both conventionally sintered alumina disks and purchased alumina disks to validate its accuracy. By comparing the Weibull distribution of rupture strengths measured by the tests to literature values, it was shown that the testing frame had a wide distribution of strength which did not align with literature values on the lower end. Through fractography, it was found that some samples fractured from the contact stress induced by the ball indenter, which could not be used to calculate rupture strength. This fracture was often linked to low stress to failure, which was initiated by a flaw on the surface near the indenter which acted as a stress concentrator. Removal of these samples from the data set increased the accuracy of the reported rupture strength values for the ceramic. Considering the equations for the magnitude of contact and flexural strength, along with observations of initiating flaws, several measures can be taken for testing the bio-inspired composite. These measures include proper polishing of both sides of the sample, reducing sample thickness, and potentially using a softer indenter material.

36 - MATERIALS SCIENCE↗
NASA NTRS1985

Space radiation studies for the reporting period, June 1983 - July 1984

Two Active Radiation Dosimeters (ARD's) flown on Spacelab 1, performed without fault and were returned to Space Science Laboratory, MSFC for recalibration. During the flight in December 1983, performance was monitored at the Huntsville Operations Center (HOSC). Despite some problems with the Shuttle data system handling the VFI, it could be established that the ARD's were operating normally. Postflight calibrations of both units determined that sensitivities were essentially unchanged from preflight values. Flight tapes were received for approximately 60% of the flight and it appears that this is the total available. The next phase of effort will involve close collaboration with Space Science Laboratory, MSFC, in the analysis of this data. The Nuclear Radiation Monitor (NRM) was under assembly and testing at MSFC. Support was rendered in the areas of materials control and parts were supplied for the supplementary heaters, dome gas-venting device and photomultiplier tube housing. Performance characteristics of some flight-space photomultipliers were measured.

Source record↗
NASA NTRS1994

Space Experiments with Particle Accelerators: SEPAC

The Space Experiments with Particle Accelerators (SEPAC), which flew on the Atmospheric Laboratory for Applications and Science (ATLAS) 1 mission, used new techniques to study natural phenomena in the Earth's upper atmosphere, ionosphere and magnetosphere by introducing energetic perturbations into the system from a high power electron beam with known characteristics. Properties of auroras were studied by directing the electron beam into the upper atmosphere while making measurements of optical emissions. Studies were also performed of the critical ionization velocity phenomenon.

Burch, J. L.↗
NASA NTRS2005

Generation and Performance of Automated Jarosite Mineral Detectors for Vis/NIR Spectrometers at Mars

Sulfate salt discoveries at the Eagle and Endurance craters in Meridiani Planum by the Mars Exploration Rover Opportunity have proven mineralogically the existence and involvement of water in Mars past. Visible and near infrared spectrometers like the Mars Express OMEGA, the Mars Reconnaissance Orbiter CRISM and the 2009 Mars Science Laboratory Rover cameras are powerful tools for the identification of water-bearing salts and other high priority minerals at Mars. The increasing spectral resolution and rover mission lifetimes represented by these missions currently necessitate data compression in order to ease downlink restrictions. On board data processing techniques can be used to guide the selection, measurement and return of scientifically important data from relevant targets, thus easing bandwidth stress and increasing scientific return. We have developed an automated support vector machine (SVM) detector operating in the visible/near-infrared (VisNIR, 300-2500 nm) spectral range trained to recognize the mineral jarosite (typically KFe3(SO4)2(OH)6), positively identified by the Mossbauer spectrometer at Meridiani Planum. Additional information is included in the original extended abstract.

Gilmore, M. S.↗
NASA NTRS2013

Robust Platinum Resistor Thermometer (PRT) Sensors and Reliable Bonding for Space Missions

Platinum resistance thermometers (PRTs) provide accurate temperature measurements over a wide temperature range and are used extensively on space missions due to their simplicity and linearity. A standard on spacecraft, PRTs are used to provide precision temperature control and vehicle health assessment. This paper reviews the extensive reliability testing of platinum resistor thermometer sensors (PRTs) and bonding methods used on the Mars Science Laboratory (MSL) mission and for the upcoming Soil Moisture Active Passive (SMAP) mission. During the Mars Exploration Rover (MER) mission, several key, JPL-packaged PRTs failed on those rovers prior to and within 1-Sol of landing due to thermally induced stresses. Similar failures can be traced back to other JPL missions dating back thirty years. As a result, MSL sought out a PRT more forgiving to the packaging configurations used at JPL, and extensively tested the Honeywell HRTS-5760-B-U-0-12 sensor to successfully demonstrate suitable robustness to thermal cycling. Specifically, this PRT was cycled 2,000 times, simulating three Martian winters and summers. The PRTs were bonded to six substrate materials (Aluminum 7050, treated Magnesium AZ231-B, Stainless Steel 304, Albemet, Titanium 6AL4V, and G-10), using four different aerospace adhesives--two epoxies and two silicones--that conformed to MSL's low out-gassing requirements. An additional epoxy was tested in a shorter environmental cycling test, when the need for a different temperature range adhesive was necessary for mobility and actuator hardware late in the fabrication process. All of this testing, along with electrostatic discharge (ESD) and destructive part analyses, demonstrate that this PRT is highly robust, and not subject to the failure of PRTs on previous missions. While there were two PRTs that failed during fabrication, to date there have been no in-flight PRT failures on MSL, including those on the Curiosity rover. Since MSL, the sensor has gone through a change in construction such that the manufacturer significantly restricts the minimum temperature. However, significant subsequent testing was performed with this new version of the part to show that it indeed is still robust to at least Mars minimum temperatures of -135(sup o)C. The additional completed testing will be described. This work has resulted in a successful sensor package qualification and a reliable bonding method suitable for use over large temperature extremes.

dectector↗
NASA NTRS2013

Robust Platinum Resistor Thermometer (PRT) Sensors and Reliable Bonding for Space Missions

Platinum resistance thermometers (PRTs) provide accurate temperature measurements over a wide temperature range and are used extensively on space missions due to their simplicity and linearity. A standard on spacecraft, PRTs are used to provide precision temperature control and vehicle health assessment. This paper reviews the extensive reliability testing of platinum resistor thermometer sensors (PRTs) and bonding methods used on the Mars Science Laboratory (MSL) mission and for the upcoming Soil Moisture Active Passive (SMAP) mission. During the Mars Exploration Rover (MER) mission, several key, JPL-packaged PRTs failed on those rovers prior to and within 1-Sol of landing due to thermally induced stresses. Similar failures can be traced back to other JPL missions dating back thirty years. As a result, MSL sought out a PRT more forgiving to the packaging configurations used at JPL, and extensively tested the Honeywell HRTS-5760-B-U-0-12 sensor to successfully demonstrate suitable robustness to thermal cycling. Specifically, this PRT was cycled 2,000 times, simulating three Martian winters and summers. The PRTs were bonded to six substrate materials (Aluminum 7050, treated Magnesium AZ231-B, Stainless Steel 304, Albemet, Titanium 6AL4V, and G-10), using four different aerospace adhesives--two epoxies and two silicones--that conformed to MSL's low out-gassing requirements. An additional epoxy was tested in a shorter environmental cycling test, when the need for a different temperature range adhesive was necessary for mobility and actuator hardware late in the fabrication process. All of this testing, along with electrostatic discharge (ESD) and destructive part analyses, demonstrate that this PRT is highly robust, and not subject to the failure of PRTs on previous missions. While there were two PRTs that failed during fabrication, to date there have been no in-flight PRT failures on MSL, including those on the Curiosity rover. Since MSL, the sensor has gone through a change in construction such that the manufacturer significantly restricts the minimum temperature. However, significant subsequent testing was performed with this new version of the part to show that it indeed is still robust to at least Mars minimum temperatures of -135 degrees Centigrade. The additional completed testing will be described. This work has resulted in a successful sensor package qualification and a reliable bonding method suitable for use over large temperature extremes

Platinum Resistor Thermometer (PRT)↗
NASA NTRS2016

Final Mission and Navigation Design for the 2016 Mars InSight Mission

Project Overview: NASA’s 12th Discovery Program mission that will place a single geophysical lander on Mars to study its deep interior using seismic (tidal, marsquake, and impact), rotational, and thermal measurements -First mission to unveil the composition, structure and thermal state of martian crust, mantle and core; Rebuild of the Phoenix flight system, upgraded with Juno/GRAIL avionics -Phoenix cruise stage: 3-axis stabilized, 3.2 square meter UTJ (Ultra Triple-Junction) solar array, X-band telecom -Phoenix aeroshell (heat shield, backshell, parachute) -Phoenix lander: radar, pulsed thrusters, legs, payload deck, 5.1 square meter UTJ solar arrays, two redundant Li-ion batteries, UHF (Ultra High Frequency)/X-band telecom -Dual string: Internally or functionally-redundant equipment; Science Payload -SEIS (Seismic Experiment for Interior Structure) / CNES (Centre National d’Etudes Spatiales); Three-axis seismometry, to measure seismic waves traveling through the interior -HP3 (Heat Flow and Physical Properties Probe) / DLR (German Aerospace Center) -Subsurface heat probe, to measure the heat flux from the interior - RISE (Rotation and Interior Structure Experiment) / JPL (Jet Propulsion Laboratory) -Radiometric geodesy, to determine precession & nutation of the planet’s rotation axis. 2016 Disclaimer: The InSight launch in 2016 was suspended due to critical issues with the Seismic Experiment for Interior Structure (SEIS) instrument that could not be fixed prior to the planned launch period. This presentation and its corresponding paper represent the state of the design for the 2016 mission. No attempt has been made to reflect the latest developments. [2018 Note: InSight (Mars Lander) was later launched and arrived on Mars on Nov. 26, 2018.]

Abilleira, F.↗
NASA NTRS1994

Wind Prelaunch Mission Operations Report (MOR)

The National Aeronautics and Space Administration (NASA) Wind mission is the first mission of the Global Geospace Science (GGS) initiative. The Wind laboratory will study the properties of particles and waves in the region between the Earth and the Sun. Using the Moon s gravity to save fuel, dual lunar swing-by orbits enable the spacecraft to sample regions close to and far from the Earth. During the three year mission, Wind will pass through the bow shock of Earth's magnetosphere to begin a thorough investigation of the solar wind. Mission objectives require spacecraft measurements in two orbits: lunar swing- by ellipses out to distances of 250 Earth radii (RE) and a small orbit around the Lagrangian point L-l that remains between the Earth and the Sun. Wind will be placed into an initial orbit for approximately 2 years. It will then be maneuvered into a transition orbit and ultimately into a halo orbit at the Earth-Sun L-l point where it will operate for the remainder of its lifetime. The Wind satellite development was managed by NASA's Goddard Space Flight Center with the Martin Marietta Corporation, Astro-Space Division serving as the prime contractor. Overall programmatic direction was provided by NASA Headquarters, Office of Space Science. The spacecraft will be launched under a launch service contract with the McDonnell Douglas Corporation on a Delta II Expendable Launch Vehicle (ELV) within a November l-l4, 1994 launch window. The Wind spacecraft carries six U.S. instruments, one French instrument, and the first Russian instrument ever to fly on an American satellite. The Wind and Polar missions are the two components of the GGS Program. Wind is also the second mission of the International Solar Terrestrial Physics (ISTP) Program. The first ISTP mission, Geotail, is a joint project of the Institute of Space and Astronautical Science of Japan and NASA which launched in 1992. The Wind mission is planned to overlap Geotail by six months and Polar by one year. The Wind and Polar missions, together with the Geotail mission (launched on July 24, 1992) and supporting equatorial measurements, will provide simultaneous data to enable the study of solar wind input to the magnetosphere and key elements of the magnetospheric response: ring current energy storage, geomagnetic tail energy storage, and ionospheric energy input.

Source record↗
DOE OSTI2024

Forecasting high-dimensional spatio-temporal systems from sparse measurements

This paper introduces a new neural network architecture designed to forecast high-dimensional spatio-temporal data using only sparse measurements. The architecture uses a two-stage end-to-end framework that combines neural ordinary differential equations (NODEs) with vision transformers. Initially, our approach models the underlying dynamics of complex systems within a low-dimensional space; and then it reconstructs the corresponding high-dimensional spatial fields. Many traditional methods involve decoding high-dimensional spatial fields before modeling the dynamics, while some other methods use an encoder to transition from high-dimensional observations to a latent space for dynamic modeling. In contrast, our approach directly uses sparse measurements to model the dynamics, bypassing the need for an encoder. This direct approach simplifies the modeling process, reduces computational complexity, and enhances the efficiency and scalability of the method for large datasets. We demonstrate the effectiveness of our framework through applications to various spatio-temporal systems, including fluid flows and global weather patterns. Although sparse measurements have limitations, our experiments reveal that they are sufficient to forecast system dynamics accurately over long time horizons. Our results also indicate that the performance of our proposed method remains robust across different sensor placement strategies, with further improvements as the number of sensors increases. This robustness underscores the flexibility of our architecture, particularly in real-world scenarios where sensor data is often sparse and unevenly distributed.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2022

WHONDRS Surface Water Dissolved Organic Carbon and FTICR-MS across Stream Orders in Four United States Watersheds in 2019 and 2020 (v3)

This dataset supports the broader Watershed Rules of Life (WROL) study examining spatial and temporal biogeochemical and microbial relationships across the Connecticut River, Deschutes River, Gunnison River, and Willamette River watersheds. The dataset provides geochemistry and organic matter characterization data generated from surface water collected from August 2019 to September 2020 in Colorado, Connecticut, Oregon, and Vermont. Related data were collected and will be published separately in collaboration with P. A. Raymond and B. C. Crump as part of WROL. This dataset is comprised of one folder containing (1) file-level metadata; (2) data dictionary; (3) readme; (4) field metadata; (5) dissolved organic carbon (DOC, measured as non-purgeable organic carbon, NPOC) data and averages; (6) surface water sampling protocol; (7) methods codes; (8) international generic sample number (IGSN) mapping file; and (9) a folder of high resolution characterization of organic matter via 12 Tesla Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) generated through the Environmental Molecular Sciences Laboratory (EMSL; https://www.pnnl.gov/environmental-molecular-sciences-laboratory). The FTICR folder contains two subfolders, one containing the .xml data files and the other containing instructions for using Formularity (https://omics.pnl.gov/software/formularity) and an R script to process the data based on the user's specific needs. All files are .csv, .pdf, .R, .ref, or .xml. This data package was originally published in October 2022. It was updated in July 2023 (v2) and again in November 2023 (v3). See the change history section in the readme for more details.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1992

SLS-1: The first dedicated life sciences shuttle flight

Spacelab Life Sciences 1 was the first space laboratory dedicated to life science research. It was launched into orbit in early June 1991 aboard the space shuttle Columbia. The data from this flight have greatly expanded our knowledge of the effects of microgravity on human physiology as data were collected in-flight, not just pre and post. Principal goals of the mission were the measurement of rapid and semichronic (8 days) changes in the cardiovascular and cardiopulmonary systems during the flight and then to measure the rate of readaptation following return to Earth. Results from the four teams involved in that research will be presented in this panel. In addition to the cardiovascular-cardiopulmonary research, extensive metabolic studies encompassed fluid, electrolyte and energy balance, renal function, hematology and musculoskeletal changes. Finally, the crew participated in several neurovestibular studies. Overall, the mission was an outstanding success and has provided much new information on the lability of human responses to the space environment.

Phillips, Robert W.↗
NASA NTRS2004

Helium Production of Prompt Neutrinos on the Moon

The subject of conducting fundamental physics and astronomy experiments on the lunar surface continues to be of interest in the planetary science community. Such an inquiry necessarily requires an analysis of the backscatter albedos produced by Galactic cosmic rays (GCRs) when they directly impact the lunar regolith. Unlike the Earth, this happens because the Moon has only a tenuous exosphere. Such secondary radiation constitutes a background that obscures and interferes with measurements conducted in the normal sense of laboratory physics on Earth. Our previous investigations using recent enhancements in the Monte Carlo program known as FLUKA included the production of charged particles, neutrons, photons, and neutrinos by the impact of Galactic protons. That investigation is extended here to include the effect of ionized helium, He-4, or a particles. Because high-energy GCRs excite planetary regoliths into giving rise to charmed mesons, neutrinos are produced. Thus a connection is established for the GCR helium production of prompt neutrinos on the Moon using the physics of charm.

Andersen, V.↗
NASA NTRS2008

Heating Augmentation in Laminar Flow Due to Heat-Shield Cavities on the Project Orion CEV

An experimental study has been conducted to assess the effects of compression pad cavities on the aeroheating environment of the Project Orion CEV heat-shield at laminar conditions. Testing was conducted in Mach 6 and Mach 10 perfect-gas wind tunnels to obtain heating measurements on and around the compression pads using global phosphor thermography. Consistent trends in heating augmentation levels were observed in the data and correlations of average and maximum heating at the cavities were formulated in terms of the local boundary-layer parameters and cavity dimensions. Additional heating data from prior testing of Genesis and Mars Science Laboratory models were also examined to extend the parametric range of cavity heating correlations.

Hollis, Brian R.↗