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At least 613 records · Page 34

Delta Method Application for the Correlation of IR Detector Thermal Parasitic Loads with Statistically Accurate Results

The Linear Etalon Imaging Spectral Array (LEISA) is a cryogenic IR detector that is passively cooled below 110K. LEISA is part of the L’Ralph instrument, which is going on the Lucy mission, with planned flyby’s of the Trojan asteroids around 5.5 AU. One of the primary thermal challenges is to successfully quantify each significant parasitic heat flow value with statistical certainty.Simulation of flight-like thermal environments and correlation of thermal models is an important part of this challenge, which can be critical for thermally sensitive systems such as cryogenic detectors that are passively cooled. It is common practice during TVAC to achieve several thermal balance points and then to correlate several design variables in order to achieve the closest match to all balance points tested. This approach lends itself to high levels of uncertainty in the correlated values due to the cumulative effect of absolute temperature uncertainty and differences between the sensors used for the measurement. Accuracy can be improved with the use of more accurate sensors, by calibrating all sensors with respect to each other, and by using Zero-Q methodologies, all of which add cost and complexity to the test.The Delta Method uses the difference in temperature caused by the changes in the boundary conditions to calculate heat flows and/or thermal resistances across temperature differentials. This eliminates the problem of high uncertainties with absolute temperature measurements, and yields statistically accurate results down to the sensor resolution of 1mK at < 100K, by taking the sensor’s calibration errors out of the equation. During testing, this method relies on parametric variations around an initial balance point, by varying the boundary conditions of the different parasitic heat sources. The Delta Method, as well as its application on the LEISA thermal test, will be discussed in detail.

Daniel G. Bae↗

Investigation of problems associated with solid encapsulation of high voltage electronic assemblies; also Reynolds connector study

Electric breakdown prevention in vacuum and encapsulation of high voltage electronic circuits was studied. The lap shear method was used to measure adhesive strengths. The permeation constants of air at ambient room temperature through four different space-grade encapsulants was measured. Order of magnitude was calculated for the time that air bubble pressures drop to the corona region. High voltage connectors with L-type cable attached were tested in a vacuum system at various pressures. The cable system was shown to suppress catastrophic breakdown when filled with and surrounded by gas in the corona region of pressures, but did not prove to be completely noise free.

Bever, R. S.↗

Test methods and design allowables for fibrous composites. Volume 2

Topics discussed include extreme/hostile environment testing, establishing design allowables, and property/behavior specific testing. Papers are presented on environmental effects on the high strain rate properties of graphite/epoxy composite, the low-temperature performance of short-fiber reinforced thermoplastics, the abrasive wear behavior of unidirectional and woven graphite fiber/PEEK, test methods for determining design allowables for fiber reinforced composites, and statistical methods for calculating material allowables for MIL-HDBK-17. Attention is also given to a test method to measure the response of composite materials under reversed cyclic loads, a through-the-thickness strength specimen for composites, the use of torsion tubes to measure in-plane shear properties of filament-wound composites, the influlence of test fixture design on the Iosipescu shear test for fiber composite materials, and a method for monitoring in-plane shear modulus in fatigue testing of composites.

Chamis, Christos C.↗

Closed-form analytical solutions of high-temperature heat pipe startup and frozen startup limitation

Previous numerical and experimental studies indicate that the high-temperature heat pipe startup process is characterized by a moving hot zone with relatively sharp fronts. Based on the above observation, a flat-front model for an approximate analytical solution is proposed. A closed-form solution related to the temperature distribution in the hot zone and the hot zone length as a function of time are obtained. The analytical results agree well with the corresponding experimental data, and provide a quick prediction method for the heat pipe startup performance. Finally, a heat pipe limitation related to the frozen startup process is identified, and an explicit criterion for the high-temperature heat pipe startup is derived. The frozen startup limit identified in this paper provides a fundamental guidance for high-temperature heat pipe design.

Cao, Y.↗

Dopant Studies in the BaCe0.9-xZrxY0.103- System

Protonic separation membranes for the hydrogen industry require thermo-chemical stability and high conductance. The perovskite BaCe0.9Y0.1O3- exhibits excellent proton conduction at high temperatures, but shows poor thermo-chemical tability. Substituting Zr for Ce in BaZr0.9Y0.1O3- improves the thermo-chemical stability but reduces proton conduction. The objective of this work was to study the optimization of protonic conductance and thermo-chemical by changing the ratio of Ce to Zr in BaCe0.9-xZrxY0.1O3-. To elucidate the dopant effect, co-precipitation method has been developed to produce single phase perovskites of composition BaCe0.9-xZrxY0.1O3- (0=x=0.9). The co-precipitation method has been optimized to yield high purity and homogeneous powders with a particle size of 100-200 nm in diameter. The sintering characteristics were studied in temperature range of 1400-1600 C. The effect of Zr substitution on sintering behavior and thermo-chemical stability will be reported.

Zhong, Zhimin↗

Thermionic Properties of Carbon Based Nanomaterials Produced by Microhollow Cathode PECVD

Thermionic emission is the process in which materials at sufficiently high temperature spontaneously emit electrons. This process occurs when electrons in a material gain sufficient thermal energy from heating to overcome the material's potential barrier, referred to as the work function. For most bulk materials very high temperatures (greater than 1500 K) are needed to produce appreciable emission. Carbon‐based nanomaterials have shown significant promise as emission materials because of their low work functions, nanoscale geometry, and negative electron affinity. One method of producing these materials is through the process known as microhollow cathode PECVD. In a microhollow cathode plasma, high energy electrons oscillate at very high energies through the Pendel effect. These high energy electrons create numerous radical species and the technique has been shown to be an effective method of growing carbon based nanomaterials. In this work, we explore the thermionic emission properties of carbon based nanomaterials produced by microhollow cathode PECVD under a variety of synthesis conditions. Initial studies demonstrate measureable current at low temperatures (approximately 800 K) and work functions (approximately 3.3 eV) for these materials.

Haase, John R.↗

Efficient High-Pressure State Equations

A method is presented for a relatively accurate, noniterative, computationally efficient calculation of high-pressure fluid-mixture equations of state, especially targeted to gas turbines and rocket engines. Pressures above I bar and temperatures above 100 K are addressed The method is based on curve fitting an effective reference state relative to departure functions formed using the Peng-Robinson cubic state equation Fit parameters for H2, O2, N2, propane, methane, n-heptane, and methanol are given.

Harstad, Kenneth G.↗

A Global Assessment of Added Value in the SMAP Level-4 Soil Moisture Product Relative to Its Baseline Land Surface Model

The Soil Moisture Active Passive (SMAP) Level-4 product provides enhanced soil moisture estimates by assimilating SMAP brightness temperature observations into a land surface model. Here, an unbiased qualitative estimate of the relative skill of SMAP Level-4 and model-only surface soil moisture (versus true soil moisture) is derived using only one additional noisy (but independent) soil moisture product. The method is applied globally and verified using high-quality, ground-based measurements where available. Results demonstrate that assimilating SMAP brightness temperature has relatively little impact in data-rich areas like the United States and Europe. In contrast, much larger improvement is observed in data-sparse regions, including much of Africa and central Australia, where model-only simulations are disproportionately impacted by low-quality model forcing. Therefore, ground validation conducted in data-rich areas does not adequately sample the added value of SMAP data assimilation for data-sparse regions and substantially underestimates the added skill provided by the SMAP Level-4 system.

SMAP L4↗

Improving the efficiency of GaP LED's which emit green light

A study of techniques for preparing n-type material and junctions which yield the most consistent high diode efficiency values high lighted the role that Ga vacancies and/or associated defects play in reducing the green luminescent efficiency of n-type GaP. A useful method for obtaining good quality material was developed. It is shown that junction formation at high temperatures in a process where the n to p transition occurs without removing the substrate from the furnace yields devices superior to those obtained by diffusion or double epitaxy in the conventional manner previously used for GaP junction formation.

Ladany, I.↗

Melting of iron by significant structure theory

From Eyring's method of significant structures, a partition function is derived for liquid iron. The solid at high temperature is described in the Einstein approximation. Magnetic and electronic contributions to the thermodynamic properties of both the liquid and solid phases are considered. The model is compatible with properties (thermal expansion, compressibility, heat capacity, entropy of melting, and volume change on melting) at one atm. The melting temperature at high pressure is found by satisfying the requirement that the Gibbs free energies of the liquid and solid phases are equal at the melting temperature. Under conditions at the earth's core-mantle boundary, the melting temperature of iron is greater than approximately 5000 K, and under inner-outer core conditions the melting temperature is greater than approximately 7000 K. These estimates are consistent with the Lindemann melting law, but not with the Kraut-Kennedy melting law.

Leppaluoto, D. A.↗

Elementary solutions of coupled model equations in the kinetic theory of gases

The method of elementary solutions is employed to solve two coupled integrodifferential equations sufficient for determining temperature-density effects in a linearized BGK model in the kinetic theory of gases. Full-range completeness and orthogonality theorems are proved for the developed normal modes and the infinite-medium Green's function is constructed as an illustration of the full-range formalism. The appropriate homogeneous matrix Riemann problem is discussed, and half-range completeness and orthogonality theorems are proved for a certain subset of the normal modes. The required existence and uniqueness theorems relevant to the H matrix, basic to the half-range analysis, are proved, and an accurate and efficient computational method is discussed. The half-space temperature-slip problem is solved analytically, and a highly accurate value of the temperature-slip coefficient is reported.

Kriese, J. T.↗

Preliminary design of a Primary Loop Pump Assembly (PLPA), using electromagnetic pumps

A preliminary design study of flight-type dc conduction-permanent magnetic, ac helical induction, and ac linear induction pumps for circulating 883 K (1130 F) NaK at 9.1 kg/sec (20 lb/sec) is described. Various electromagnetic pump geometrics are evaluated against hydraulic performance, and the effects of multiple windings and numbers of pumps per assembly on overall reliability were determined. The methods used in the electrical-hydraulic, stress, and thermal analysis are discussed, and the high temperature electrical materials selected for the application are listed.

Moss, T. A.↗

Inversion of infrared limb emission measurements for temperature and trace gas concentrations

Limb emission measurements are characterized by sharp weighting functions at high altitudes, and for temperature determinations, strongly nonlinear dependence of the weighting function on the temperature. Several methods for inverting this type of measurement have been described and used, including iterative, statistical, nonlinear and approximate direct approaches. These approaches are described and advantages and disadvantages of each are outlined.

Gille, J. C.↗

Artificial Voids In Ceramic Materials

Method for creating voids in ceramic specimens developed. Silicon carbide and silicon nitride are high-temperature structural ceramic materials considered for applications in advanced gas-turbine engines. Ability to detect and characterize voids (by sizes, shapes, and locations) in structural ceramics vital for increasing strengths and reliabilities of materials. Small holes made deliberately to help quantify techniques of nondestructive evaluation.

Roth, Don J.↗

Relationship between fatigue life in the creep-fatigue region and stress-strain response

On the basis of mechanical tests and metallographic studies, strainrange partitioned lives were predicted by introducing stress-strain materials parameters into the Universal Slopes Equation. This was the result of correlating fatigue damage mechanisms and deformation mechanisms operating at elevated temperatures on the basis of observed mechanical and microstructural behavior. Correlation between high temperature fatigue and stress strain properties for nickel base superalloys and stainless steel substantiated the method. Parameters which must be evaluated for PP- and CC- life are the maximum stress achievable under entirely plastic and creep conditions respectively and corresponding inelastic strains, and the elastic modulus. For plasticity/creep interaction conditions (PC and CP) two more pairs of stress strain parameters must be ascertained.

Berkovits, A.↗

TiCl4 as a source of TiO2 particles for laser anemometry measurements in hot gas

A method of reacting TiCl4 with water saturated gaseous nitrogen (GN2) at the entrance into a high temperature gas flow is described. The TiO2 particles formed are then entrained in the gas flow and used as seed particles for making laser anemometry (LA) measurements of the flow velocity distribution in the hot gas. Scanning electron microscope photographs of the TiO2 particles are shown. Data rate of the LA processor was measured to determine the amount of TiO2 formed. The TiCl4 and mixing gas flow diagram is shown. This work was performed in an open jet burner.

Weikle, Donald H.↗

Relationship between fatigue life in the creep-fatigue region and stress-strain response

On the basis of mechanical tests and metallographic studies, strainrange partitioned lives were predicted by introducing stress-strain materials parameters into the Universal Slopes Equation. This was the result of correlating fatigue damage mechanisms and deformation mechanisms operating at elevated temperatures on the basis of observed mechanical and microstructural behavior. Correlation between high temperature fatigue and stress strain properties for nickel base superalloys and stainless steel substantiated the method. Parameters which must be evaluated for PP- and CC- life are the maximum stress achievable under entirely plastic and creep conditions respectively and corresponding inelastic strains, and the two more pairs of stress strain parameters must be ascertained.

Berkovits, A.↗

Comparison between the magnetic and transport critical current densities in high critical current density melt-textured yttrium barium copper-oxide

Using a recently developed pulsed critical current density (Jc) measuring system, the Jc of the high-Jc melt-textured YBa2Cu3O(7-delta) (Y123) bulk samples has been determined. I-V curves with a voltage resolution of 0.5 microV were obtained, and transport Jc's along the a-b plane as high as 7.2 x 10 to the 4th A/sq cm were extracted. These results are comparable to the values obtained magnetically. On the other hand, transport Jc along the c axis were found to be two orders of magnitude smaller, even though the magnetic Jc along the c axis is only about five times smaller than Jc along the a-b plane. It is suggested that for the high-temperature superconducting materials which are highly anisotropic, caution should be taken when using the nontransport magnetic methods to determine Jc.

Gao, L.↗