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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Argon added to helium during gas tungsten arc cover-pass welding in the horizontal position results in a better controlled wider bead width, increased arc stability, and reduction in heat input. Adequate filler material wetness and penetration pass coverage is possible with only one pass.
Filling honeycomb matrix with deaerated paste filler
Carbon and graphite research and development, with detailed data on Santa Maria coke as filler material
Rare earth trifluorides have potential use as lubricating fillers for mechanical carbons and as coatings on metallic substrates. Friction experiments show that they are effective in reducing metallic wear.
Gas-tungsten arc welding with a filler of Rene-41 produces strong welded joints. When Rene-41 is used, resistance to strain-age cracking is greatly increased by post-weld solution annealing in an inert atmosphere. Mechanical properties of Rene-41 and Hastelloy-W are compared.
Electrically conductive plastics fabrication and applications limitations, discussing plastic matrix materials loaded with various conductive fillers
Teflon crosshatched ablation patterns elimination by grooving or glass filler addition
Liners for nitric and hydrofluoric acid tanks show no sign of deterioration after 18 months of continuous use. Each side of each edge of the polypropylene sheets is chamfered, and sheets are welded from both sides with polypropylene filler rod and a special hot-air welding torch.
Metal spinning forms combustion chamber sections and nozzle sections, arc welding joints sections to form rocket motor. Hastelloy-X as filler results in slightly weaker weld than the TD nickel weld, but permits formation of larger rocket motor than is otherwise possible.
Space shuttle systems structural joints thermal control, discussing contact conductance with and without interstitial fillers
Ablative polymers synthesis from formaldehyde, phenols and ethers reaction products, discussing char yield, thermally stable fillers incorporation and thermogravimetric analysis
Handbook describes relationship between phase-change materials and more conventional thermal control techniques and discusses materials' space and terrestrial applications. Material properties of most promising phase-change materials and purposes and uses of metallic filler materials in phase-change material composites are provided.
This handbook is intended to provide theory and data needed by the thermal design engineer to bridge the gap between research achievements and actual flight systems, within the limits of the current state of the art of phase change materials (PCM) technology. The relationship between PCM and more conventional thermal control techniques is described and numerous space and terrestrial applications of PCM are discussed. Material properties of the most promising PCMs are provided; the purposes and use of metallic filler materials in PCM composites are presented; and material compatibility considerations relevant to PCM design are included. The engineering considerations of PCM design are described, especially those pertaining to the thermodynamic and heat transfer phenomena peculiar to PCM design. Methods of obtaining data not currently available are presented. The special problems encountered in the space environment are described. Computational tools useful to the designer are discussed. In summary, each aspect of the PCM problem important to the design engineer is covered to the extent allowed by the scope of this effort and the state of the art.
Preliminary results of the research on carbon and graphite accomplished during this report period are presented. Included are: particle characteristics of Santa Maria fillers, compositions and density data for hot-molded Santa Maria graphites, properties of hot-molded Santa Maria graphites, and properties of hot-molded anisotropic graphites. Ablation-resistant graphites are also discussed.
The effects of grinding on Santa Maria coke are considered, as well as the production of resin-bonded graphite from the coke. Kynol fibers, properties and purities of coal tar pitches, carbonization of resin components, synthesis of gamma BL (4-furfuryl 2-pentenoic acid gamma lactone), and a glass-like carbon powder for use as a filler are also discussed. The hydrogen contents of commercial cokes and graphites are tabulated, and a quantimet image-analyzing computer and its operation are described.
A literature survey was conducted to collect material properties data on all advanced high temperature materials. Three of these, Y2O3-stabilized ZrO2, ThO2, and ZrB2 with additives of C and SiC were selected for further study. Stabilized ZrO2 and ThO2 were found to have higher temperature oxidation resistance than any metal and great potential for use in advanced biowaste resistojets. ZrO2 has a lower electrical resistivity and sublimation and a higher creep endurance strength. ZrO2 and ThO2 tubular heat exchangers, electrically heated indirectly, were evaluated in short tests to about 1900 K in flowing CO2. ZrO2 was subjected to N2, H2, H2O and vacuum as well. X-ray diffraction and fluorescence analyses were made. The metal-to-ceramic seal technology for ZrO2 and ThO2 was developed using chemical vapor deposition of tantalum for metallizing and 82 Au - 18 Ni filler braze.
A study to correlate stress wave emission characteristics with fracture in welded and unwelded aluminum alloys tested at room and cryogenic temperature is reported. The stress wave emission characteristics investigated were those which serve to presage crack instability; viz., a marked increase in:(1) signal amplitude; (2) signal repetition rate; and (3) the slope of cumulative count plotted versus load. The alloys were 7075-T73, 2219-T87 and 2014-T651, welded with MIG and TIG using 2319 and 4043 filler wire. The testing was done with both unnotched and part-through-crack (PTC) tension specimens and with 18-in.-dia subscale pressure vessels. In the latter testing, a real time, acoustic emission, triangulation system was used to locate the source of each stress wave emission. With such a system, multiple emissions from a given location were correlated with defects found by conventional nondestructive inspection.
An applied research program is considered for a preliminary design and development of a flexible ablative covering for the space shuttle vehicle that could be easily replaced and/or refurbished. The program was structured to concentrate resources on the major technical problem areas associated with the flexible ablator concept. These areas included: (1) fabrication of a suitable woven carpet reinforcement, (2) modification of a flexible ablator formulation for filling the woven carpet construction, and (3) testing of the flexible ablator concept. Several approaches were evaluated to obtain a flexible ablator. The final recommended solution was one in which the ablative filler was based on a low-density formulation of the elastomeric shield material series (ESM). The preferred approach is one in which a light-weight fabric backing is bonded to preformed and fully cured ESM, and the composite tufted with Astroquartz fiber to the desired tuft or pile density. Ablation tests performed in a hyperthermal arc facility demonstrated the ablation performance of the concept and overshoot capability of the system.