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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 613 records · Page 34
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Defect identification in simulated Bragg coherent diffraction imaging by automated AI

X-ray Bragg coherent diffraction imaging is a powerful technique for operando and in situ materials characterization and provides a unique means of quantifying the influence of one-dimensional (1D) and two-dimensional (2D) material defects on material response. However, obtaining full images from raw x-ray diffraction data is nontrivial and computationally intensive, precluding real-time experimental feedback. Here, we present a machine learning approach to identify the presence of crystalline line defects (edge and screw) in samples from the raw, 2D, coherent diffraction data without the need for image reconstruction through iterative phase retrieval. Further, we compare different approaches to designing neural networks for this application and demonstrate the potential of automated ML (autoML) approaches.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Resonant X-ray scattering of biological assemblies

Understanding the relationship between structure and function for biological assemblies can guide identification of new therapeutics, design of biomaterials, and development of biotechnological processes. Resonant X-ray scattering provides a chemically-specific approach to characterize complex biological structures based on anomalous or resonant scattering from a specific element or chemical moiety. Anomalous or resonant diffraction can provide structural details with high atomic resolution, while resonant X-ray scattering can provide structural details with lower resolution through tender or soft X-rays. Furthermore, we review applications, challenges, and opportunities for resonant X-ray scattering in the field of structural biology.

36 MATERIALS SCIENCE↗
NASA NTRS1967

Impact glass in the Cachari eucrite.

Preatmospheric hypervelocity impact black glass in Cachari eucrite studied by optical microscopy, electron microprobe and X-ray diffraction

VITREOUS MATERIAL↗
NASA NTRS1974

Stress-rupture strength and microstructural stability of W-HF-C wire reinforced superalloy composites

W-Hf-C/superalloy composites were found to be potentially useful for turbine blade applications on the basis of stress-rupture strength. The 100-and 1000-hour rupture strengths obtained for 70 volume percent fiber composites tested at 1090 C were 420 and 280 MN/sq m (61,000 and 41,000 psi). The investigation indicated that with better quality fibers, composites having 100- and 1000-hour rupture strengths of 570 and 370 MN/sq m (82,000 and 54,000 psi) may be obtained. Metallographic studies indicated sufficient fiber-matrix compatibility for long time applications at 1090 C for 1000 hours or more.

Petrasek, D. W.↗
NASA NTRS1974

Stress-rupture strength and microstructural stability of tungsten-hafnium-carbon-wire reinforced superalloy composites

Tungsten-hafnium-carbon - superalloy composites were found to be potentially useful for turbine blade applications on the basis of stress-rupture strength. The 100- and 1000-hr rupture strengths calculated for 70 vol. % fiber composites based on test data at 1090C (2000F) were 420 and 280 MN/m2 (61,000 and 41,000 psi, respectively). The investigation indicated that, with better quality fibers, composites having 100- and 1000-hr rupture strengths of 570 and 370 MN/m2 (82,000 and 54,000 psi, respectively), may be obtained. Metallographic studies indicated sufficient fiber-matrix compatibility for 1000 hr or more at 1090C (2000F).

Petrasek, D. W.↗
NASA NTRS1979

State-of-the-art of SiAlON materials

Research presented includes work on phase relations, crystal structure, synthesis, fabrication, and properties of various SiAlONs. The essential features of compositions, fabrication methods, and microstructure are reviewed. High temperature flexure strength, creep, fracture toughness, oxidation, and thermal shock resistance are discussed. These data are compared to those for some currently produced silicon nitride ceramics to assess the potential SiAlON materials for use in advanced gas turbine engines.

Dutta, S.↗
NASA NTRS1979

SPAR 5 experiment no. 74-30 agglomeration in immiscible liquids

The influence of gravity, cooling rate, and composition on the macro-and microstructure of liquid phase immiscible alloys were researched. Aluminum indium alloys of compositions 30, 40, 70, and 90 weight percent indium were processed aboard two sounding rocket flights, SPAR 2 and SPAR 5. Radiographic and metallographic examination of the SPAR 2 flight and ground base samples showed the expected separation at lg of the ground base alloys into indium rich and aluminum rich layers. The flight alloys produced an aluminum rich core surrounding by indium rich metal. The results obtained from the SPAR 5 40 and 70 weight percent indium alloys were essentially identical to those from SPAR 2. The 30 and 90 weight percent indium alloys also showed massive separation into configuration similar to the 40 and 70 weight percent indium alloys. The 90 weight percent indium alloy showed additional evidence that surface tension induced droplet migration had occurred in this alloy which could at least in part account for the observed structures.

Gelles, S.↗
NASA NTRS1980

State-of-the-art SiAlON materials

The state of the art of SiAlONs is examined. The review includes work on phase relations, crystal structure, synthesis, fabrication, and properties of various SiAlONs. The essential features of compositions, fabrication methods, and microstructure are reviewed. High temperature flexure strength, creep, fracture toughness, oxidation, and thermal shock resistance are discussed. These data are compared to those for some currently produced silicon nitride ceramics to assess the potential of SiAlON materials for use in advanced gas turbine engines.

Dutta, S.↗
NASA NTRS1979

State-of-the-art of SiAlON materials

The state of the art of 'SiAlONs' is reviewed, noting that the term has become a generic one applied to Si3N4 based materials. Attention is given to work on phase relations, crystal structure, synthesis, fabrication, and properties of various SiAlONs. Also discussed are the essential features of compositions, fabrication methods, and microstructures. In addition, consideration is given to high temperature flexure strength, creep, fracture toughness, oxidation, and thermal shock resistance. Finally, these data are compared to those for some currently produced silicon nitride ceramics to assess the potential of SiAlON materials for use in advanced gas turbine engines.

Dutta, S.↗
NASA NTRS1984

Microstructure and orientation effects on properties of discontinuous silicon carbide/aluminum composites

Composite panels containing up to 40 vol % discontinuous silicon carbide SiC whisker, nodule, or particulate reinforcement in several aluminum matrices are commercially fabricated and the mechanical properties and microstructual characteristics are evaluated. The yield and tensile strengths and the ductility are controlled primarily by the matrix alloy, the temper condition, and the reinforcement content. Particulate and nodule reinforcements are as effective as whisker reinforcement. Increased ductility is attributed to purer, more uniform starting materials and to more mechanical working during fabrication. Comparing mechanical properties with those of other aluminum alloys shows that these low cost, lightweight composites demonstrate very good potential for application to aerospace structures.

Mcdanels, D. L.↗
NASA NTRS1986

Dendrite characteristics in directionally solidified Pb-8 pct Au and Pb-3 pct Pd alloys

An investigation of Pb-8 pct Au and Pb-3 pct Pd alloy specimens which have been partially directionally solidified and then quenched is performed in order to characterize their dendritic microstructural details and solute composition profiles. A controlled sectioning technique is employed to measure dendrite tip radii. It is found that most of the observed behavior is predicted quite well by a modification of the Burden and Hunt (1974) model proposed by Laxmanan (1984), in addition to the models based on the marginal stability approach. Results indicate that quantitative comparison of the primary arm spacing measurements can not form the basis of distinguishing among the various dendrite growth models in a positive temperature gradient.

Tewari, S. N.↗
NASA NTRS1987

Preliminary investigation of inertia friction welding B2 aluminides

An attempt is made to achieve inertia friction-welding in FeAl and NiAl samples, taking into account their intermetallics' compositions, extrusion parameters, and microstructural data. The energy required for the weld is stored in a rotating flywheel mass attached to one of the two pieces to be joined; when enough energy is introduced, the flywheel is disconnected and an axial load is applied which forces the spinning piece against the stationary one, converting the energy into heat by means of friction. Due to the inherent brittleness of the aluminides, a step-load program was used in which an initial, low-pressure heat buildup increased the work pieces' ductility.

Whittenberger, J. Daniel↗
NASA NTRS1993

Microchemical analysis of the SCS-6 silicon carbide fiber

A detailed quantitative study of the microstructural variation of chemical composition of chemically vapor-deposited commercial SiC SCS-6 fiber is presented. Chemical etching and various electron-optical techniques including SEM, TEM, scanning Auger microscopy, AES, and parallel electron energy loss spectroscopy are used to analyze the chemical composition of the as-received fiber. In addition, some results on stereology of the high-temperature annealed fiber are presented. The results show that the carbon-to-silicon atom ratio in the SiC layers decreases in a stepwise fashion from about 3:2 to about 1:1 in going from the innermost layer to the outermost layer.

Ning, Xian-Jie↗
NASA NTRS1992

The effect of fiber microstructure on evolution of residual stresses in silicon carbide/titanium aluminide composites

This paper examines the effect of the morphology of the SCS6 silicon carbide fiber on the evolution of residual stresses in SiC/Ti composites. A micromechanics model based on the concentric cylinder concept is presented which is used to calculate residual stresses in a SiC/Ti composite during axisymmetric cooling by a spatially uniform temperature change. The silicon carbide fiber is modeled as a layered material with five distinct transversely isotropic and orthotropic, elastic layers, whereas the titanium matrix is taken to be isotropic, with temperature-dependent elastoplastic properties. The results arc compared with those obtained based on the assumption that the silicon carbide fiber is isotropic and homogeneous.

Pindera, Marek-Jerzy↗
NASA NTRS1994

Processing and Mechanical Properties of Directionally Solidified NiAl/NiAlTa Alloys

Promising creep strengths were found for a directionally solidified NiAl-NiAlTa alloy when compared to other NiAl based intermetallics. The directionally solidified alloy had an off-eutectic composition that resulted in microstructures consisting of NiAl dendrites surrounded by aligned eutectic regions. The room temperature toughness of the two phase alloy was similar to that of polycrystalline NiAl even with the presence of the brittle Laves phase NiAlTa. Alloying additions that may improve the room temperature toughness by producing multiphase alloys are discussed.

Johnson, D. R.↗