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At least 631 records · Page 35

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DOE OSTI2026

AutoSAC-Automated Sample Activation Calculation on VULCAN

AutoSAC is an automated python program to conduct sample activation calculation immediately after neutron scattering experiment on VULCAN. AutoSAC takes account of sample dimensions, compositions, forms, sample environments, neutron beam configurations, neutron scattering history, and proton charged resolved beam power etc., and uses a simplified method to rapidly estimate the radioactivity at end of beam or after. It generates a draft report per sample and repository of radioactivity per measurement and provides feedback of current radioactivity and decay time back to a neutron proposal Slack channel to inform users immediately on sample handling. It also utilizes either the sample note field in EPICS or sample composition or thickness correction and takes slack prompt or command to conduct post-beam SAC by demand. The program can be shared to be used in other beamlines at spallation neutron source with modified instrument configurations including instrument specific characteristic beam fluxes.

An, Ke [Oak Ridge National Laboratory (ORNL), Oak ↗

DOE OSTI2024

Towards Construction of a Novel Nanometer-Resolution MeV-STEM for Imaging Thick Frozen Biological Samples

Driven by life-science applications, a mega-electron-volt Scanning Transmission Electron Microscope (MeV-STEM) has been proposed here to image thick frozen biological samples as a conventional Transmission Electron Microscope (TEM) may not be suitable to image samples thicker than 300–500 nm and various volume electron microscopy (EM) techniques either suffering from low resolution, or low speed. The high penetration of inelastic scattering signals of MeV electrons could make the MeV-STEM an appropriate microscope for biological samples as thick as 10 μm or more with a nanoscale resolution, considering the effect of electron energy, beam broadening, and low-dose limit on resolution. The best resolution is inversely related to the sample thickness and changes from 6 nm to 24 nm when the sample thickness increases from 1 μm to 10 μm. To achieve such a resolution in STEM, the imaging electrons must be focused on the specimen with a nm size and an mrad semi-convergence angle. This requires an electron beam emittance of a few picometers, which is ~1000 times smaller than the presently achieved nm emittance, in conjunction with less than 10 -4 energy spread and 1 nA current. We numerically simulated two different approaches that are potentially applicable to build a compact MeV-STEM instrument: (1) DC (Direct Current) gun, aperture, superconducting radio-frequency (SRF) cavities, and STEM column; (2) SRF gun, aperture, SRF cavities, and STEM column. Beam dynamic simulations show promising results, which meet the needs of an MeV-STEM, a few-picometer emittance, less than 10 -4 energy spread, and 0.1–1 nA current from both options. Also, we designed a compact STEM column based on permanent quadrupole quintuplet, not only to demagnify the beam size from 1 μm at the source point to 2 nm at the specimen but also to provide the freedom of changing the magnifications at the specimen and a scanning system to raster the electron beam across the sample with a step size of 2 nm and the repetition rate of 1 MHz. This makes it possible to build a compact MeV-STEM and use it to study thick, large-volume samples in cell biology.

36 MATERIALS SCIENCE↗

DOE OSTI2022

The Solar System calcium isotopic composition inferred from Ryugu samples

The Hayabusa2 spacecraft has returned samples from the Cb-type asteroid (162173) Ryugu to Earth. Previous petrological and chemical analyses support a close link between Ryugu and CI chondrites that are presumed to be chemically the most primitive meteorites with a solar-like composition. However, Ryugu samples are highly enriched in Ca compared to typical CI chondrites. To identify the cause of this discrepancy, here we report stable Ca isotopic data (expressed as δ 44/40 Ca SRM915a ) for returned Ryugu samples collected from two sites. We found that samples from both sites have similar δ 44/40 Ca SRM915a (0.58 ± 0.03 ‰ and 0.55 ± 0.08 ‰, 2 s.d.) that fall within the range defined by CIs. This isotopic similarity suggests that the Ca budget of CIs and Ryugu samples is dominated by carbonates, and the variably higher Ca contents in Ryugu samples are due to the abundant carbonates. Precipitation of carbonates on Ryugu likely coincided with a major episode of aqueous activity dated to have occurred ~5 Myr after Solar System formation. Based on the pristine Ryugu samples, the average δ 44/40 Ca SRM915a of the Solar System is defined to be 0.57 ± 0.04 ‰ (2 s.d.).

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS1971

Description of core samples returned by Apollo 12

Three core samples were collected by the Apollo 12 astronauts. Two are single cores, one of which (sample 12026) was collected close to the lunar module during the first extravehicular activity period and is 19.3 centimeters long. The second core (sample 12027) was collected at Sharp Crater during the second extravehicular activity period and is 17.4 centimeters long. The third sample is a double core (samples 12025 and 12028), which was collected near Halo Crater during the second extravehicular activity period. Unlike the other cores, the double-drive-tube core sample has complex layering with at least 10 clearly defined stratigraphic units. This core sample is approximately 41 centimeters long.

Lindsay, J. F.↗

NASA NTRS1972

Documentation of Apollo 15 samples

A catalog is presented of the documentation of Apollo 15 samples using photographs and verbal descriptions returned from the lunar surface. Almost all of the Apollo 15 samples were correlated with lunar surface photographs, descriptions, and traverse locations. Where possible, the lunar orientations of rock samples were reconstructed in the lunar receiving laboratory, using a collimated light source to reproduce illumination and shadow characteristics of the same samples shown in lunar photographs. In several cases, samples were not recognized in lunar surface photographs, and their approximate locations are known only by association with numbered sample bags used during their collection. Tables, photographs, and maps included in this report are designed to aid in the understanding of the lunar setting of the Apollo 15 samples.

Sutton, R. L.↗

NASA NTRS1973

Chemical composition of Apollo 15, 16, and 17 samples

The authors analyzed 22 Apollo 15 samples, 21 Apollo 16 samples, 4 Luna 20 samples, and 6 Apollo 17 samples for 26 to 30 major, minor, and trace elements by instrumental neutron activation analysis (INAA). Major attention is given to Apollo 16 results and recent Apollo 17 data. The roster of elements via INAA has been extended to include Nd, Ni, Ir, and Au in the Apollo 16 and 17 samples. The latter three elements are highly abundant in these samples. Sample preparation, activation conditions, and the detailed INAA analytical procedure are essentially the same as reported by Laul and Schmitt (1973).

Laul, J. C.↗

NASA NTRS1974

Digital redesign of continuous systems by matching of states at multiple sampling periods

This paper presents a method of digital approximation of a continuous-data system by the matching of states at multiple sampling periods. Two alternate methods are presented; one method samples the states every sampling period, and alters the forward and feedback gains, so as to match the states of the two systems at the end of N sampling periods. The second method requires the sampling of the states every N sampling periods, with the change of gains at each sampling period. An illustrative example using the one-axis dynamics of the Skylab Satellite is presented.

Yackel, R. A.↗

NASA NTRS1975

Stability of multirate sampled-data systems

Current adaptive sampling schemes that can be used in sampled-data systems with variable rate sampling does not guarantee the stability of the resulting closed-loop system. A study was undertaken with the objective of finding a stable control law for multirate sampled-data systems. The problem is formulated such that the sampling interval is selected from a set of fixed number of sample intervals. A necessary and sufficient condition under which these types of systems can be stabilized is given. For a certain subclass of these types of systems, a sampling selection algorithm is given which results in a stable closed-loop system.

Stanford, D. P.↗

NASA NTRS1974

Preservation of lunar core samples - Preparation and interpretation of three-dimensional stratigraphic sections

Preservation and analysis of core samples collected from the lunar regolith are discussed. The objectives of core sampling are described together with the core-sampling equipment used in the Apollo program. The effects of disaggregation in core samples are summarized, and ways to preserve the stratigraphy in these samples are reviewed, particularly partial impregnation of samples with polybutyl methacrylate. It is shown that stratigraphic sections preserved in this way reveal individual fragments of the regolith in their original positions, primary and secondary depositional structures related to lunar processes, and the nature and extent of deformations caused by sampling equipment. It is concluded that since the core sedimentary structures indicate complex three-dimensional variations in the regolith, quantitative models of regolith evolution must allow for distinctive local histories as well as irregular reworking and deposition events due to impact processes.

Fryxell, R.↗

NASA NTRS1971

Plural output optimetric sample cell and analysis system

An apparatus suitable for receiving a sample for optimetric analysis includes a sample cell comprising an opaque hollow tube. Several apertures are defined in the wall of the tubing and a lens barrel which extends beyond to opposite surfaces of the wall is supported within at least one of the apertures. A housing is provided with one channel for receiving the sample cell and a series of channels extending from the exterior housing to the sample cell apertures. A filter element is housed in each of these latter channels. These channels slidingly receive an excitation light source for a photodetector cell to permit selective focusing. A sample cell containing at least three apertures in the walls can be mounted for rotation relative to a light source or photoconduction means for simultaneous or alternative optimetric determination of the components of a single sample. The sample cell is fabricated by supporting a lens barrel within the aperture. A molten portion of glass is deposited in the lens barrel and cooled while in a horizontal position to form a lens having an acceptable angle.

Haley, F. C.↗

NASA NTRS1979

Recovering the spectrum of a narrow-band process from syncopated samples

A nonuniform sampling strategy, phase quadrature sampling, in which a process of bandwith B is sampled at rate B in each of two channels where the two channels are pi/2 out of phase at frequency B is described. Phase quadrature sampling is a special case of sampling, where the phase between channels is fixed but arbitrary. A simple method for recovering the spectrum of the input process from syncopated samples is derived. The derivation indicates what values of phase between channels result in lossless sampling.

Milenkovic, P. H.↗

NASA NTRS1978

Luna 24: 90-150 micrometer fraction - Implications for remote sampling of regolith

An analysis of the mineral grains and glasses found in the 90 to 150 micron fraction of the Luna 24 core sample is presented and implications for the automatic collection of planetary and asteroidal regoliths are discussed. Electron microprobe analysis for pyroxene, olivine, plagioclase, opaque minerals and glass in samples at various depths indicate that polymineralic grains have compositions similar to those of gabbroic and basaltic fragments from coarser samples, while monomineralic grains contain an additional population of Mg-rich olivines and pyroxene. Most of the glasses are found to be related to mare basalts or local regolith, with nonmare material represented by glasses of highland basalt and low K Fra Mauro composition. It is concluded that as regards mineralogy and petrology, a single grab sample would have been as useful and a series of grab samples on a long traverse would have been more useful than the Luna 24 core sample, with the fine sample being more informative than the coarse.

Papp, H. A.↗

NASA NTRS1981

CCD correlated quadruple sampling processor

A correlated quadruple sampling processor for improved signal-to-noise ratio in the output of a charge-coupled device (CCD) is comprised of: switching means for momentarily clamping a CCD signal line at a first reference level A before a CCD data pulse and then obtaining a first data sample B with respect to the reference A during a CCD data pulse, and storing the positive sample B-A; switching means for momentarily clamping the CCD signal line a second time at the level C during the presence of the CCD data pulse and then obtaining a second data sample D with respect to the reference level C after the CCD data pulse, and storing the negative sample D-C; and means for obtaining the difference between the stored samples +(B-A) and -(D-C), thus increasing the net signal amplitude by a factor of about 2 while the noise would be increased by only a factor of square root of 2 since there will be no correlation in the noise between the double samples +(B-A) and -(D-C) effectively added.

Gaalema, S. D.↗

NASA NTRS1982

Studies with sample conductivity, insertion rates, and particle deflection in a continuous flow electrophoresis system

The continuous flow electrophoresis system makes electrophoresis possible in a free-flowing film of aqueous electrolyte medium. The sample continuously enters the electrolyte at the top of the chamber and is subjected to the action of a lateral dc field. This divides the sample into fractions since each component has a distinctive electrophoretic mobility. Tests were made using monodisperse polystyrene latex microspheres to determine optimum sample conductivity, insertion rates and optimum electric field applications as baseline data for future STS flight experiments. Optimum sample flow rates for the selected samples were determined to be approximately 26 micro-liters/min. Experiments with samples in deionized water yielded best results and voltages in the 20 V/cm to 30 V/cm range were optimum. Deflections of formaldehyde fixed turkey and bovine erythrocytes were determined using the continuous flow electrophoresis system. The effects of particle interactions on sample resolution and migration in the chamber was also evaluated.

Williams, G., Jr.↗

NASA NTRS1983

Influence of sampling rate on the calculated fidelity of an aircraft simulation

One of the factors that influences the fidelity of an aircraft digital simulation is the sampling rate. As the sampling rate is increased, the calculated response of the discrete representation tends to coincide with the response of the corresponding continuous system. Because of computer limitations, however, the sampling rate cannot be increased indefinitely. Moreover, real-time simulation requirements demand that a finite sampling rate be adopted. In view of these restrictions, a study was undertaken to determine the influence of sampling rate on the response characteristics of a simulated aircraft describing short-period oscillations. Changes in the calculated response characteristics of the simulated aircraft degrade the fidelity of the simulation. In the present context, fidelity degradation is defined as the percentage change in those characteristics that have the greatest influence on pilot opinion: short period frequency omega, short period damping ratio zeta, and the product omega zeta. To determine the influence of the sampling period on these characteristics, the equations describing the response of a DC-8 aircraft to elevator control inputs were used. The results indicate that if the sampling period is too large, the fidelity of the simulation can be degraded.

Howard, J. C.↗

NASA NTRS1984

Sampling system for wheat (Triticum aestivum L) area estimation using digital LANDSAT MSS data and aerial photographs

A procedure to estimate wheat (Triticum aestivum L) area using sampling technique based on aerial photographs and digital LANDSAT MSS data is developed. Aerial photographs covering 720 square km are visually analyzed. To estimate wheat area, a regression approach is applied using different sample sizes and various sampling units. As the size of sampling unit decreased, the percentage of sampled area required to obtain similar estimation performance also decreased. The lowest percentage of the area sampled for wheat estimation with relatively high precision and accuracy through regression estimation is 13.90% using 10 square km as the sampling unit. Wheat area estimation using only aerial photographs is less precise and accurate than those obtained by regression estimation.

Parada, N. D. J.↗

NASA NTRS1983

A sampling system for estimating the cultivation of wheat (Triticum aestivum L) from LANDSAT data

Using digitally processed MSS/LANDSAT data as auxiliary variable, a methodology to estimate wheat (Triticum aestivum L) area by means of sampling techniques was developed. To perform this research, aerial photographs covering 720 sq km in Cruz Alta test site at the NW of Rio Grande do Sul State, were visually analyzed. LANDSAT digital data were analyzed using non-supervised and supervised classification algorithms; as post-processing the classification was submitted to spatial filtering. To estimate wheat area, the regression estimation method was applied and different sample sizes and various sampling units (10, 20, 30, 40 and 60 sq km) were tested. Based on the four decision criteria established for this research, it was concluded that: (1) as the size of sampling units decreased the percentage of sampled area required to obtain similar estimation performance also decreased; (2) the lowest percentage of the area sampled for wheat estimation with relatively high precision and accuracy through regression estimation was 90% using 10 sq km s the sampling unit; and (3) wheat area estimation by direct expansion (using only aerial photographs) was less precise and accurate when compared to those obtained by means of regression estimation.

Parada, N. D. J.↗

NASA NTRS1984

Estimating optimal sampling unit sizes for satellite surveys

This paper reports on an approach for minimizing data loads associated with satellite-acquired data, while improving the efficiency of global crop area estimates using remotely sensed, satellite-based data. Results of a sampling unit size investigation are given that include closed-form models for both nonsampling and sampling error variances. These models provide estimates of the sampling unit sizes that effect minimal costs. Earlier findings from foundational sampling unit size studies conducted by Mahalanobis, Jessen, Cochran, and others are utilized in modeling the sampling error variance as a function of sampling unit size. A conservative nonsampling error variance model is proposed that is realistic in the remote sensing environment where one is faced with numerous unknown nonsampling errors. This approach permits the sampling unit size selection in the global crop inventorying environment to be put on a more quantitative basis while conservatively guarding against expected component error variances.

Hallum, C. R.↗